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  • Analytical Chemistry and Spectroscopy  (358)
  • EARTH RESOURCES AND REMOTE SENSING  (265)
  • SPACE RADIATION  (179)
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  • 1
    Electronic Resource
    Electronic Resource
    Evaluation of dead time calculation in liquid chromatography using a linearization procedure for homologous series (1987)
    Weinheim : Wiley-Blackwell
    Journal of High Resolution Chromatography 10 (1987), S. 191-200 
    Details
    ISSN: 0935-6304
    Keywords: Liquid chromatography, HPLC ; Dead time calculation ; Homologous series ; Chemistry ; Analytical Chemistry and Spectroscopy
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology
    Notes: A mathematical method for the calculation of the dead time (tm) in HPLC was evaluated using a computer simulation approach, in which artificial perturbations were introduced to Simulated homolog retention times. The calculation was based on a modified and extended Grobler and Bálisz (GB) method. Investigated wav how the precision of the calculated tM is affected by: statistical fluctuations in retention times and which, and how many homolog retention times are used. Based on these simulations a two-step procedure for the tM calculation is proposed: In the first step the linearity of log tR, n vs carbon number n is checked using as many homolog retention times as possible. The slope value bo of the first linear regression in the GB method is used for the selection of homolog retention times in the final tM calculation. In the second step the optimal selection of homologs is made and the final tM calculation is carried out. Guidelines for homolog selection are given.
    Additional Material: 2 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/jhrc.1240100407
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  • 2
    Electronic Resource
    Electronic Resource
    Etude en RMN du 13C de Mérocyanines Benzimidazoliniques (1978)
    Chichester : Wiley-Blackwell
    Organic Magnetic Resonance 11 (1978), S. 493-498 
    Details
    ISSN: 0030-4921
    Keywords: Chemistry ; Analytical Chemistry and Spectroscopy
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology
    Description / Table of Contents: A series of α-oxobenzimidazolinic merocyanines differently substituted on the ‘phenolate’ part and bearing a paraffinic chain on one heterocyclic nitrogen, has been studied by 13C NMR. Electron donating substituents bring about an increase of the electronic density on the 3 methine carbon and an increase of the alternation of electron density on the 3,4-dimethine bridge. A bathochromic shift of the lower energy electronic transition is also observed. Furthermore, the low field resonance of the 3 methine proton is probably due to a specific interaction between this proton and the ‘phenolate’ oxygen atom. This implies the existence of a favoured trans configuration for merocyanine dyes.
    Notes: Une série de mérocyanines α-oxo benzimidazoliniques diversement substituées sur la partie ‘phénolate’ et possédant une chaǐne grasse sur l'un des azotes hétérocycliques, a été étudiée en RMN du carbone- 13. Des substituants donneurs d'électrons provoquent une augmentation de la densité électronique sur le carbone méthinique C-3 et une augmentation de l'alternance de la distribution de charge sur le pont diméthinique 3,4. Corrélativement un déplacement bathochrome de la transition électronique de plus basse énergie est observé. Par ailleurs, l'apparition de la résonance à champ faible du proton méthinique H-3 semble due à une interaction spécifique intervenant entre ce proton et l'atome d'oxygène ‘phénolate’, ce qui suppose l'existence d'une configuration trans privilégiée pour les mérocyanines.
    Additional Material: 1 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/mrc.1270111004
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  • 3
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    The effects of merging TM and A/C radar on wetland classification (1985)
    In:  CASI
    Details
    Publication Date: 2006-02-14
    Description: While radar does not provide detailed begetation discrimination, it provide the means to separate areas of different moisture conditions. Thus, the use of LANDSAT Thematic Mapper (TM) in conjunction with the microwave data was attempted. If successful, information on shoreline cover, emergent wetland vegetation and extent, and submerged grassbeds would provide much needed data for planning and maintenance of wetlands. Originally, the goal was to determine the accuracy with which one could categorize various types of vegetation and land use within an inland wetland using LANDSAT TM data. First, a Level 1/2 supervised classification was performed. Following a more detailed ground trust survey, a Level 3 classification was done. Aircraft L-band radar data were received and the decision was made to merge the TM and L-band data and assess whether vegetation catagories within the wetland areas could be better defined. Preliminary results indicate vegetation delineation is improved for open agricultural areas and water, but other features are more confused.
    Keywords: EARTH RESOURCES AND REMOTE SENSING
    Type: JPL NASA(JPL Aircraft SAR Workshop Proc.; p 37-38
    Format: text
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    NASA TECHNICAL REPORTS
  • 4
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    Implications of new measurements of O-16 + p + C-12,13, N-14,15 for the abundances of C, N isotopes at the cosmic ray source (1985)
    In:  CASI
    Details
    Publication Date: 2019-06-28
    Description: The fragmentation of a 225 MeV/n O-16 beam was investigated at the Bevalac. Preliminary cross sections for mass = 13, 14, 15 fragments are used to constrain the nuclear excitation functions employed in galactic propagation calculations. Comparison to cosmic ray isotonic data at low energies shows that in the cosmic ray source C-13/C approximately 2% and N-14/0=3-6%. No source abundance of N-15 is required with the current experimental results.
    Keywords: SPACE RADIATION
    Type: OG-4.3-2 , 19th Intern. Cosmic Ray Conf - Vol. 2; p 80-83; NASA-CP-2376-VOL-2
    Format: application/pdf
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    NASA TECHNICAL REPORTS
  • 5
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    Spatial variability of surface temperature as related to cropping practice with implications for irrigation management (1980)
    In:  Other Sources
    Details
    Publication Date: 2019-07-13
    Description: Crop stress measured using thermal infrared emission is evaluated with the stress-degree-day (SDD) concept. Throughout the season, the accumulation of SDD during the reproductive stage of growth is inversely related to yield. This relationship is shown for durum wheat, hard red winter wheat, barley, grain sorghum and soybeans. It is noted that SDD can be used to schedule irrigations for maximizing yields and for applying remotely sensed data to management of water resources. An airborne flight with a thermal-IR scanner was used to examine the variability in temperature that may exist from one field to another and to determine realistic within-field temperature variations. It was found that the airborne and the ground-based data agreed very well and that there was less variability in the fields that were completely covered with crops than those of bare soil.
    Keywords: EARTH RESOURCES AND REMOTE SENSING
    Type: International Symposium on Remote Sensing of Environment; Apr 23, 1980 - Apr 30, 1980; San Jose; Costa Rica
    Format: text
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    NASA TECHNICAL REPORTS
  • 6
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    Spectral properties of the X-ray objects GX 3 plus 1, GX 354-5 and Sco XR-1. (1968)
    In:  Other Sources
    Details
    Publication Date: 2011-08-12
    Description: Spectral properties of celestial X ray objects near galactic center from balloon observation, noting supernova origin and magnetic bremsstrahlung emission mechanism
    Keywords: SPACE RADIATION
    Type: ; ADEMIE DES SCIENCES
    Format: text
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    NASA TECHNICAL REPORTS
  • 7
    Electronic Resource
    Electronic Resource
    Practical considerations in the use of stable isotope labelled compounds as tracers in clinical studies (1989)
    Chichester : Wiley-Blackwell
    Biological Mass Spectrometry 18 (1989), S. 321-327 
    Details
    ISSN: 0887-6134
    Keywords: Chemistry ; Analytical Chemistry and Spectroscopy
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology
    Notes: Increasingly widespread usage of stable isotope tracers to aid clinical diagnosis and support basic research has stemmed from both advances in mass spectrometry and the availability of competitively priced labelled compounds. Stable isotopes have been used generally to investigate normal and abnormal metabolic pathways, to estimate energy expenditure and body composition and to quantitate substrate flux and oxidation rates. Despite the fact that the underlying principles relating to the use of stable isotopes for in vivo studies are straightforward, careful consideration must be given to all aspects of human studies. This review highlights some of these, including choice of label and tracer molecule, mode of tracer administration and sampling site, analytical instrumentation, interpretation of data and ethical constraints.
    Additional Material: 1 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/bms.1200180507
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  • 8
    Electronic Resource
    Electronic Resource
    Mathematical model for the optimization of the reaction between 2,3-bis(m-tolyl)quinolizinium bromide and piperidine using a factorial design (1992)
    New York, NY : Wiley-Blackwell
    Journal of Chemometrics 6 (1992), S. 1-10 
    Details
    ISSN: 0886-9383
    Keywords: Derivatization reaction ; Factorial design ; Chemistry ; Analytical Chemistry and Spectroscopy
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology
    Notes: A number of nucleophiles have been successfully identified and quantified using the Kröhnke reaction with 2,3-diphenyl derivatives of quinolizinium salts. Optimization of the reaction conditions by means of a mathematical model involving analysis of the response surface has led to a better understanding of the factors exerting an influence on the above reaction.The parameters chosen were temperature, reaction time, base concentration, water concentration and nucleophile concentration. The reaction was developed in polar aprotic solvents (acetone, acetonitrile). To facilitate the nucleophilic attack, the presence of an organic base (triethylamine) was necessary, although concentrations in excess of 0·15M did not alter the development of the reaction. Since pharmaceutical solutions are often aqueous, the influence of water on the reaction was studied. Low water volumes have no significant influence on the opening of the quinolizinium ring by the nucleophilic reagent. However, when the water proportion exceeded that of the organic solvent, the fluorescence intensity was lower than expected. Development of the fluorescent reaction product was first detected 5 min after the reaction started. The fluorescence intensity reached its optimum value after 138 min.
    Additional Material: 2 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/cem.1180060102
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  • 9
    Electronic Resource
    Electronic Resource
    Separation of structually similar, biologically active peptides from their impurities (1979)
    Weinheim : Wiley-Blackwell
    Journal of High Resolution Chromatography 2 (1979), S. 255-256 
    Details
    ISSN: 0935-6304
    Keywords: Liquid Chromatography, HPLC ; Peptide analysis ; Angiotensin I and II, peptide hormones, resolution of impurities ; Chemistry ; Analytical Chemistry and Spectroscopy
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology
    Additional Material: 1 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/jhrc.1240020516
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  • 10
    Electronic Resource
    Electronic Resource
    Simple press-fit connectors for flexible fused silica tubing in gas-liquid chromatography (1986)
    Weinheim : Wiley-Blackwell
    Journal of High Resolution Chromatography 9 (1986), S. 295-297 
    Details
    ISSN: 0935-6304
    Keywords: Gas-liquid chromatography, GC ; Fused silica tubing ; Connector ; Coupling ; Press-fit ; Chemistry ; Analytical Chemistry and Spectroscopy
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology
    Additional Material: 4 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/jhrc.1240090510
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