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  • 101
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    [S.l.] : American Institute of Physics (AIP)
    Review of Scientific Instruments 71 (2000), S. 2800-2806 
    ISSN: 1089-7623
    Source: AIP Digital Archive
    Topics: Physics , Electrical Engineering, Measurement and Control Technology
    Notes: In electroconvection experiments with planarly aligned nematic liquid crystals the director orientation is, conventionally, fixed through a mechanical treatment (rubbing) of the polymer-coated electrodes. Without rubbing, on the other hand, the flow direction during sample filling imposes the director orientation. We report atomic force microscopy and x-ray measurements that show an anisotropy in the polymer surface structure on several scales as a result of the rubbing. In particular we observe a fish-bone structure on a 10 nm scale. We visualize the orientation of the director both during and after filling the system using the electroconvection pattern. This is a convenient tool for exploring new director configurations. We confirm for the observed surface structure that when flow and surface designate different orientations, the mechanical surface treatment dominates. We have been able to obtain regions with radial director orientation of millimeter size. Such an alignment renders possible new types of electroconvection experiments. © 2000 American Institute of Physics.
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  • 102
    ISSN: 1089-7623
    Source: AIP Digital Archive
    Topics: Physics , Electrical Engineering, Measurement and Control Technology
    Notes: We present an experimental setup for the investigation of the processes occurring during the deposition of mass-selected clusters on a well-defined surface. The sample is analyzed in situ by two complementary methods: thermal energy atom scattering (TEAS) and scanning tunneling microscopy (STM). TEAS is used to study the dynamical processes during the deposition and to gather statistical information about the resulting structures on the surface. Subsequent STM measurements allow us to investigate the collision outcome on an atomic scale. The setup is highly versatile and guarantees ultra-high-vacuum conditions and cryogenic temperatures ((approximate)30 K) of the sample at all times even during sample transfer. Clusters are produced in a CORDIS-type cluster source. A new compact multichannel effusive He source in combination with a new Wien-filter-based He detector are used for TEAS measurements. The new low-temperature STM allows measurements in a temperature range between 8 and 450 K. Atomic resolution on the Pt(111) surface is regularly observed at Tsample=8 K. The performances of the setup are illustrated by STM images obtained after the deposition of Ag7+ clusters with Ekin=95 and 1000 eV on bare Pt(111) and by measurements made of the deposition of Ag7+ clusters with Ekin=20 eV in a Xe–rare-gas matrix adsorbed on Pt(111). © 2000 American Institute of Physics.
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  • 103
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    [S.l.] : American Institute of Physics (AIP)
    Review of Scientific Instruments 71 (2000), S. 2839-2842 
    ISSN: 1089-7623
    Source: AIP Digital Archive
    Topics: Physics , Electrical Engineering, Measurement and Control Technology
    Notes: In situ temperature monitoring is extremely important in plasma immersion ion implantation (PIII) of semiconductors. For instance, the silicon wafer must be heated to 600 °C or higher in separation by plasma implantation of oxygen, and in the PIII/ion-cut process, the wafer temperature must remain below 300 °C throughout the experiment. In this article, we present a thermocouple-based direct temperature measurement system for planar samples such as silicon wafers. In order to ensure reliable high-voltage operation and overall electrical isolation, the thermocouple assembly and wires are integrated into the sample chuck and feedthrough. Hydrogen plasma immersion ion implantation is performed in silicon to demonstrate the effectiveness and reliability of the device. Our experimental results indicate that instrumental parameters such as implantation voltage, pulse duration, and pulsing frequency affect the sample temperature to a different extent. The measured temperature rise is higher than that predicted by a theoretical model based on the Child–Langmuir law. The discrepancy is attributed to the finite-sample size and the nonplanar, conformal plasma sheath. © 2000 American Institute of Physics.
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  • 104
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    [S.l.] : American Institute of Physics (AIP)
    Review of Scientific Instruments 71 (2000), S. 2855-2861 
    ISSN: 1089-7623
    Source: AIP Digital Archive
    Topics: Physics , Electrical Engineering, Measurement and Control Technology
    Notes: This article compares resonant ultrasound spectroscopy (RUS) and other resonant methods for the determination of viscoelastic properties such as damping. RUS scans from 50 to 500 kHz were conducted on cubical specimens of several materials including brass, aluminum alloys, and polymethyl (methacrylate) (PMMA), a glassy polymer. Comparison of damping over the frequency ranges for broadband viscoelastic spectroscopy (BVS) and RUS for indium tin alloy in shear modes of deformation discloses a continuation of the tan δ power-law trend for ultrasonic frequencies up to 300 kHz. For PMMA, resonant peaks were sufficiently broad that higher modes in RUS began to overlap. Tan δ via RUS and BVS for PMMA agreed well in the frequency range where the methods overlap. RUS is capable of measuring tan δ as high as several percent at the fundamental frequency. Since higher modes are closely spaced, it is impractical to determine tan δ above 0.01–0.02 at frequencies other than the fundamental. © 2000 American Institute of Physics.
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  • 105
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    [S.l.] : American Institute of Physics (AIP)
    Review of Scientific Instruments 71 (2000), S. 2867-2872 
    ISSN: 1089-7623
    Source: AIP Digital Archive
    Topics: Physics , Electrical Engineering, Measurement and Control Technology
    Notes: The simple techniques generally used to investigate the biomechanical properties associated with the respiratory process are able to identify only basic characteristics, just supplying an initial representation of the complex behavior of the respiratory system. A much more detailed description can be obtained by the forced oscillation technique (FOT). Requiring very little cooperation of the subject, this technique allows a noninvasive evaluation of the mechanical impedance of the respiratory system. Although the FOT has a great scientific and clinical potential, this is attended by technical difficulties and has yet to be put to widespread use. In this context, this work describes a new flexible, open architecture, virtual-instrument-based impedance spectrometer for the FOT. After the design details are described, the system accuracy is evaluated investigating mechanical models simulating normal and individuals with restrictive disease. This analysis revealed errors smaller than 4% in modulus and 7° in phase. Experimental results obtained in a normal and an asthmatic subject, presented as examples, revealed mean resistance in asthmatic (5.72 cm H2O/l/s) higher than in normal (2.47 cm H2O/l/s). The mean-reactance curve revealed higher resonance frequency in the asthmatic subject (∼29 Hz) than in the normal one (∼9 Hz). A higher influence of the upper airways impedance of the asthmatic individual was also observed. These results are in close agreement with physiological fundamentals, supplying substantial evidence that this instrument can contribute to the production of more detailed biophysical respiratory descriptions and composes an improved basis for the fast and easy implementation of complex medical research projects. © 2000 American Institute of Physics.
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  • 106
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    [S.l.] : American Institute of Physics (AIP)
    Review of Scientific Instruments 71 (2000), S. 2873-2881 
    ISSN: 1089-7623
    Source: AIP Digital Archive
    Topics: Physics , Electrical Engineering, Measurement and Control Technology
    Notes: We describe a high transition temperature superconducting, first-order gradiometer intended for biomagnetic measurements in an unshielded environment. The gradiometer involves a single-layer, planar flux transformer with two loops of unequal size, the smaller of which is inductively coupled to the pickup loop of a directly coupled magnetometer. In this configuration, the presence of the flux transformer reduces the sensitivity of the magnetometer by only about 5%. The flux transformer is patterned in a thin film of YBa2Cu3O7−δ deposited on a 100 mm diam wafer, and has a baseline of 48 mm. The flux transformer and magnetometer substrates are permanently bonded together in a flipchip arrangement. The common mode rejection of uniform magnetic field fluctuations in any direction is better than 1 part per 100. The outputs of two such gradiometers are subtracted to form a second-order gradiometer, which rejects first-order gradient fluctuations to about 1 part in 100. With the aid of three orthogonally mounted magnetometers, one can reduce the response of the gradiometers to uniform field fluctuations to below 100 ppm. This system is used to detect magnetic signals from the human heart in an unshielded environment. © 2000 American Institute of Physics.
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  • 107
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    [S.l.] : American Institute of Physics (AIP)
    Review of Scientific Instruments 71 (2000), S. 2890-2894 
    ISSN: 1089-7623
    Source: AIP Digital Archive
    Topics: Physics , Electrical Engineering, Measurement and Control Technology
    Notes: We present a technique for the control of a double pendulum suspension system used to carry the optical elements of a 30 m long Fabry–Pérot cavity, a prototype for the mode cleaner of the VIRGO experiment. The movement of the payload is sensed with a charge coupled device camera, and the feedback forces are applied to the intermediate stage of the suspension via coil–magnet systems. The control strategy is explained and the application of the system for the longitudinal locking of the cavity is demonstrated. © 2000 American Institute of Physics.
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  • 108
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    [S.l.] : American Institute of Physics (AIP)
    Review of Scientific Instruments 71 (2000), S. 2914-2921 
    ISSN: 1089-7623
    Source: AIP Digital Archive
    Topics: Physics , Electrical Engineering, Measurement and Control Technology
    Notes: We describe toroidal cross capacitors built to accurately measure the dielectric constant of gases. We tested the capacitors by measuring the dielectric polarizability of helium and argon at 7 and 50 °C at pressures up to 3 MPa. For helium, the results are consistent with the ab initio calculation of the molar polarizability and are limited by the uncertainties of the capacitance measurements. For argon, the results are consistent with the best previously published measurements of the polarizability and are limited by the uncertainties of the pressure measurements. Lessons learned are provided.
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  • 109
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    [S.l.] : American Institute of Physics (AIP)
    Review of Scientific Instruments 71 (2000), S. 2922-2927 
    ISSN: 1089-7623
    Source: AIP Digital Archive
    Topics: Physics , Electrical Engineering, Measurement and Control Technology
    Notes: We describe an instrument for local, instantaneous, noninvasive, simultaneous measurements of solid volume fraction and convective heat transfer at the wall of a vertical tube containing a relatively dense, entrained suspension of gas and fine solids. The instrument combines a small platinum coil and a guarded capacitance sensor. The capacitance sensor records instantaneous solid volume fraction in the near vicinity of the wall. The coil is maintained at constant temperature by a rapid anemometer bridge circuit. The vessel is wrapped in electric heaters to avoid artificially high rates associated with developing heat transfer and to minimize conduction losses from the coil. Using a model capturing these losses, convective heat transfer rates are inferred from the power input to the coil. The instrument is tested in a cold circulating fluidized bed riser. The temporal response of the thermal sensor is faster than 30 ms. © 2000 American Institute of Physics.
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  • 110
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    [S.l.] : American Institute of Physics (AIP)
    Review of Scientific Instruments 71 (2000), S. 2933-2937 
    ISSN: 1089-7623
    Source: AIP Digital Archive
    Topics: Physics , Electrical Engineering, Measurement and Control Technology
    Notes: A liquid-ambient-compatible thermal wave resonant cavity (TWRC) has been constructed for the measurement of the thermal diffusivity of liquids. The thermal diffusivities of distilled water, glycerol, ethylene glycol, and olive oil were determined at room temperature (25 °C), with four-significant-figure precision as follows: (0.1445±0.0002)×10−2 cm2/s (distilled water); (0.0922±0.0002)×10−2 cm2/s (glycerol); (0.0918±0.0002)×10−2 cm2/s (ethylene glycol); and (0.0881±0.0004)×10−2 cm2/s (olive oil). The liquid-state TWRC sensor was found to be highly sensitive to various mixtures of methanol and salt in distilled water with sensitivity limits 0.5% (v/v) and 0.03% (w/v), respectively. The use of the TWRC to measure gas evolution from liquids and its potential for environmental applications has also been demonstrated. © 2000 American Institute of Physics.
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  • 111
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    Review of Scientific Instruments 71 (2000), S. 2263-2266 
    ISSN: 1089-7623
    Source: AIP Digital Archive
    Topics: Physics , Electrical Engineering, Measurement and Control Technology
    Notes: Integrated diffractive/refractive microlens with dual focus point is introduced in detail in the view of design, microfabrication, and testing. Two manufacturing methods—milling and deposition directly by focused ion beam technology is discussed and compared. It was shown by testing results that the deposition method is more suitable to form the refractive spherical/aspherical lens and milling is suitable for microfabrication of diffractive optical elements. Focusing spot size (full width at half maximum) are 0.55 and 0.87 μm (λ=638 nm) for refractive and diffractive lens, respectively, with NA 0.35 and 0.5. © 2000 American Institute of Physics.
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  • 112
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    [S.l.] : American Institute of Physics (AIP)
    Review of Scientific Instruments 71 (2000), S. 2270-2278 
    ISSN: 1089-7623
    Source: AIP Digital Archive
    Topics: Physics , Electrical Engineering, Measurement and Control Technology
    Notes: A procedure for obtaining the correct hemispherical reflectance and transmittance of anisotropically scattering samples in focusing Coblentz spheres are presented. Consideration is taken not only to the angle-dependent detector efficiency and to multiple reflections between sample and detector, but a separation of the scattered light into a low and a high angle fraction is also introduced. To validate the formalism, the correction procedure is applied to six samples with different scattering characteristics in the visible and near-infrared region. The agreement with results from a double beam spectrophotometer, equipped with an integrating sphere, was found to be good. Without making the separation into high and low angle scattering, it was not possible to reach agreement between the results from the Coblentz and integrating spheres, and errors of the order of 10% could be obtained. © 2000 American Institute of Physics.
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  • 113
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    [S.l.] : American Institute of Physics (AIP)
    Review of Scientific Instruments 71 (2000), S. 2288-2291 
    ISSN: 1089-7623
    Source: AIP Digital Archive
    Topics: Physics , Electrical Engineering, Measurement and Control Technology
    Notes: Experimental investigation of laser output characteristics of an elemental copper vapor laser using a cylindrical grid electrode has been carried out. The grid electrode, which is placed at the inside of a cathode and separated 2 cm away from a cathode, is used for increasing the output power by improving the discharge characteristics. When the grid electrode is coupled with a peaking capacitor, it is observed that the peak voltage (voltage hold-off) in the pulsed discharge wave forms increases by about 20%. Also, the initial part of the discharge current pulse is reduced. The laser average output power increased from 16 to 21 W. Additionally, when applying dc voltage (0–100 V) to the grid electrode, the output power increased by around 6%. The effect of employing the grid electrode and the mechanisms responsible for the improved characteristics are discussed. © 2000 American Institute of Physics.
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  • 114
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    [S.l.] : American Institute of Physics (AIP)
    Review of Scientific Instruments 71 (2000), S. 2279-2282 
    ISSN: 1089-7623
    Source: AIP Digital Archive
    Topics: Physics , Electrical Engineering, Measurement and Control Technology
    Notes: A novel method to measure low absorption of pulsed laser radiation by materials with high optical transparency is demonstrated. The absorbed energy generates a temperature gradient and thus a refractive index profile. A probe laser beam is deflected by the refractive index profile and its deflection is a measure of pure volume absorption without interference from surface effects. Numerical calculations were carried out to estimate the sensitivity of the discussed laser induced deflection (LID) arrangement and to optimize the path of the probe beam in relation to the irradiated field within the sample. The experimental results agree sufficiently with numerical calculations by finite element method combined with raytracing procedures. Because the transparency is not measured directly a calibration is necessary. To provide this, a sample with known bulk absorption coefficient and thermal properties was used. In order to compensate probe beam fluctuations in air outside the sample, a double beam arrangement was designed. The LID method is applied to investigate fused silica with high ultraviolet (UV) transparency under KrF excimer laser irradiation (λ=248 nm). A He/Ne laser serves as probe beam source. Using sample dimensions of 20×20×10 mm3 and UV beam cross sections of 5×5 mm2 absorbed power down to 1 mW is detected. At typical irradiation conditions (50 s−1, 300 mJ/cm2), this value corresponds with an absorption coefficient of around 2.5×10−4 cm−1. The limitation of the absorption measurement depends on the input power of the pump laser. © 2000 American Institute of Physics.
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  • 115
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    [S.l.] : American Institute of Physics (AIP)
    Review of Scientific Instruments 71 (2000), S. 2296-2300 
    ISSN: 1089-7623
    Source: AIP Digital Archive
    Topics: Physics , Electrical Engineering, Measurement and Control Technology
    Notes: A new hardware compensation method reducing displacement measurement errors, caused by tilt of the index scale in a moiré linear encoder, has been developed. In conventional moiré linear encoders, the detectors are aligned perpendicular to the line of the moiré fringes and this structure is very sensitive to an unwanted tilt of the gratings. In this article, a newly designed grating, called a phase-modulated grating, is developed to compensate for nonorthogonal errors. By using the phase-modulated grating instead of a conventional index, it is possible to reduce nonorthogonal errors of the moiré linear encoder. © 2000 American Institute of Physics.
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  • 116
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    [S.l.] : American Institute of Physics (AIP)
    Review of Scientific Instruments 71 (2000), S. 2309-2320 
    ISSN: 1089-7623
    Source: AIP Digital Archive
    Topics: Physics , Electrical Engineering, Measurement and Control Technology
    Notes: In the present work, we propose a novel technical approach in time domain impedance spectroscopy enabling both enhanced time and current resolution by an improved data analysis and hardware setup. We introduce nonstationary time-to-frequency conversion methods such as short-time Fourier transform and wavelet transform resulting in an improved time resolution. The combination of a time domain impedance spectrometer with a patch-clamp amplifier enables the resolution of gigaohm impedance at low perturbation signal amplitudes. A fast impedance spectroscopy (FIS) setup is presented which is optimized for biophysical application of single ion channel measurements in supported biomembranes. The applicability and performance of the technique is first evaluated by simulations. It is then verified by measurements on model circuits which exhibit the characteristic key properties of single ion channel measurements. Here, FIS improves the time resolution by about three orders of magnitude down to milliseconds. The general aspects derived in this work are also valid in other fields, where the spectral information of a perturbation applied on a system and its response is analyzed, e.g., mechanical impedance spectroscopy and microrheology. © 2000 American Institute of Physics.
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  • 117
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    Review of Scientific Instruments 71 (2000), S. 2321-2328 
    ISSN: 1089-7623
    Source: AIP Digital Archive
    Topics: Physics , Electrical Engineering, Measurement and Control Technology
    Notes: In this work the possibility of using corona discharge as an ionization source in ion mobility spectrometry has been investigated. The results for both positive and negative polarity in air are consistent with the Townsend formula which states that I/V is a linear function of V. The distribution profile of the corona ions has also been investigated and compared with that of the 63Ni ionization source. Generally, the total ion current obtained from the corona ionization source was greater than that of the 63Ni source by about an order of magnitude, which results in a better sensitivity and a higher signal-to-noise ratio. The positive and negative spectra of air were recorded and the positive spectra of acetone and dimethylmethyl-phosphonate were compared with that of 63Ni. In the negative mode, a number of new peaks, apart from those of reactant ions, were observed which are mainly due to nitrogen oxides, formed by corona discharge. This problem was minimized by increasing the interdistance of the electrodes. © 2000 American Institute of Physics.
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  • 118
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    [S.l.] : American Institute of Physics (AIP)
    Review of Scientific Instruments 71 (2000), S. 2353-2359 
    ISSN: 1089-7623
    Source: AIP Digital Archive
    Topics: Physics , Electrical Engineering, Measurement and Control Technology
    Notes: A novel frequency modulation scheme has been developed for the multichannel reflectometer used to measure density profiles and density fluctuations on the Joint European Torus (JET) tokamak. This reflectometer normally uses slow frequency sweeping (6 ms), combined with fixed-frequency operation, to measure the group delay, as well as plasma fluctuations, at ten different microwave frequencies. The novel scheme uses continuous frequency modulation on a time scale much shorter (1/65 μs) than that of plasma fluctuations, the main aim being to make the group delay measurement more robust against plasma fluctuations. This article discusses the theoretical background of the scheme, gives a detailed description of the system, and presents results from plasma measurements. Although the implementation used suffered from an excessive power-dependent group delay distortion (resulting in a positional error of 10 cm), the main objectives have been achieved. © 2000 American Institute of Physics.
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  • 119
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    Review of Scientific Instruments 71 (2000), S. 2334-2352 
    ISSN: 1089-7623
    Source: AIP Digital Archive
    Topics: Physics , Electrical Engineering, Measurement and Control Technology
    Notes: Doppler-free two-photon excitation of hydrogen Lyman-α fluorescence is investigated as a possible laser-induced fluorescence (LIF) technique for the diagnosis of magnetically confined fusion (MCF) plasmas. A formal analysis is presented of the underlying atomic and plasma physics as well as of various practical aspects, such as parameter optimization and experimental precision. The latter is analyzed with regard to the photon noise and to the sensitivity of the fluorescence signals to the plasma and laser parameters. The diagnostic potential of the LIF technique described relies on its high spectral resolution. Thus, the absorption lines of the hydrogen isotopes H, D, and T are clearly separated from each other and can serve for isotope-selective density measurements. In addition, using a tunable laser system with small bandwidth, various plasma parameters can be inferred from the spectral line shapes, such as the neutrals' temperatures or the effective charge number Zeff. The polarization of the fluorescence can, under favorable circumstances, be exploited for magnetic field measurements. The photon statistics impose neutral densities above 1014 m−3 and thus make the diagnostic suitable primarily for the plasma edge. However, previous work has shown that it is applicable even in the plasma bulk of large machines if a neutral beam is used that generates sufficient neutral densities by charge exchange with the plasma ions. Variations or insufficient knowledge of the neutrals' temperatures are found to seriously affect the precision of absolute isotope density measurements. They are rather uncritical, however, for the determination of the H/D/T density ratios, which are of prime importance for the burn control of large MCF devices. A notable sensitivity is also found to variations of the laser frequency detuning, which should be known and stable to better than 100 MHz. The perspectives demonstrated in the present study and the success of a first experiment on the plasma generator PSI 1 at IPP Berlin are considered to be sufficient motivation for testing the diagnostic on a tokamak or other MCF device. © 2000 American Institute of Physics.
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  • 120
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    Review of Scientific Instruments 71 (2000), S. 2367-2370 
    ISSN: 1089-7623
    Source: AIP Digital Archive
    Topics: Physics , Electrical Engineering, Measurement and Control Technology
    Notes: α particles emitted from an 241Am radioactive source at energies of 5.4 MeV generate bursts of about ten electrons when passing through an aluminized Mylar foil. Besides the typical surface barrier electrons, the energy spectra of the secondary electrons clearly reveal two additional peaks. One at 66 eV is ascribed to aluminum LVV Auger electrons and another at 10.5 eV is attributed to the decay of aluminum volume plasmons. The well-resolved angular and energy distributions of these secondary electrons are used to calibrate the relative detection efficiencies of a large set of individual detectors of a complex multicoincidence system. © 2000 American Institute of Physics.
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  • 121
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    Review of Scientific Instruments 71 (2000), S. 2371-2376 
    ISSN: 1089-7623
    Source: AIP Digital Archive
    Topics: Physics , Electrical Engineering, Measurement and Control Technology
    Notes: A new type of microstructure device for a gas radiation detector is proposed. This microstructure, the microhole and strip plate structure, merges the structures of a gas electron multiplier and a microstrip plate in one single plate. This design allows two-multiplication stages and a separation of the sensitive and the detection regions, with full optical positive feedback suppression. Simulations for gas gain and electron transparency of the microstructure are presented. Different applications are discussed. © 2000 American Institute of Physics.
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  • 122
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    Review of Scientific Instruments 71 (2000), S. 2377-2379 
    ISSN: 1089-7623
    Source: AIP Digital Archive
    Topics: Physics , Electrical Engineering, Measurement and Control Technology
    Notes: The influence of secondary electrons released by gamma radiation from the cathode of a nitrogen-filled tube, on probability of electrical breakdown and memory curve, has been investigated. The results show that the nitrogen-filled tube is sensitive to gamma radiation only at longer afterglow periods in the case of overvoltage values grater than 50%. For shorter afterglow periods, the lower values of overvoltages can be used to separate the contribution of gamma rays. © 2000 American Institute of Physics.
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  • 123
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    Review of Scientific Instruments 71 (2000), S. 2386-2390 
    ISSN: 1089-7623
    Source: AIP Digital Archive
    Topics: Physics , Electrical Engineering, Measurement and Control Technology
    Notes: We report on the development of a circularly polarized x-ray microprobe in the intermediate energy range from 5 to 10 keV. In this experiment linearly polarized synchrotron radiation was circularly polarized by means of a Bragg-diffracting diamond phase retarder and subsequently focused down to a spot size of about 4×2 μm2 by a Fresnel zone plate. The properties of the microprobe were characterized, and the technique was applied to the two-dimensional mapping of magnetic domains in HoFe2. © 2000 American Institute of Physics.
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  • 124
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    Review of Scientific Instruments 71 (2000), S. 2380-2385 
    ISSN: 1089-7623
    Source: AIP Digital Archive
    Topics: Physics , Electrical Engineering, Measurement and Control Technology
    Notes: The prospects of a miniature photoconducting capacitor array as a source for THz radiation are discussed. The device consists of an alternately biased capacitor array built on a semiconductor substrate and illuminated by a short laser pulse. The laser pulse creates a propagating plasma front inside the crystal volume by side illumination, and triggers the discharging of the capacitor by shorting out the photoconducting material between each capacitor plate. The sequential discharge of the capacitor array inside the expending plasma region can be considered as an interaction between a static wave and a superluminous ionizing front. In the present article we have demonstrated production of two cycle pulses with a center frequency of up to 1.5 THz. The device combines elements from the well-known "frozen-wave" generator and from the photoconducting switches array. The underlying physics of this radiation mechanism is very similar to the dc-to-ac conversion mechanism inside a gas-filled capacitor array which generates coherent microwave radiation. © 2000 American Institute of Physics.
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  • 125
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    Review of Scientific Instruments 71 (2000), S. 2414-2417 
    ISSN: 1089-7623
    Source: AIP Digital Archive
    Topics: Physics , Electrical Engineering, Measurement and Control Technology
    Notes: We implemented tip–sample distance control in a scanning evanescent microwave probe for nonlinear dielectric microscopy. With the analytic expression of the tip–sample capacitance as a function of tip–sample distance, we can quantitatively regulate the tip–sample separation and independently measure the dielectric nonlinearity by application of an ac bias voltage. Simultaneous imaging of topography and ferroelectric domains has been demonstrated on periodically poled LiNbO3 single crystals. © 2000 American Institute of Physics.
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  • 126
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    Review of Scientific Instruments 71 (2000), S. 2403-2408 
    ISSN: 1089-7623
    Source: AIP Digital Archive
    Topics: Physics , Electrical Engineering, Measurement and Control Technology
    Notes: For a quantitative evaluation of nanoscale elasticity, atomic force microscopy, and related methods measure the contact stiffness (or force gradient) between the tip and sample surface. In these methods the key parameter is the contact radius, since the contact stiffness is changed not only by the elasticity of the sample but also by the contact radius. However, the contact radius is very uncertain and it makes the precision of measurements questionable. In this work, we propose a novel in situ method to estimate the tip shape and the contact radius at the nanoscale contact of the tip and sample. Because the measured resonance frequency sometimes does not depend so sensitively on the contact force as expected from the parabolic tip model, we introduced a more general model of an axial symmetric body and derived an equation for the contact stiffness. Then, the parameters in the model are unambiguously determined from a contact force dependence of the cantilever resonance frequency. We verified that this method is able to provide an accurate prediction of the cantilever thickness, the tip shape, and the effective elasticity of soft and rigid samples. © 2000 American Institute of Physics.
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    Review of Scientific Instruments 71 (2000), S. 2391-2402 
    ISSN: 1089-7623
    Source: AIP Digital Archive
    Topics: Physics , Electrical Engineering, Measurement and Control Technology
    Notes: We describe an apparatus designed to quantitatively measure friction dynamics at the mesoscopic scale. This lateral force apparatus, LFA, uses double parallel leaf springs in leaf-spring units as force transducers and two focus error detection optical heads, optical heads, to measure deflections. The design of the leaf-spring units is new. Normal spring constants are in the range of 20–4000 N/m, and lateral spring constants are 7–1000 N/m. The optical heads combine a 10 nm sensitivity with a useful range of about 100 μm. The proven range of normal forces is 400 nN–150 mN. The leaf-spring units transduce friction and normal forces independently. Absolute values of normal and friction forces are calibrated. Typical errors are less than 10%. The calibration is partly in situ, for the sensitivity of the optical heads, and partly ex situ for the normal and lateral spring constants of the leaf-spring units. There is minimal coupling between the deflection measurements in the lateral and normal directions. This coupling is also calibrated in situ. It is typically 1% and can be as low as 0.25%. This means that the displacements of the tip can be measured accurately in the sliding direction and normal to the surface. Together, these characteristics make the LFA, well suited for quantitative study of friction dynamics at mesoscopic scales. Furthermore the design of the leaf-spring unit allows exchange of tips which may be fabricated (e.g., etched) from wire material (d(approximate)0.4 mm) and can have customized shapes, e.g., polished flat squares. The ability of the LFA to study friction dynamics is briefly illustrated by results of stick-slip measurements on soft polymer surfaces. © 2000 American Institute of Physics.
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  • 128
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    Notes: Motional Stark effect measurements of internal field structure in low-field magnetic confinement configurations are considered for both magnitude and direction of the local magnetic field. The amplitude and phase delay of an oscillating spectral linewidth driven by a rotating polarizer provides a means of determining the magnitude and direction of the total field simultaneously while avoiding difficulties of neutral beam energy drift. Photon-noise limit estimates for a diagnostic beam on the low-field PEGASUS toroidal experiment indicate sensitivities of roughly 20 G and 0.2° for the magnitude and direction angle. These values are sufficient to provide significant constraints on magnetic equilibrium reconstructions. © 2001 American Institute of Physics.
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    Review of Scientific Instruments 72 (2001), S. 1012-1014 
    ISSN: 1089-7623
    Source: AIP Digital Archive
    Topics: Physics , Electrical Engineering, Measurement and Control Technology
    Notes: A motional Stark effect (MSE) instrument to measure q(r) using the Torus Experiment for Technology (TEXT) neutral beam on the Alcator C-Mod tokamak has been designed and installed. The neutral beam is on the midplane, aimed radially, and designed to operate in hydrogen at 50 keV. The MSE optics view the outer half of the plasma −0.3〈(R−R0)/a〈1.05. This geometry results in a spatial resolution of 1 (edge)–3 (center) cm from a beam apertured horizontally to 2 cm. Estimates of the signal levels indicate for Hα that photoelectron statistical errors in the measurement of Bθ/Bφ can be less than 0.2% for ne0〈2.0×1014 cm−3 similar to other MSE instruments. The collection optics reside within the vacuum chamber reflecting and imaging the neutral beam through a vacuum window in the neutral beam port. The optics are designed so that beam emission spectroscopy can be carried out simultaneously with MSE measurements. Optical signals are transmitted to remote detectors by fiber optics. Low Verdet glass and dielectric mirrors are used to minimize polarization changes caused by the ambient fields. Polarization is measured by conventional techniques using photoelastic modulators, optical filters, and photomultipliers. © 2001 American Institute of Physics.
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  • 130
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    Notes: Charge exchange spectroscopy is one of the key ion diagnostics on the DIII-D tokamak. It allows measurement of impurity densities, toroidal and poloidal rotation speeds, ion temperatures, and the radial electric field. For the 2000 experimental campaign, we have replaced the intensified photodiode array detectors on the edge portion of the system with advanced charge-coupled device (CCD) detectors mounted on faster (f/4.7) Czerny–Turner spectrometers equipped with toroidal mirrors. The combination has improved the photoelectron signal level by about a factor of 20 and the signal to noise by a factor of 2–8, depending on the absolute signal level and readout mode. A major portion of the signal level improvement comes from the improved quantum efficiency of the back-illuminated, thinned CCD detector (70% to 85% quantum efficiency for the CCD versus 10% for the image intensifier) with the remainder coming from the faster spectrometer. The CCD camera also allows shorter minimum integration times: 0.33 ms while archiving to computer memory and 0.15 ms using temporary storage on the CCD chip. © 2001 American Institute of Physics.
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    Review of Scientific Instruments 72 (2001), S. 103-107 
    ISSN: 1089-7623
    Source: AIP Digital Archive
    Topics: Physics , Electrical Engineering, Measurement and Control Technology
    Notes: The Alcator C-Mod divertor bypass has for the first time allowed in situ variations to the mechanical baffle design in a tokamak. The design utilizes small coils which interact with the ambient magnetic field inside the vessel to provide the torque required to control small flaps of a Venetian blind geometry. Plasma physics experiments with the bypass have revealed the importance of the divertor baffling to maintain high divertor gas pressures. These experiments have also indicated that the divertor baffling has only a limited effect on the main chamber pressure in C-Mod. © 2001 American Institute of Physics.
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    Review of Scientific Instruments 71 (2000), S. 2598-2602 
    ISSN: 1089-7623
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    Topics: Physics , Electrical Engineering, Measurement and Control Technology
    Notes: This article deals with the study and fabrication of a system for the automation of a multipurpose spectrograph used in Astronomy. This system allows the 19 movements of the instrument to run by using high-level software, a "master" board, and 19 "slave" boards. The Astrophysique Lineal et BIdimensional par RÉseaux Optiques (ALBIREO) spectrograph has three working modes and is installed in the Observatorio de Sierra Nevada, Granada, Spain. We describe a low-cost system realized for the automatization of a multifunction spectrograph. It allows the control of a large number of motors: 19 for Albireo; the theoretical limit is 32 768! Another advantage of this architecture based on "slave" boards is to supply each motor with exactly the current it needs to reach the required torque (reliability and repetitivity of motions are obtained when the motor torque is at least twice the resistant torque). Thus, we can avoid unnecessary overheating which would be detrimental to the material as well as to the local image quality (seeing). The reliability of the system is obtained by software filtering the commands and also by using optocoupled electronics to avoid interference. For a complex instrument, the high-level software must be user friendly. The efficiency of the present software in this respect has been appreciated since first being used on the telescope. This system may be of interest to laboratories and observatories with similar needs for automation of motions. The adoption of this system will be supported by the IAA Laboratory, Granada, Spain. © 2000 American Institute of Physics.
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    Review of Scientific Instruments 71 (2000), S. 2603-2607 
    ISSN: 1089-7623
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    Topics: Physics , Electrical Engineering, Measurement and Control Technology
    Notes: A design is presented for a compact capacitive position sensor suitable for operation at cryogenic temperatures and high magnetic fields. The four quadrants of a base electrode are excited with phases differing by 90°; from its in- and out-of-phase components, the current injected into the movable electrode yields simultaneous information about the x and y sensor positions. This current is also linear in the position of the sensor. The effects of possible sensor imperfections are analyzed in detail. © 2000 American Institute of Physics.
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    Review of Scientific Instruments 71 (2000), S. 2608-2609 
    ISSN: 1089-7623
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    Topics: Physics , Electrical Engineering, Measurement and Control Technology
    Notes: A compact retarding-potential Mott polarimeter combined with microsphere plates (MSP) as electron detectors was built to perform spin-resolved time-of-flight electron spectroscopy. The comparison of the performance of MSP and channeltron detectors shows that the MSP detector has a better time resolution but a lower efficiency. The overall time resolution of the system was determined to be 350 ps using synchrotron radiation pulses. © 2000 American Institute of Physics.
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    Review of Scientific Instruments 71 (2000), S. 1929-1960 
    ISSN: 1089-7623
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    Topics: Physics , Electrical Engineering, Measurement and Control Technology
    Notes: We review the field of femtosecond pulse shaping, in which Fourier synthesis methods are used to generate nearly arbitrarily shaped ultrafast optical wave forms according to user specification. An emphasis is placed on programmable pulse shaping methods based on the use of spatial light modulators. After outlining the fundamental principles of pulse shaping, we then present a detailed discussion of pulse shaping using several different types of spatial light modulators. Finally, new research directions in pulse shaping, and applications of pulse shaping to optical communications, biomedical optical imaging, high power laser amplifiers, quantum control, and laser-electron beam interactions are reviewed. © 2000 American Institute of Physics.
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    Review of Scientific Instruments 71 (2000), S. 2610-2611 
    ISSN: 1089-7623
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    Topics: Physics , Electrical Engineering, Measurement and Control Technology
    Notes: In this note we present a PC-based remote control and data processing setup and the associated software, developed in LabVIEW, working in conjunction with a laser beam analyzer. The setup expands the imaging processing techniques for the laser beam profile, especially in relation to the three-dimensional data representation and manipulation, by using the strong graphical processing and presentation libraries of the HIQ and IMAQ Vision software packages. One novelty of the proposed program consists in its multi-image processing ability with regard to images acquired under different conditions, and which have to be processed aligned to their centroids and their major axes. © 2000 American Institute of Physics.
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    Review of Scientific Instruments 71 (2000), S. 2582-2584 
    ISSN: 1089-7623
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    Topics: Physics , Electrical Engineering, Measurement and Control Technology
    Notes: A selection method to improve temperature compensation is proposed, which is effective in forming current regulator device with low temperature coefficient. The experimental results show that the temperature coefficients are of the order of 10−5/°C. The method is simple and the device stable and reliable. © 2000 American Institute of Physics.
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    Review of Scientific Instruments 71 (2000), S. 1975-1980 
    ISSN: 1089-7623
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    Topics: Physics , Electrical Engineering, Measurement and Control Technology
    Notes: By optimizing the size of a photoacoustic cell for decreasing acoustic loss and noise, and using a proper multipass arrangement for increasing light power in the cell and optical coupling to the acoustic wave, a high-resolution external laser photoacoustic spectrometer with a detection sensitivity of 6.35×10−9 cm−1 (1:1 signal to noise level) has been developed. Using this apparatus, the high quality Doppler-limited overtone spectra of AsH3 (600) and H2Se (60) have been observed at room temperature in the wave number regions 11 500–11 650 and 12 600–12 925 cm−1, respectively. Results are presented which highlight the applicability of this apparatus to the spectroscopy of weak optical transitions. © 2000 American Institute of Physics.
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    Review of Scientific Instruments 71 (2000), S. 1971-1974 
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    Topics: Physics , Electrical Engineering, Measurement and Control Technology
    Notes: This article describes measurements of the velocity and temperature in a turbulent flow by means of a photothermal effect. We developed a new differential interferometer for detecting small phase variation caused by the photothermal effect without influence of turbulent phase fluctuation. The detected fringe point of the interferometer is scanned repeatedly by moving a photomultiplier. An electric system is constructed for compulsorily operating the interferometer at the maximum inclination point of the fringe intensity curve. Using a turbulent jet of nitrogen gas mixed with ethylene gas, we confirmed that this measurement system is useful to measure the velocity and temperature in the turbulent flow. © 2000 American Institute of Physics.
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    Review of Scientific Instruments 71 (2000), S. 1961-1970 
    ISSN: 1089-7623
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    Topics: Physics , Electrical Engineering, Measurement and Control Technology
    Notes: A complete noise analysis of a two-beam photopyroelectric (thermal-wave) destructive interferometric sensor instrument is presented and compared to its single-beam, noninterferometric counterpart. The noise analysis is performed using a Green-function formalism applied to experimental observations. The instrumental background noise contribution from the detector and the amplifier is separated from the laser noise and the instrumental noise due to amplification associated with different sensitivity scales. The latter serves as the source of comparison between the two sensor configurations. It is found that the dc laser drift noise and low-frequency fluctuation noise, which are dominant in the single-beam mode, are greatly reduced to the same order of magnitude as the instrumental background noise in the two-beam mode. The system white noise resulting from the incident laser beam and from the sensitivity scale (amplification) of the demodulating lock-in amplifier are also examined in light of the experimental data. It is found that the detectivity D* (the inverse of the noise equivalent power), of the instrument is enhanced by at least 1 order of magnitude in the interferometric mode. © 2000 American Institute of Physics.
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    Review of Scientific Instruments 71 (2000), S. 1991-2000 
    ISSN: 1089-7623
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    Topics: Physics , Electrical Engineering, Measurement and Control Technology
    Notes: Tapered capillaries are frequently used as beam-concentrating optics in microbeam x-ray diffraction experiments. The beams exiting such devices are usually highly divergent and may possess nonuniform intensity distributions. In addition, their alignment poses some special challenges. In this article, the effects of these factors on the precision and accuracy of diffraction data are presented. © 2000 American Institute of Physics.
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    Review of Scientific Instruments 72 (2001), S. 1129-1132 
    ISSN: 1089-7623
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    Topics: Physics , Electrical Engineering, Measurement and Control Technology
    Notes: An electronics system has been installed and tested for the readout of avalanche photodiode (APD) detectors for the National Spherical Torus Experiment (NSTX) Thomson scattering system. Similar to previous designs, it features preamps with a fast and a slow output. The fast output uses pulse shaping to optimize sensitivity for the 8 ns scattered light pulse while rejecting noise in the intrinsic plasma background. A low readout noise of ∼25 photoelectrons is achieved at an APD gain of 75. The design incorporates a number of features to provide flexibility for various modes of calibration. © 2001 American Institute of Physics.
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  • 143
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    Topics: Physics , Electrical Engineering, Measurement and Control Technology
    Notes: We are building a new Thomson scattering diagnostic system to measure electron temperature and density on the Madison Symmetric Torus (MST) reversed-field pinch experiment. This system has been designed to produce accurate single-shot measurements for 10 eV〈Te〈2 keV at electron densities ≥1018 m−3. Scattered light will be simultaneously recorded from 20 radial locations across the 50 cm minor radius of the plasma. Multipulse capability will be provided by two identical Nd:YAG pulsed lasers whose trigger timing can be independently varied. This will allow several combinations of input energy and pulse timing during an MST discharge, ranging from one 4 J pulse for increased accuracy during low density operation to 1 J pulses at 100 Hz for temporal evolution measurements. Scattered light will be collected by a custom deep-focus lens and coupled by optical fiber to 20 identical filter polychromators. These polychromators are being manufactured by General Atomics and use silicon avalanche photodiode detectors. Each polychromator contains three wavelength channels to allow determination of Te, plus one channel at the laser wavelength to allow calibration using Rayleigh scattering for measurement of ne. System control and data acquisition will be done with dedicated personal computers. © 2001 American Institute of Physics.
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    Review of Scientific Instruments 72 (2001), S. 1147-1147 
    ISSN: 1089-7623
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    Topics: Physics , Electrical Engineering, Measurement and Control Technology
    Notes: A collective Thomson scattering diagnostic is being developed for the measurement of confined fast ions in hot, dense plasmas. This includes such measurements as the ion tail in JT-60U and the alphas produced in a burning reactor or the upgraded Joint European Torus device. The diagnostic also has the capability of measuring the isotopic ratio of the core ions such as the D/T ratio (required in optimizing a burning plasma experiment). The advances under development for this diagnostic include improvements in the high power source laser, increased bandwidth and reduced noise in the receiver, and the development of an intermediate frequency electronic filter bank. Such improvements are designed to permit the temporal measurement of the fast ions and improve the accuracy in determining their velocity distribution. Modeling of the expected scattered signals produced by these improvements and the diagnostics capability to measure the velocity distribution and isotopic ratio are presented. © 2001 American Institute of Physics.
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  • 145
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    Topics: Physics , Electrical Engineering, Measurement and Control Technology
    Notes: Collective light scattering measurement is a powerful tool for investigating fluctuations and their relation with anomalous transport since it allows a direct, discriminating analysis of the turbulent scales. This high scale resolution has a counterpart in a poor spatial resolution, but some localization can be recovered allowing us to discriminate edge from core turbulence behavior and to determine turbulence profiles. More information about localization can be obtained using temporal dynamics of the scattered signal when the fluctuation velocity in the poloidal plane is sheared. Making use of the consequently separated Doppler shifts, different technics are used to extract localized information from frequency spectra and from the signal phase derivative. Capabilities of the diagnostic are illustrated by recent results obtained on Tore Supra in different regimes. © 2001 American Institute of Physics.
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    Review of Scientific Instruments 72 (2001), S. 1166-1166 
    ISSN: 1089-7623
    Source: AIP Digital Archive
    Topics: Physics , Electrical Engineering, Measurement and Control Technology
    Notes: The Chandra X-ray telescope has four separate detectors, two charge coupled devices, and two microchannel plates, behind a set of four highly polished, nested mirrors. The on-orbit performance of the imaging system is 〈1 arcsec, a dramatic improvement from the 5–8 arcsec previously available. In addition, two transmission gratings can be placed in the system, which for point sources can reach resolutions of 300–1000+ over the range λ∼1.5–160 Å. The entire system was calibrated prelaunch at NASA/MSFC in Huntsville, Alabama. The results have been dramatic: the first light image of the supernova remnant Cas A showed a never-before-seen point source near the center of the remnant that may be the neutron star left over after the explosion. Even the calibration image of a distant quasar (taken for focusing purposes) showed an x-ray emitting jet extending out from the nucleus for more than 20 kpc, which challenges current theories about jet propagation. The grating observations done by Chandra take x-ray astrophysics out of the photometry era into the spectroscopic age. Astrophysical plasmas reach conditions far out of the reach of any terrestrial laboratory, and astronomers are just beginning to understand the diagnostics of these plasmas; Chandra observations may even someday provide the best measurements of certain atomic rates. However, before that point is reached the astronomical community must gain a much better understanding of the existing and ongoing work in x-ray diagnostics from other fields. The general state of x-ray diagnostics for astronomical plasmas will also be discussed. © 2001 American Institute of Physics.
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    Review of Scientific Instruments 72 (2001), S. 1183-1187 
    ISSN: 1089-7623
    Source: AIP Digital Archive
    Topics: Physics , Electrical Engineering, Measurement and Control Technology
    Notes: A fully calibrated multilayer mirror (MLM) based soft x-ray spectrometer has been developed and installed on the Compact Helical System (CHS). This MLM based spectrometer is a new approach to devising a soft x-ray spectrometer with medium time and energy resolutions. The spectrometer mainly consists of a MLM as the dispersive element and a 20-channel (p-i-n) pin diode array for the detection of the soft x-rays. Both the MLM and the pin diodes have been calibrated at the KEK (High Energy Accelerator Research Organization) Photon Factory for an energy range of 300–1200 eV. The reflectivity of the mirror was found to increase from 3% (photon energy of 335 eV) to 25% (photon energy of 1050 eV). The pin diodes were found to have almost 100% efficiency for creating electron-hole pairs in the calibrated energy range. The spectrometer was installed on the CHS with the aim of fast electron temperature measurement and study of fast magneto-hydrodynamic (MHD) events occurring in plasmas. The experiments show that in the energy range of measurement, the electron "temperature" determined from the slope of the soft x-ray spectrum is much lower than that measured by the Thomson scattering diagnostic. Analysis showed that the soft x-ray spectrum is highly contaminated by impurity emission. Therefore it may be possible to measure electron temperature with this diagnostic if we choose another energy range where we can measure the continuous spectrum. The present time resolution of the system is of the order ∼0.1 ms, which made it possible to study the behavior of the plasma during fast MHD events. Modulations in the soft x-ray intensity were observed during MHD events in CHS plasmas. Analysis of these shows that these may be due to modulations in the temperature or the impurity concentration. © 2001 American Institute of Physics.
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  • 148
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    Topics: Physics , Electrical Engineering, Measurement and Control Technology
    Notes: Laser–plasma instabilities that produce an unacceptably high level of hot electrons are potentially dangerous for both direct-drive and indirect-drive inertial confinement laser fusion. The hot electrons preheat the fuel and prevent compression of the capsule to the requisite conditions for ignition. Fast electron generation and preheat can be inferred from the hard x-ray radiation generated by the interaction of the hot electrons with the target. On the University of Rochester's OMEGA laser system, time-resolved hard x-ray detectors have been operating in an energy range from 10 to 500 keV. In this article we will present initial results for the yield and spectrum of the hard x-ray radiation. The concept used on OMEGA can be easily extended to infer the amount of laser energy coupled to suprathermal electrons and to the target for both direct- and indirect-drive implosions on the upcoming National Ignition Facility, as well as to measure the conversion efficiency in high-x-ray-yield experiments. © 2001 American Institute of Physics.
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    Review of Scientific Instruments 72 (2001), S. 119-127 
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    Topics: Physics , Electrical Engineering, Measurement and Control Technology
    Notes: Recent development of the JT-60U charge exchange recombination spectroscopy (CXRS) diagnostic system is reported. The measurements of the radial profiles of the ion temperatures, the toroidal and poloidal rotation velocities, and the impurity density are based on CXR spectra of fully stripped carbon ions induced by neutral beam injection. Measurements are made simultaneously at 59 spatial points (23 toroidal and 36 poloidal) with a time resolution of 1/60 s throughout the full discharge pulse of 15 s. Considerable effort has been expended to ensure the automatic provision of reliable profile data, where the mechanical components of the system must cope with both a baked tokamak vessel (∼300 °C) and an expected disruption-induced acceleration of up to 60 g, where g denotes the gravitational acceleration, i.e., 9.8 m2/s. © 2001 American Institute of Physics.
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    Review of Scientific Instruments 71 (2000), S. 2050-2052 
    ISSN: 1089-7623
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    Topics: Physics , Electrical Engineering, Measurement and Control Technology
    Notes: The absolute detection efficiency (ADE) of microchannel plates for neutral sodium and potassium atoms is measured in the low keV energy range. It is shown that ADE is primarily a function of the particle energy. This result is compared to measurements made by other authors for ionic particles. © 2000 American Institute of Physics.
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    Review of Scientific Instruments 71 (2000), S. 2053-2057 
    ISSN: 1089-7623
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    Topics: Physics , Electrical Engineering, Measurement and Control Technology
    Notes: A high-resolution thermoluminescence dosimetry (TLD) spectroscopy reader has been developed in order to perform detailed quantitative studies of the kinetics of TLD materials. The key features of this system are high wavelength resolution (1.3 nm), low cost, and compact size. In addition, the spectrometer is fiber optic coupled to the sample material isolating the system from thermal influences and electrical noise generated by the heating system. Temperature rate control can be computer set with a heat rate accuracy of better than 0.12% and a temperature readout accuracy of 1 °C or better. Analysis of all three parameters: temperature, wavelength, and intensity, is easily visualized with integrated 2D/3D analysis software. Preliminary analysis on TLD300 samples irradiated with 60Co from 5 to 60 Gy show temperature peaks and wavelength locations consistent with other published measurements. Details of the hardware system and software are discussed along with sample results. © 2000 American Institute of Physics.
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    Review of Scientific Instruments 71 (2000), S. 2068-2070 
    ISSN: 1089-7623
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    Topics: Physics , Electrical Engineering, Measurement and Control Technology
    Notes: Using a rotating polyhedral mirror and a vacuum ultraviolet (VUV) monochromater, a space-time resolving VUV diagnostic system is developed. Measurement of the O VI (103.2 nm) radiation on the HT-6M tokamak shows that the time resolution of the system is better than 4 ms and the space resolution is better than 2 cm. Compared with traditional instruments, this system has improved measurement efficiency, and error from shot-to-shot discharge variations is avoided. © 2000 American Institute of Physics.
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    Review of Scientific Instruments 71 (2000), S. 1716-1722 
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    Topics: Physics , Electrical Engineering, Measurement and Control Technology
    Notes: In order to achieve the strictest tolerances required in the manufacturing of an x-ray interferometer of the triple Laue type (LLL) to be used in the accurate determination of the silicon lattice parameter, a new shape of the analyzer crystal is considered. The simulation of its behavior proves that, if specified elastic and thermal load upper limits are satisfied, the lattice plane deformations are compatible with a measurement uncertainty of a few parts in 109. © 2000 American Institute of Physics.
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    Review of Scientific Instruments 71 (2000), S. 1723-1732 
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    Topics: Physics , Electrical Engineering, Measurement and Control Technology
    Notes: A tunable x-ray waveguide with an air gap as the guiding medium is presented. Discrete transverse-electric modes excited in the air gap propagate almost undisturbed. Filling the air gap with a fluid allows for studies of ordering phenomena in a confined geometry. Since the guided modes are mainly confined to the guiding layer, background scattering from the plates is very low. Starting from the propagation characteristics of the modes in the empty waveguide, requirements on the x-ray source and on the positioning accuracy of the plates are derived. The construction of the waveguide is described and measurements of the far-field angular distributions of intensity exiting the waveguide are presented which illustrate the waveguide's properties. © 2000 American Institute of Physics.
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  • 155
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    Notes: A set of experiments on neutron and x-ray generation was performed on the S-300 facility for the last few months. The S-300 facility is a pulse generator with electric current achieving 3.5 MA, voltage 400–500 kV, and rise time ∼100 ns. (Chernenko et al., Proc. of the 11th International Conference of Power Particle Beams, Prague, 1966, p. 154). It is designed as van eight-module machine transmitting electromagnetic power to the low-inductive load through the vacuum line with self-magnetic isolation. Diagnostic techniques and methods on S-300 used are described in this article. Ten-channel polychromator is used for the soft x-ray and vacuum ultraviolet bands (50–500 eV) measurements with spectral resolution of 5%–20% and time resolution less than 2.5 ns. Radiated power measurements in the region of 0.1–10 keV are performed by vacuum x-ray diodes and semiconductor detectors equipped with different filters. Curved crystal x-ray spectrography is intended for plasma density, electron, and ion temperature evaluation. Visible and x-ray radiation image converter tubes and a streak camera reproduce plasma dynamics. Laser shadow and schlieren probing are used to investigate rare periphery plasma motion. Time-of-flight and activation technique is designed for total neutron yield determination. © 2001 American Institute of Physics.
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  • 156
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    Review of Scientific Instruments 72 (2001), S. 1224-1227 
    ISSN: 1089-7623
    Source: AIP Digital Archive
    Topics: Physics , Electrical Engineering, Measurement and Control Technology
    Notes: We report the development of techniques to diagnose plasmas produced by x-ray photoionization of thin foils placed near the Z-pinch on the Sandia Z Machine. The development of 100+ TW x-ray sources enables access to novel plasma regimes, such as the photoionization equilibrium. To diagnose these plasmas one must simultaneously characterize both the foil and the driving pinch. The desired photoionized plasma equilibrium is only reached transiently for a 2-ns window, placing stringent requirements on diagnostic synchronization. We have adapted existing Sandia diagnostics and fielded an additional gated three-crystal Johann spectrometer with dual lines of sight to meet these requirements. We present sample data from experiments using 1-cm, 180-eV tungsten pinches to photoionize foils made of 200 Å Fe and 300 Å NaF co-mixed and sandwiched between 1000 Å layers of Lexan (C16H14O3), and discuss the application of this work to benchmarking astrophysical models. © 2001 American Institute of Physics.
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  • 157
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    Review of Scientific Instruments 71 (2000), S. 1752-1755 
    ISSN: 1089-7623
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    Topics: Physics , Electrical Engineering, Measurement and Control Technology
    Notes: We describe a modified version of a magneto-optical Kerr magnetometer which allows measuring the hysteresis loop of a specific portion of the sample surface. The diameter of the sampled area can be optically tuned from several mm down to 15 μm. High quality hysteresis loops can be measured in a few seconds. Strong fluctuations are observed when the spot diameter is reduced to a few hundred microns or less. These fluctuations are related to the well-known Barkhausen noise here investigated for the first time in a systematic way using optical techniques. Preliminary data for epitaxial Fe grown on MgO are presented. © 2000 American Institute of Physics.
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  • 158
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    Review of Scientific Instruments 71 (2000), S. 1745-1751 
    ISSN: 1089-7623
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    Topics: Physics , Electrical Engineering, Measurement and Control Technology
    Notes: Conventional radiative furnaces require sample containment that encourages contamination at elevated temperatures and generally need windows which restrict the entrance and exit solid angles required for diffraction and scattering measurements. We describe a contactless windowless furnace based on aerodynamic levitation and laser heating which has been designed for high temperature neutron scattering experiments. Data from initial experiments are reported for crystalline and amorphous oxides at temperatures up to 1900 °C, using the spallation neutron source ISIS together with our laser-heated aerodynamic levitator. Accurate reproduction of thermal expansion coefficients and radial distribution functions have been obtained, demonstrating the utility of aerodynamic levitation methods for neutron scattering methods. © 2000 American Institute of Physics.
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    Review of Scientific Instruments 71 (2000), S. 1756-1765 
    ISSN: 1089-7623
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    Topics: Physics , Electrical Engineering, Measurement and Control Technology
    Notes: A new measuring set for measurements of the speed of sound in liquids under high pressures (up to 300 MPa), designed and constructed in our laboratory, is described. It operates on the principle of the pulse-echo-overlap method. A single transmitting–receiving piezoelectric ceramic transducer operating at 4 MHz and an acoustic reflector were applied. Details concerning the designing and operation of all the elements of the acoustic path, assuring high accuracy of the speed measurements, are given. © 2000 American Institute of Physics.
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  • 160
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    Review of Scientific Instruments 71 (2000), S. 1766-1771 
    ISSN: 1089-7623
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    Topics: Physics , Electrical Engineering, Measurement and Control Technology
    Notes: The temperature rise produced in iron and copper specimens by high strain deformation in a compression split Hopkinson pressure bar was measured simultaneously using two independent techniques: (i) small thermocouples (0.2 mm junction size) and (ii) an infrared (IR) camera system based on mercury cadmium telluride (spectral response between 8 and 12 μm). The response time of the thermocouple system was limited by the time taken for heat to diffuse into the junction. In order to obtain useful data with the IR camera system, the emissivity of the specimen surface needed to be modified by depositing a layer of soot. Even so, the measured emissivity was low (0.4), suggesting that the soot layer was semitransparent to IR radiation. The thermocouples, however, yielded temperature measurements that were consistent with all the mechanical work performed on the specimens being converted to heat. The main positive result obtained with the IR camera system is that heating of the iron specimens was spatially nonuniform. © 2000 American Institute of Physics.
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  • 161
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    Review of Scientific Instruments 71 (2000), S. 1772-1775 
    ISSN: 1089-7623
    Source: AIP Digital Archive
    Topics: Physics , Electrical Engineering, Measurement and Control Technology
    Notes: For a piezoelectric device with multiple electrodes, it should be possible to quantitatively and conveniently measure the piezoelectric coefficient d31 by use of the double piezoelectric effect, without the need for any unusual apparatus or a calibration sample. One pair of electrodes is used to excite the piezo, and another is used to measure the response. For example, for a piezoelectric tube this should allow measurement of d31 as a function of temperature or of lateral offset voltage. An important correction to the current theory is described. Measurements on two piezo tubes are presented for excitation voltages in the range of 0.5–110 Vpp. An inductive proximity sensor was used to measure the actual piezo motion. It is shown that the current theory disagrees with this and previous experiments by a simple factor of 2 for symmetric excitations. However, for asymmetric excitations the disagreement with theory is more complex, and the current theory does not accurately predict the effects of varying tube geometry. © 2000 American Institute of Physics.
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  • 162
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    Review of Scientific Instruments 71 (2000), S. 1776-1780 
    ISSN: 1089-7623
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    Topics: Physics , Electrical Engineering, Measurement and Control Technology
    Notes: We describe a low-noise cryogenic probing system capable of measuring currents at the femtoAmpere (fA) level with integration time ≤1 s and current noise spectra at the 1 fA/(square root of)Hz level with the sample cooled to cryogenic temperatures. The system consists of a low-noise electrometer and a low-noise cryogenic probe with completely guarded sample chamber. The low-noise electrometer has amplification of 0.1 V/1 pA with f3 dB=70 Hz, 1.1 V/pA with f3 dB=20 Hz, and/or 10.1 V/pA with f3 dB=1.4 Hz, and input current noise power density of 0.4 fA/(square root of)Hz rms and input voltage noise power density of (approximate)0.3 μV/(square root of)Hz rms at 1 Hz frequency. With the cryogenic probe, the entire measurement system has input current noise of 0.8 fA/(square root of)Hz rms at 1 Hz. The completely guarded sample chamber reduces parasitic conductance to 〈10−16 S and parasitic capacitance to ≤15 fF between pairs of pins for current–voltage measurements. With this instrumentation, we are able to characterize the current and current noise of quantum well infrared photodetectors for sensitive zero-background applications. © 2000 American Institute of Physics.
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    Review of Scientific Instruments 71 (2000), S. 1781-1787 
    ISSN: 1089-7623
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    Topics: Physics , Electrical Engineering, Measurement and Control Technology
    Notes: We present a general technique to assess and remove unwanted contributions from closely spaced features in spectra acquired using Auger-photoelectron coincidence spectroscopy. We use the Ag 3d5/2 and 3d3/2 core levels and their associated core valence–valence Auger decays, the Ag M5VV and M4VV Auger lines, to demonstrate this technique. Ag M5VV and M4VV Auger spectra were obtained in coincidence with 3d5/2 and 3d3/2 core photoelectrons, respectively. We have also measured the 3d5/2 and 3d3/2 core level spectra in coincidence with M5VV and M4VV Auger electrons. In the coincidence spectra, the contribution from the spin-orbit partner is considerably reduced but, in general, not eliminated. However, by measuring all four coincidence spectra, enough information is obtained to unambiguously assess and remove the unwanted contributions and thus determine the intrinsic line shape of the M5VV and M4VV Auger lines. As a cross-check of this subtraction technique, we find that the intrinsic M5VV and M4VV line shapes give an excellent account of the conventional, noncoincidence Ag M4,5VV spectrum with the expected 6:4 ratio. The correction technique described here can be applied to a large number of systems where the close separation of core lines produces additional spectral features in the coincidence measurements of their associated Auger spectra. © 2000 American Institute of Physics.
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    Review of Scientific Instruments 71 (2000), S. 1788-1792 
    ISSN: 1089-7623
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    Topics: Physics , Electrical Engineering, Measurement and Control Technology
    Notes: We developed an apparatus of differential thermal analysis (DTA) capable of simultaneous surface specific ultraviolet (UV) photoemission measurements to investigate thin-film phase transitions. The apparatus was installed in a vacuum chamber of 10−6 Torr range for thermal isolation and the measurements of UV photoemission. As a sample substrate, we used a thin (10 μm) copper sheet supported by two wires for optimal thermal resistivity. The performance of the apparatus was examined using a 650-Å-thick pentacontane (n-C50H102) film, which may exhibit a unique monolayer phase transition known as surface freezing. We observed two anomalies of DTA curve around the bulk melting temperature, one of which is apparently due to the bulk melting. Since the temperature dependence of the surface specific UV photoemission measurements showed corresponding changes in photoemission current, we could conclude that the other phase transition peak originates from the surface freezing effect. This demonstrates that our DTA-UV apparatus is sufficiently sensitive to examine such monolayer phase transitions. © 2000 American Institute of Physics.
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    Review of Scientific Instruments 71 (2000), S. 1804-1810 
    ISSN: 1089-7623
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    Topics: Physics , Electrical Engineering, Measurement and Control Technology
    Notes: In this article we describe an electrochemical experimental setup for cyclic voltammetry operating from low (1 V/s) to very high (200 kV/s) scan rates. The system is designed to achieve an acceptable cost and to be user friendly for nonexperts. The instrumentation is based on a commercial arbitrary wave form generator, a digital oscilloscope, a general purpose interface bus interface to a PC, and a laboratory-built potentiostat. There are no complicated manual operations, instead the software creates dialog with an operator to control commands for the instruments. Requirements for the wave form synthesis and the data acquisition are given. Various data-smoothing methods for treating 8-bit fast scan data are evaluated. The performance was tested on the oxidation of ferrocene in acetonitrile. The estimated value of the standard heterogeneous rate constant, k0=0.8±0.1 cm s−1, is in reasonable agreement with the most recent reports from other laboratories. © 2000 American Institute of Physics.
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    Review of Scientific Instruments 71 (2000), S. 1793-1803 
    ISSN: 1089-7623
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    Topics: Physics , Electrical Engineering, Measurement and Control Technology
    Notes: We present an experimental setup for measuring the electrical conductance through metallic quantum point contacts (QPCs) under constant or time-dependent bias voltage conditions. The response time of the setup is as short as 25 ns and typical bias voltages range from 10 mV to 2 V. A function generator is used as bias voltage supply. With this, voltage bursts with a frequency of up to 100 kHz can be applied to the QPCs, whereby current-to-voltage (I–V) curves can be acquired using a homebuilt, 30 MHz bandwidth I–V converter, and a 100 Msamples/s digital storage oscilloscope. Test experiments on resistors show that nonlinear contributions to the I–V curves are always less than 1% of the current for all applied voltages. From the slope of the I–V curves, the conductance can be determined with an accuracy better than 1%. The QPCs are formed between a single-crystal metal sample and the tip of a scanning tunneling microscope under clean ultrahigh vacuum conditions. We demonstrate how the setup can be used to capture the I–V curves of several metastable states in a Au QPC, as it breaks during a period of 200 μs at room temperature. © 2000 American Institute of Physics.
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    Review of Scientific Instruments 71 (2000), S. 1811-1815 
    ISSN: 1089-7623
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    Topics: Physics , Electrical Engineering, Measurement and Control Technology
    Notes: A sensitive and generally applicable technique for high resolution infrared spectroscopy of weakly bound ionic complexes is presented. The method is based on the direct absorption of tunable diode laser radiation in an expansion cooled planar plasma. The plasma is generated by electron impact ionization of gas that is expanded supersonically through a long and narrow slit. This technique allows a fast and effective production modulation. Online monitoring by a quadrupole mass spectrometer yields direct information on the plasma characteristics. Rotational temperatures as low as 15 K and densities of the order of 109–1010 complexes/cm3 are routinely obtained. The technique is discussed on the example of N4+ and demonstrated with results on the proton bound complexes N2–H+–N2, Ar–HN2+, and Ar–HCO+. © 2000 American Institute of Physics.
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  • 168
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    Review of Scientific Instruments 71 (2000), S. 1816-1823 
    ISSN: 1089-7623
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    Topics: Physics , Electrical Engineering, Measurement and Control Technology
    Notes: A pulsed Laval nozzle, low Mach number supersonic expansion kinetics apparatus has been constructed to study neutral–neutral kinetics by a rather general laser photolysis initiation and laser photoionization detection of the product species. This new apparatus permits laboratory studies of low temperature rate coefficients (e.g., 70–170 K) on condensable gases that have insufficient vapor pressures at low temperatures for conventional methods of kinetic measurements. The design considerations, the uniformity of the reaction zone over 10–20 cm, and the skimmer sampling of the pulsed Laval expansion are examined. The direct measurement of a rate coefficient at 90 K is also demonstrated using this new apparatus. © 2000 American Institute of Physics.
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    Review of Scientific Instruments 71 (2000), S. 1824-1831 
    ISSN: 1089-7623
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    Topics: Physics , Electrical Engineering, Measurement and Control Technology
    Notes: A detailed description of a differential isothermal titration microcalorimeter with Peltier compensation is reported here. It can be considered as a heat flux or conduction microcalorimeter with dynamic power compensation. The design, based on the twin principle, is very simple and the manufacture is of low cost and complexity. The system operation is completely automatized and computer controlled, including the data acquisition tasks, the controller of the power compensation feedback loop and the reagent injection system. The purpose of the closed loop control is to improve the dynamic performance of the microcalorimeter, resulting in an enhanced sensitivity and accuracy. The instrument performance is demonstrated by calibration experiments showing that the baseline noise (root-mean-square of the temperature difference between the cells) to be 0.4 μK and the specific sensitivity about 2–8 μJ/ml. The main time constant can be reduced from 120 s (without power compensation) to 22 s or even less (with power compensation). In a subsequent article, a precise characterization of the microcalorimeter will be given. © 2000 American Institute of Physics.
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  • 170
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    Notes: In a previous article a comprehensive description of an isothermal titration microcalorimeter with Peltier compensation was reported. This work deals with the characterization procedure and the operation mode. The transfer function parameters (time constants, calibration constants, and thermal properties of the system components) have been determined using a rigorous physical model for the microcalorimeter. To check the good performance of the instrument, titration experiments of cytidine and adenosine protonation have been carried out. Finally, as an example of the instrument applicability, differential heat measurements of myoglobin adsorption onto polymeric (polystyrene) latex particles are presented. © 2000 American Institute of Physics.
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    Review of Scientific Instruments 71 (2000), S. 1841-1848 
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    Topics: Physics , Electrical Engineering, Measurement and Control Technology
    Notes: The design features and the performances of a prototype photon counting imaging detector, being developed for the international ultraviolet (UV) space mission Spectrum UV, are presented. The photon counter is an intensified charge coupled device (ICCD) in which photon events, generating an electron cascade through a high gain microchannel plate (MCP) stack, are transduced, via a phosphor screen and a fiber optics reducer, into a 3×3 pixel2, quasi-Gaussian charge distributions on a 15×15 μm2,512×512 pixel2 format CCD matrix. The CCD is read out in the frame-transfer mode at a pixel rate of 19.75 MHz, and its output data flow is acquired serially as to generate a 3×3 pixel2 event sash that sweeps dynamically the CCD matrix at the 50.6 ns rate of the readout clock. Each and every event sash is searched for the presence of events whose charge content lie within proper limits and satisfy a given set of morphological rules, i.e., a single peak charge profile. The centroid coordinates of identified events are determined with subpixel accuracy (up to a 210 bin/pixel) and subsequently stored as photon list coordinate pairs. The data acquisition and processing system is based on field programmable gate array technology and is capable of satisfying the requirements of real-time operation. The modular construction of the data acquisition and processing electronics provides a great deal of flexibility for supporting advancements in CCD readout techniques (multiple output and higher clocking speed) and of MCPs (larger formats, smaller pore, and higher dynamic range). The results of the performance verification of the data acquisition and processing system integrated with a laboratory ICCD prototype are presented and discussed. © 2000 American Institute of Physics.
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    Review of Scientific Instruments 71 (2000), S. 1849-1852 
    ISSN: 1089-7623
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    Topics: Physics , Electrical Engineering, Measurement and Control Technology
    Notes: A phase sensitive detector employed in microwave/mm wave radiometric systems measures an output as a pure dc, proportional to the difference between the phase of the input modulated signal and a reference signal. This difference signal takes the form of a square wave, one level corresponding to a constant blackbody temperature and the other to the incoming radiation, cancelling the inherent noise of the receiver, thereby achieving a high degree of stability of the radiometer. A phase sensitive (or a synchronous) detector was designed and fabricated to be used in the microwave receiver. The phase sensitive detector was fabricated for a minimum reference signal of 3 V square wave and a minimum signal input of 75 mV with an integration time of 6 s. © 2000 American Institute of Physics.
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    Review of Scientific Instruments 71 (2000), S. 1853-1861 
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    Topics: Physics , Electrical Engineering, Measurement and Control Technology
    Notes: It is shown that the avalanche multiplication factor of transistors, which plays a key role in the functioning of the Marx bank circuit, can be considerably enhanced when the collector has a Gaussian doping profile, compared to uniform doping. The limiting of the maximum field in the collector, and the base push out are the events involved in the occurrence of the current mode second breakdown of avalanche transitors in the Marx circuit. Calculations show that the limiting of the maximum field, followed by the base push out, is the sequence conducive to the enhancement of the avalanche gain. Preliminary experimental assessment of the doping profiles of the same model of transistors from two different manufacturers supports the proposed idea. © 2000 American Institute of Physics.
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    Review of Scientific Instruments 71 (2000), S. 1862-1868 
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    Topics: Physics , Electrical Engineering, Measurement and Control Technology
    Notes: A new instrumentation system for measuring wide frequency band complex permittivity (1 MHz–2 GHz) during the microwave curing process has been developed using an original system coupled with coaxial discontinuity. The instrumentation operates through the automatic commutation of the wide frequency band cell on a power supply or a probe supply. This system allows the use of different heating frequencies (215 MHz, 434 MHz, or 2.45 GHz) with the same cell. This instrumentation has been used to study microwave curing compared with conventional heating, but it can also be applied to the use of microwaves in chemical processes or to study the biological effects of microwaves. © 2000 American Institute of Physics.
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    Review of Scientific Instruments 71 (2000), S. 1869-1872 
    ISSN: 1089-7623
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    Topics: Physics , Electrical Engineering, Measurement and Control Technology
    Notes: We demonstrate photoacoustic thermal imaging of the voids occurring at the interface of directly bonded silicon wafers. The wafers are not touched by probes, minimizing wafer contamination, and the technique does not require the outer surfaces of the bonded wafers to be polished. The method is effective for infrared-opaque materials, as demonstrated by coating a silicon bonded pair with bismuth and obtaining an improvement in the contrast. © 2000 American Institute of Physics.
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    Review of Scientific Instruments 71 (2000), S. 1876-1882 
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    Topics: Physics , Electrical Engineering, Measurement and Control Technology
    Notes: A new measuring device has been developed for diesel injection nozzle testing, allowing measuring of the steady flow through injection nozzle and the injection rate. It can be best applied for measuring the low and high injection rates of the pintle and single hole nozzle. In steady flow measuring the fuel pressure at the inlet of the injection nozzle is 400 bar. The sensor of the measuring device measures the fuel charge, resulting from fuel rubbing in the fuel injection system, as well as from the temperature gradient in the sensor electrode. The electric charge is led to the charge amplifier, where it is converted into electric current and amplified. The amplifier can be used also to measure the mean injection rate value. © 2000 American Institute of Physics.
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    Review of Scientific Instruments 71 (2000), S. 1379-1384 
    ISSN: 1089-7623
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    Topics: Physics , Electrical Engineering, Measurement and Control Technology
    Notes: A compact cesium deposition system was used for direct deposition of cesium atoms and ions onto the inner surface of the 1/3 scale hydrogen negative ion source for the large helical device-neutral beam injection (LHD-NBI), system. A small, well defined amount of cesium deposition in the range of 3–200 mg was tested. Negative ion extraction and acceleration were carried out both in the pure hydrogen operation mode and in the cesium mode. Single Cs deposition of 3–30 mg to the plasma chamber has produced temporary 2–5 times increases of H− yield, but the yield was decreased within several discharge pulses to the previous steady-state value. Two consecutive 30 mg depositions done within a 3–5 h/60 shot interval, produced a similar temporary increase of H− beam, but reached a large H− yield steady-state value. Deposition of larger 0.1–0.2 g Cs portions with a 20–120 h/150–270 shot interval improved the H− yield for a long (2–5 days) period of operation. Directed depositions of Cs to the various walls of the plasma chamber showed approximately the same H− increase. Deposition of 0.13 g Cs to a surface polluted by a water leak, produced a temporary increase, and a H− steady-state level similar to that from a single 30 mg cesium deposition. Deposition of 0.1 g with a cesium plasma produced one half the H− yield obtained by deposition of the same amount of cesium atoms. A higher steady-state H− current value and a smaller rate of H− yield decrease was recorded during the eight filament discharge operation, as compared to the 12 filament operation at the same discharge power. © 2000 American Institute of Physics.
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    Review of Scientific Instruments 71 (2000), S. 1409-1412 
    ISSN: 1089-7623
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    Topics: Physics , Electrical Engineering, Measurement and Control Technology
    Notes: Operation of the laser ion source of He-like light ions designed for the first stage of the ITEP Terra Watt Accumulator (TWAC) project is discussed. A 5 J/0.5 Hz rep-rate CO2 laser was used for generation of highly charged light ions. The absolute number of ions with different charge states for carbon and aluminum ion beams has been measured. The obtained number of C+4 ions (∼1011ions/pulse) is sufficient to start the experimental proof of the accelerator scheme of the TWAC project. The investigation of shot to shot stability indicates significant increasing (∼2–3 times) of highly charged ion yield for the first shot onto the fresh target surface with respect to the next shots onto the same spot of aluminum target. This effect was not observed for the carbon target. Experimental results for highly charged light and medium mass (F, Mg, Al, Ca, Ti) ions produced by of 75 J single pulse CO2 laser consisting of a master oscillator and power amplifier are also presented. © 2000 American Institute of Physics.
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    Review of Scientific Instruments 71 (2000), S. 1417-1420 
    ISSN: 1089-7623
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    Topics: Physics , Electrical Engineering, Measurement and Control Technology
    Notes: A Thomson parabola ion spectrograph (TP) is a very useful tool for the investigation of pulsed laser ablation. Measurements performed with the TP give useful information about physical processes, ion species and their energy distributions, as well as charge states. For ions with the lower charge states, q〈20, complete information about energy distributions of all ionization states of ions can be obtained from a single laser shot. For ions with higher ionization states, parabolas generated in the TP interfere and it is impossible to get energy distributions for all the ion species. In this situation, the registered ions are composed of a few groups with different charge states and different energies. The TP enables the charge states and energetic ranges of different ion groups to be estimated. This presentation describes a method of processing experimental results, obtained from a TP, using a microchannelplate (MCP) image converter. Ion energy distributions for C1+–C6+ and Ta1+–Ta12+ are shown, and the effects of correcting the obtained ion energy distributions for the detection efficiency of the MCP are illustrated. © 2000 American Institute of Physics.
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    Review of Scientific Instruments 71 (2000), S. 1441-1446 
    ISSN: 1089-7623
    Source: AIP Digital Archive
    Topics: Physics , Electrical Engineering, Measurement and Control Technology
    Notes: A ribbon-like magnetoelastic thick-film sensor can be considered the magnetic analog of an acoustic bell. In response to an externally applied magnetic field impulse the magnetoelastic sensor magnetically rings, in a bell-like fashion, emitting magnetic flux with a characteristic resonant frequency that is determined from a fast Fourier transform of the transient response captured using a pickup coil. The resonant frequency of the sensor changes in response to mass loading and, when immersed in liquid, interfacial shear forces associated with viscosity. We report on the use of magnetoelastic sensors to measure the viscosity and density of highly viscous liquids. When characterizing highly viscous liquids, to avoid over damping of the sensor due to the liquid mass load the sensor is suspended from a boat-like structure with one end of the sensor immersed a fixed distance into the liquid. Using this method liquid viscosities ranging from 1.3 to 12 P are measured. © 2000 American Institute of Physics.
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    Review of Scientific Instruments 71 (2000), S. 1479-1487 
    ISSN: 1089-7623
    Source: AIP Digital Archive
    Topics: Physics , Electrical Engineering, Measurement and Control Technology
    Notes: An ultrahigh vacuum chemical beam epitaxy growth system has been built using multiple supersonic jets as precursors. Supersonic jets provide very high flux to the growth front while maintaining low growth pressures (10−5 Torr). Activation barriers to chemisorption are overcome by using hyperthermal (1–10 eV) precursors for heteroepitaxial growth. Improvement in growth rates and higher degrees of structural orientation are obtained at lower temperatures. Wide band gap semiconductors (SiC, GaN, and AlN) are deposited on silicon substrates using neutral chemical precursors. Epitaxial growth of SiC on silicon has been obtained at the lowest temperatures reported to date using a supersonic jet of methylsilane. © 2000 American Institute of Physics.
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  • 182
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    Review of Scientific Instruments 71 (2000), S. 1475-1478 
    ISSN: 1089-7623
    Source: AIP Digital Archive
    Topics: Physics , Electrical Engineering, Measurement and Control Technology
    Notes: We present a scanning tunneling microscope (STM) designed to operate between 275 mK and room temperature, in magnetic fields up to 14 T and in ultrahigh vacuum (UHV). The system features a compact STM connected to an UHV compatible 3He refrigerator fitting into a bottom loading cryostat with a superconducting magnet. In this configuration, the cryostat is sitting on top of the UHV chamber, resulting in a very short distance between the STM access and the experimental position. It further enables proper thermal anchoring of the entire STM setup, allowing millikelvin temperatures to be reached in true UHV conditions. We achieve a hold time of about 40 h at 275 mK and a turnaround time of 10 h between room and base temperature. We demonstrate atomic resolution and present tunneling spectra obtained at 275 mK on the high-Tc superconductors Bi2Sr2CaCu2O8+δ and YBa2Cu3O7−δ. © 2000 American Institute of Physics.
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    Review of Scientific Instruments 71 (2000), S. 1495-1499 
    ISSN: 1089-7623
    Source: AIP Digital Archive
    Topics: Physics , Electrical Engineering, Measurement and Control Technology
    Notes: An ultrahigh vacuum preparation and analysis chamber with an externally attached high pressure reaction cell is described. The novel all-glass design of the reaction cell allows the study of reaction kinetics in a clean environment but under conditions close to those of conventional catalysis. Reactions on supported metals can be studied on pairs of "real" and "inverse" type model catalysts in the same experimental system under identical sample geometry. No supports or wires are connected to the catalyst while in the high pressure cell, and background activity can therefore be excluded. The experimental setup described required the construction of a special transfer mechanism for in situ manipulation of the samples. As a test reaction, CO hydrogenation has been studied on a transition metal oxide modified rhodium metal surface, and some initial results are presented. © 2000 American Institute of Physics.
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    Review of Scientific Instruments 71 (2000), S. 1505-1508 
    ISSN: 1089-7623
    Source: AIP Digital Archive
    Topics: Physics , Electrical Engineering, Measurement and Control Technology
    Notes: Strontium sulfide (SrS) was used as the evaporant material to prepare the phosphor layer for a blue electroluminescent (EL) element. SrS evaporation was performed by using a resistively heated carbon heater. No heat treatment of the phosphor layer after deposition was made. A crucible temperature of more than 1400 °C was obtained in this evaporation system which makes this system equally applicable for the evaporation of other materials with high melting temperature. Cerium (Ce) luminescent centers were doped in SrS films and a Ce concentration of 0.3 mol % was determined to be optimum for EL. For SrS:Ce films deposited onto a quartz substrate, x-ray diffraction and photoluminescent measurements indicated an optimum substrate temperature (Tsub) of 500 °C. In the EL fabrication process, Tsub was restricted to [less, double equals]410 °C by the softening temperature of the alumino-silicate substrate used in the EL device. © 2000 American Institute of Physics.
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    Review of Scientific Instruments 71 (2000), S. 1529-1533 
    ISSN: 1089-7623
    Source: AIP Digital Archive
    Topics: Physics , Electrical Engineering, Measurement and Control Technology
    Notes: Measurements of the magnetic field noise and the spatial correlation of the noise were made in a typical laboratory environment using two three-axis fluxgate magnetometers. The magnitude of the magnetic field noise was found to be approximately 100 pT/Hz at 10 Hz with a correlation of 90% at a separation of 1 m between the two sensors. The correlation was significantly reduced from noise induced eddy currents near large metallic surfaces. © 2000 American Institute of Physics.
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  • 186
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    Review of Scientific Instruments 71 (2000), S. 1548-1551 
    ISSN: 1089-7623
    Source: AIP Digital Archive
    Topics: Physics , Electrical Engineering, Measurement and Control Technology
    Notes: Interferometer measurements are extremely informative in shock wave studies allowing direct evaluations of the gas density. The primary goal of the work presented is to build a laser interferometer that meets the requirements of the highest possible simplicity, economy, convenience, and ease of construction. In our experiments, we used a low average power (10 mW) He–Ne laser without complication, expense, and environmental section. The He–Ne laser interferometer with the Michelson arrangement was used to measure the line-averaged gas densities of shock waves. Temporal and spatial measurements of the density were performed for shock wave developments from high-current pulse discharges. The shock wave propagates in the radial direction of the discharge channel with supersonic speed. The shock velocity, however, decreased from 2–0.5 km/s with the distance of the shock propagation. The width of the high density region, that is in the vicinity of the shock front was compressed from 3.5 to 1.8 mm according to the time variation of the discharge current. © 2000 American Institute of Physics.
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    Review of Scientific Instruments 72 (2001), S. 247-251 
    ISSN: 1089-7623
    Source: AIP Digital Archive
    Topics: Physics , Electrical Engineering, Measurement and Control Technology
    Notes: A modular, low-cost, digital signal processor (DSP)-based lock-in card is described for measuring optical attenuation. By transferring the lock-in operation from the analog domain to the digital domain, the nonlinearities gain, and offset errors and drifts are virtually eliminated. The dual phase lock-in operation has been implemented on the low-cost DSP56002 evaluation module (DSP56002EVM) of Motorola that is widely used in audio signal processing. This evaluation board contains a 24 bit DSP56002 DSP and a stereo CD-quality audio codec that makes the board ideal for implementing signal processing algorithms. Due to the maximum sampling rate of the codec embedded on the DSP56002EVM, the frequencies of the processed signals must be below 20 kHz. This specification is enough for the most common applications in the field of optics, where low or very low frequency (〈1 kHz) references are frequent. The software algorithm implementing the lock-in amplifier can be particularized by the user on the basis of the needed performances. The effects of finite word length in the digital filter implementation are analyzed. This analysis reveals that a 24 bit word length is not enough to ensure the filter stability and the required frequency response. To overcome this problem, the double precision multiply mode must be used. When the DSP56002 enters this mode, double precision 48 bit by 48 bit multiplication can be performed. The lock-in performance has been tested. The measured amplitude variations of the reference sine signal are about 0.003%, which do not affect the signal measurement. The lock-in behaves like a band-pass filter centered on the reference frequency whose bandwidth is related to the low-pass filter cutoff frequency. The measured frequency response shows that the lock-in performs as theoretically predicted. The DSP56002EVM can be used as a lock-in for electrical signals in stand-alone operation. Besides, we have designed a card that interconnects to the DSP56002EVM and allows the ensemble to act as an optical attenuation detector that measures optical losses over 70 dB. This range is similar to that achievable by commercially available optical loss testers and makes it suitable for optical return loss measurements of all kinds of commercially available optical connectors. © 2001 American Institute of Physics.
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  • 188
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    Source: AIP Digital Archive
    Topics: Physics , Electrical Engineering, Measurement and Control Technology
    Notes: Electron cyclotron emission (ECE) has been employed as a standard electron temperature profile diagnostic on many tokamaks and stellarators, but most magnetically confined plasma devices cannot take advantage of standard ECE diagnostics to measure temperature. They are either "overdense," operating at high density relative to the magnetic field (e.g., ωpe(very-much-greater-than)Ωce in a spherical torus) or they have insufficient density and temperature to reach the blackbody condition (τ〉2). Electron Bernstein waves (EBWs) are electrostatic waves that can propagate in overdense plasmas and have a high optical thickness at the electron cyclotron resonance layers as a result of their large kperp. In this article we report on measurements of EBW emission on the CDX-U spherical torus, where B0∼2 kG, 〈ne〉∼1013 cm−3 and Te(approximate)10–200 eV. Results are presented for electromagnetic measurements of EBW emission, mode converted near the plasma edge. The EBW emission was absolutely calibrated and compared to the electron temperature profile measured by a multipoint Thomson scattering diagnostic. Depending on the plasma conditions, the mode-converted EBW radiation temperature was found to be ≤Te and the emission source was determined to be radially localized at the electron cyclotron resonance layer. A Langmuir triple probe and a 140 GHz interferometer were employed to measure changes in the edge density profile in the vicinity of the upper hybrid resonance where the mode conversion of the EBWs is expected to occur. Initial results suggest EBW emission and EBW heating are viable concepts for plasmas where ωpe(very-much-greater-than)Ωce. © 2001 American Institute of Physics.
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  • 189
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    Topics: Physics , Electrical Engineering, Measurement and Control Technology
    Notes: A heavy ion beam diagnostic is being developed for the tokamak ISTTOK (R=0.46 m, a=0.085 m, Bt≅0.5 T, Ip=6–9 kA), based on multiple cell array detectors, aimed at the study of the time variation of the plasma density, electron temperature, poloidal magnetic field, and plasma potential radial profiles. In this article we describe an alternative method to the traditional electrostatic energy analyzers for measurements of the plasma potential based on the time-of-flight technique. The initial results of the measurements of the changes on the average plasma potential during tokamak discharges with minor disruptions are also presented. These results have been obtained measuring the time-of-flight of the ions of a pulsed primary beam from the electrostatic plates of the ion gun to the primary detector. © 2001 American Institute of Physics.
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    Review of Scientific Instruments 72 (2001), S. 579-582 
    ISSN: 1089-7623
    Source: AIP Digital Archive
    Topics: Physics , Electrical Engineering, Measurement and Control Technology
    Notes: A direct calibration technique for the heavy ion beam probe system using the mesh probe is established. The mesh probe makes it possible to calibrate the diagnostic system with the same condition as a real plasma measurement. The location of the sample volume could be determined with the spatial resolution of about 7.5 mm. It shows good agreement with this expected result by the trajectory code with an accuracy of about 1%. © 2001 American Institute of Physics.
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  • 191
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    Topics: Physics , Electrical Engineering, Measurement and Control Technology
    Notes: The MEDUSA array is a multielement, scintillator-based neutron time-of-flight spectrometer designed primarily to measure primary and secondary neutron production from indirect drive DD and DT capsule implosions at the Omega Laser in Rochester, NY. The array consists of 824 identical scintillator-photomultiplier tube detectors coupled to analog signal discriminators and high resolution, multihit time-to-digital converters, and is located 19.4 m from the center of the Omega target chamber. It is possible to accurately measure the neutron energy spectrum by simply measuring an adequate sample of neutron flight times to the array (the burn time width is negligible). However it is essential to understand the response of the array detectors to the fusion neutrons before an energy spectrum can be deduced from the data. This array response function is generally given in terms of a calibration constant that relates the expected number of detector hits in the array to the number of source neutrons. The calibration constant is a function of the individual detector gains, the thresholds of the discriminators, and the amount of neutron attenuating material between the array and the target. After gain matching the detectors, a calibration constant can be generated by comparing the array response against a known yield of neutrons (this requires dozens of implosions) or from a first principles measurement of the individual detector efficiencies. In this article, we report on the results of both calibrations of the MEDUSA array. In particular, we will focus on the issues and errors associated with the very different measurements required and discuss a new technique being considered for rapid in situ future calibrations. © 2001 American Institute of Physics.
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    Review of Scientific Instruments 71 (2000), S. 1090-1093 
    ISSN: 1089-7623
    Source: AIP Digital Archive
    Topics: Physics , Electrical Engineering, Measurement and Control Technology
    Notes: By switching the polarization of the screen and accelerator grid of a two grid extraction system, an ion or electron beam can be extracted from the same gas discharge. Such ion source operation mode, called bipolar extraction neutralization (BEN), allows a filamentless current neutralization of electrically insulated substrates. In this study BEN was used for a broad (12 cm), high current (0.36 A) ion beam from an electron cyclotron resonance ion source. The neutralization process is controlled by the duty cycle and frequency of the electron extraction pulses. An electrostatic monitor was positioned in the vicinity of the sputter target and used for monitoring the beam plasma potential and control of the neutralization parameters. The beam potential and extraction grid currents are presented time resolved for neutralization frequency from 20 to 80 kHz and duty cycle from 10% to 80%. This kind of monitoring allows not only control of the ion/electron extraction but also determination of the ion time of flight between the extraction grid and the substrate. © 2000 American Institute of Physics.
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    Review of Scientific Instruments 71 (2000), S. 1101-1103 
    ISSN: 1089-7623
    Source: AIP Digital Archive
    Topics: Physics , Electrical Engineering, Measurement and Control Technology
    Notes: An electron of a negative hydrogen ion (H−) can be easily detached by collisions with an external laser beam or residual gas molecules in the beam line, because its electron affinity is small (0.754 eV). The detached electrons provide information about the original negative hydrogen ions and should have the same velocity as the original hydrogen ions. By measuring the energy of the detached electrons, the energy of a negative hydrogen-ion beam can be estimated. A preliminary experimental result of an energy analysis of a H− beam using detached electrons is presented. © 2000 American Institute of Physics.
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  • 194
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    Review of Scientific Instruments 71 (2000), S. 1104-1106 
    ISSN: 1089-7623
    Source: AIP Digital Archive
    Topics: Physics , Electrical Engineering, Measurement and Control Technology
    Notes: The pepper-pot method and two slit-and-collector type techniques are tested for their applicability to measure the emittance of low energy ion beams. The exposure of Kapton foil, used here as the detector in the pepper-pot method, has been found to show a nonlinear behavior of the image contrast with the local power density of He+ beam for energy less than 10 keV. Therefore, the emittance measurement with the pepper-pot method must be made with the calibration of the contrast of the Kapton film in advance. The measured values of emittance, obtained by the different diagnostic schemes, are similar. From the view point of the negative ion beam measurement, the pepper-pot type system using Kapton film and the multislit-and-Faraday-cup system are proved to be promising. © 2000 American Institute of Physics.
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  • 195
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    Review of Scientific Instruments 72 (2001), S. 742-742 
    ISSN: 1089-7623
    Source: AIP Digital Archive
    Topics: Physics , Electrical Engineering, Measurement and Control Technology
    Notes: A pinhole soft x-ray imaging camera is being developed for use on the Caltech solar prominence simulation experiment and also the Caltech spheromak experiment. The camera is based upon a commercial gated intensifier which produces an image on a phosphor screen. Moderate signal level, excellent time resolution, and reasonable imaging have been obtained, but there has not been any determination of the x-ray energy spectrum. An estimation of the spectrum is now underway using filtered AXUV diodes and it is expected that knowledge of the x-ray energy will enable further optimization of the camera.© 2001 American Institute of Physics.
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  • 196
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    Review of Scientific Instruments 71 (2000), S. 2737-2741 
    ISSN: 1089-7623
    Source: AIP Digital Archive
    Topics: Physics , Electrical Engineering, Measurement and Control Technology
    Notes: The operation of a novel monolithic sapphire transducer from room temperature to cryogenic temperature is presented. The transducer is a microwave sapphire resonator that senses the motion of internal acoustic resonances through the interaction between electric and acoustic fields. The system is noncontacting and has low mechanical and electrical losses. Also, the microwave characteristics of sapphire are used as an inherent temperature sensor. High mechanical quality factors of 108 and 4.5×108 were attained at 300 and 4 K, respectively. © 2000 American Institute of Physics.
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    Review of Scientific Instruments 71 (2000), S. 2746-2750 
    ISSN: 1089-7623
    Source: AIP Digital Archive
    Topics: Physics , Electrical Engineering, Measurement and Control Technology
    Notes: We present a direct one-step technique to measure the torsional spring constant of cantilevers used for lateral or friction measurements with the atomic force microscope. The method simultaneously calibrates the photodiode response to the angular deflection of the cantilever. It does not rely upon any approximate theory for friction, nor upon any simplified model cantilever geometry or elasticity. The technique is verified by comparison with the calculated spring constant and with an independent measurement of the angle calibration. This nondestructive calibration may be performed with any type of cantilever, and the friction may subsequently be measured with any type of substrate or probe. © 2000 American Institute of Physics.
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    Review of Scientific Instruments 71 (2000), S. 2765-2771 
    ISSN: 1089-7623
    Source: AIP Digital Archive
    Topics: Physics , Electrical Engineering, Measurement and Control Technology
    Notes: The combination of two well-established dynamic scanning force microscopy (SFM) modes is incorporated for SFM in combined dynamic X mode or CODY Mode® SFM. A vertical modulation of low frequency and large amplitude is superimposed with a second vertical modulation of high frequency and low amplitude leading to a combination of pulsed force mode SFM, force modulation, and phase sensitive SFM. SFM in the new mode allows the simultaneous mapping of a number of physical surface properties including adhesive force and elasticity over one scan. The new SFM technique is nondestructive and alteration or even destruction of the sample surface is reduced to a minimum. A polymer blend (two homopolymers spin coated on silicon from a tetrahydrofuorane solution of a mixture of poly-2-vinylpyridin and polytertbutylmethacrylate) was used as a sample for comparative measurements between pulsed force mode, force modulation mode and the new SFM mode. © 2000 American Institute of Physics.
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    Review of Scientific Instruments 71 (2000), S. 2772-2775 
    ISSN: 1089-7623
    Source: AIP Digital Archive
    Topics: Physics , Electrical Engineering, Measurement and Control Technology
    Notes: In atomic force microscopy cantilevers are used to detect forces caused by interactions between probing tip and sample. The minimum forces which can be detected with commercial sensors are typically in the range of 10−12 N. In the future, the aim will be to construct sensors with improved sensitivities to detect forces in the range of 10−18 N. These sensors could be used for mass spectroscopy or magnetic resonance force microscopy. Achieving this goal requires smaller sensors and increased quality factor Q. In this article we describe a model to characterize the dynamics of cantilevers of each eigenmode. In contrast to previous models, the damping is treated rigorously in the calculations. © 2000 American Institute of Physics.
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    Review of Scientific Instruments 71 (2000), S. 2781-2783 
    ISSN: 1089-7623
    Source: AIP Digital Archive
    Topics: Physics , Electrical Engineering, Measurement and Control Technology
    Notes: We report fabrication and measurements with two- and four-point probes with nanoscale dimensions, for high spatial resolution conductivity measurements on surfaces and thin films. By combination of conventional microfabrication and additive three-dimensional nanolithography, we have obtained electrode spacings down to 200 nm. At the tips of four silicon oxide microcantilevers, narrow carbon tips are grown in converging directions and subsequently coated with a conducting layer. The probe is placed in contact with a conducting surface, whereby the electrode resistance can be determined. The nanoelectrodes withstand considerable contact force before breaking. The probe offers a unique possibility to position the voltage sensors, as well as the source and drain electrodes in areas of nanoscale dimensions. © 2000 American Institute of Physics.
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