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  • Articles  (113)
  • Articles: DFG German National Licenses  (113)
  • porous silicon  (61)
  • morphology  (55)
  • 2000-2004  (113)
  • 1
    Electronic Resource
    Electronic Resource
    Porosified Silicon Wafer Structures Impregnated With Platinum Anti-Tumor Compounds: Fabrication, Characterization, and Diffusion Studies (2000)
    Springer
    Biomedical microdevices 2 (2000), S. 265-272 
    Details
    ISSN: 1572-8781
    Keywords: porous silicon ; cis-platin ; drug delivery ; calcium phosphate ; carbo-platin
    Source: Springer Online Journal Archives 1860-2000
    Topics: Medicine , Technology
    Notes: Abstract In this work, the incorporation and characterization of cis-platin (cis-diammine dichloroplatinum(II)), carbo-platin [cis-diammine(cyclobutane-1,1-dicarboxylato] platinum(II)), and Pt(en)Cl2 (ethylenediamminedichloro platinum(II)) within layers of calcium phosphate on porous Si/Si substrates are described. These materials have been characterized by scanning electron microscopy, secondary ion mass spectrometry, and X-ray energy dispersive spectroscopy. The diffusion of platinum species from the doped calcium phosphate layers has also been investigated by UV-visible absorption spectrometry and inductively-coupled plasma spectroscopy. The influence of initial platinum concentration, the impact of thermal annealing of the calcium phosphate/porous Si/Si matrix, as well as the effect of varying the ligand coordination sphere of the Pt complex on its ability to be delivered to the surroundings have also been analyzed. For the case of cis-platin, it is found that increasing the concentration of platinum complex in the electrolyte during cathodic growth of calcium phosphate results in a relatively greater concentration of Pt incorporated into the calcium phosphate layers and a larger amount of Pt which subsequently can be delivered to the surrounding medium upon exposure to solvent.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1023/A:1009951121205
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  • 2
    Electronic Resource
    Electronic Resource
    Submersible observations of Equatorial Atlantic mantle: The St. Paul Fracture Zone region (2000)
    Springer
    Marine geophysical researches 21 (2000), S. 529-560 
    Details
    ISSN: 1573-0581
    Keywords: Structure ; morphology ; petrology ; peridotite-basalt
    Source: Springer Online Journal Archives 1860-2000
    Topics: Geosciences , Physics
    Notes: Abstract The St. Paul F.Z. is a large structural domain made up of multiple transform faults interrupted by several Intra-Transform Ridge (ITR) spreading segments. Two regions were studied in details by submersible: (1) The ITR short (〈20 km in length) segment near 0° 37′N–25° 27′W and 1° N–27° 42′W and (2) The St. Peter and St. Paul's Rocks (SPPR) massif located at 29° 25′W (¡3700 m depth). (1) The short ITR segments consist of a magma starved rift valley with recent volcanic activities at 4700 m depth. A geological profile made along the rift valley wall showed localized volcanics (basalts and dykes) which are believed to overlay and intrude the ultramafics. The geological setting and the high ultramafic/volcanic ratio suggest an extremely low magmatic supply and crustal-mantle uplift during lithospheric stretching and denudation. (2) The St. Peter and St. Paul's Rocks (SPPR) massif consists of a sigmoidal ridge within the active transform zone. The SPPR is divided into two different geological domains called the North and the South Ridges. The North Ridge consists of strongly tectonized fault scarps composed of banded and mylonitized peridotite, sporadic gabbros (3900–2500 m) and metabasalts (2700–1700 m). The South Ridge is less tectonized with undeformed, serpentinized spinel lherzolite (2000–1400 m) and basalts. Extensional motion and denudation accompanied by diapirism affected the South Ridge within a transform domain. Instead, the North Ridge was formed during an important strike-slip and faulting motion resulting in the uplifted portion of the St. Paul F.Z. transverse ridge. There is a regional compositional variation of the volcanics where E-MORBs and alkali basalts are produced on the SPPR massif and are comparable to the adjacent northern segments of the Mid-Atlantic Ridge. On the other hand, N and T- MORBs collected from the eastern part of the St. Paul F.Z. (25° 27′ W IRT) are similar to the volcanics from the southern segments of the MAR. The peridotites exposed in these provinces (SPPR and ITR) are similar in their REE and trace element distribution. Different degrees (3–15%) of partial melting of a mixed composite mantle consisting of spinel and amphibole bearing lherzolite veined with 5–40% clinopyroxenite gave rise to the observed MORBs and alkali basalts.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1023/A:1004819701870
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  • 3
    Electronic Resource
    Electronic Resource
    T.H. Huxley's Criticism of German Cell Theory: An Epigenetic and Physiological Interpretation of Cell Structure (2000)
    Springer
    Journal of the history of biology 33 (2000), S. 247-289 
    Details
    ISSN: 1573-0387
    Keywords: cell theory ; morphology ; Thomas Henry Huxley ; physiology ; Schleiden-Schwann cell theory ; Romantic biology ; scientific zoology ; cytology ; preformationism ; natural history ; epigenesis ; Kernmonopol ; histology ; Albert von Kölliker ; embryology
    Source: Springer Online Journal Archives 1860-2000
    Topics: Biology , History
    Notes: Abstract In 1853, the young Thomas Henry Huxley published a long review of German cell theory in which he roundly criticized the basic tenets of the Schleiden-Schwann model of the cell. Although historians of cytology have dismissed Huxley’s criticism as based on an erroneous interpretation of cell physiology, the review is better understood as a contribution to embryology. “The Cell-theory” presents Huxley’s “epigenetic” interpretation of histological organization emerging from changes in the protoplasm to replace the “preformationist” cell theory of Schleiden and Schwann (as modified by Albert vonKölliker), which posited the nucleus as the seat of organic vitality. Huxley’s views influenced a number of British biologists, who continued to oppose German cell theory well into the twentieth century. Yet Huxley was pivotal in introducing the new German program of “scientific zoology” to Britain in the early 1850s,championing its empiricist methodology as a means to enact broad disciplinary and institutional reforms in British natural history.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1023/A:1004881730937
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  • 4
    Electronic Resource
    Electronic Resource
    TMDSC and Atomic Force Microscopy Studies of Morphology and Recrystallization in Polyesters Including Oriented Films (2000)
    Springer
    Journal of thermal analysis and calorimetry 59 (2000), S. 227-243 
    Details
    ISSN: 1572-8943
    Keywords: atomic force microscopy (AFM) ; morphology ; polyester ; recrystallization ; TMDSC
    Source: Springer Online Journal Archives 1860-2000
    Topics: Chemistry and Pharmacology
    Notes: Abstract The thermal and crystal morphological properties of poly[ethylene teraphthalate] (PET) and poly(ethylene-2,6-naphthalenedicarboxylate) (PEN) biaxially oriented films were compared to amorphous and other isotropic semi-crystalline samples. Crystal melting as a function of temperature was characterized by temperature modulated DSC (TMDSC) and found to begin just above the glass transition for both oriented films. About 75°C above the glass transitions, substantial exothermic recrystallization begins and continues through the final melting region in oriented films. The maximum in the non-reversing TMDSC signal for the oriented films signifies the maximum recrystallization exothermic activity with peaks at 248°C and 258°C for PET and PEN, respectively. The final melting endotherm detected was 260°C and 270°C for PET and PEN, and is shown by the TMDSC data and by independent rapid heating rate melting point determinations to be due to the melting of species recrystallized during the heating scan. The results are compared with TMDSC data for initially amorphous and melt crystallized samples. The volume fraction of rigid species (Frigid=total crystal fraction plus ‘rigid amorphous or non-crystalline species’) were measured by TMDSC glass transition data, and contrasted with the area fraction of rigid species at the oriented film surface characterized with very high resolution atomic force microscopy (AFM) phase data. The data suggest that the 11 nm wide hard domains in PET, and 21 nm wide domains in PEN film detected by AFM consist of both crystal and high stiffness interphase species.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1023/A:1010148331705
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  • 5
    Electronic Resource
    Electronic Resource
    Polypropylene Crystallization in an Ethylene-propylene-diene Rubber Matrix (2000)
    Springer
    Journal of thermal analysis and calorimetry 61 (2000), S. 437-450 
    Details
    ISSN: 1572-8943
    Keywords: crystallization ; EPDM ; kinetics ; morphology ; PP ; rubber
    Source: Springer Online Journal Archives 1860-2000
    Topics: Chemistry and Pharmacology
    Notes: Abstract The effect of the incorporation of an amorphous immiscible polymer (ethylene-propylene-diene- terpolymer) on the PP crystallization kinetics and thermodynamics is investigated by thermal analysis. The results of the investigation have shown that EPDM acts as a nucleant agent. A marked decrease of the half time of PP crystallization, τ1/2 , as well as a sensible increase of the overall crystallization rate, K n , has been observed in the presence of EPDM. Moreover, at any crystallization temperature, a minimum of τ1/2 , is obtained at 25% EPDM content in the blend. The Avrami model has been successfully applied to describe the crystallization kinetics of the blend. The kinetic curves obtained under non-isothermal conditions confirm the results obtained under isothermal conditions and demonstrate the nucleant action of the EPDM phase on the PP crystallization.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1023/A:1010165317028
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  • 6
    Electronic Resource
    Electronic Resource
    Mechanical Properties of Natural Fibre Mat Reinforced Thermoplastic (2000)
    Springer
    Applied composite materials 7 (2000), S. 403-414 
    Details
    ISSN: 1573-4897
    Keywords: flax fibres ; natural fibres ; thermoplastics ; tensile properties ; impact properties ; anisotropy ; electron microscopy ; morphology ; compression moulding ; processing
    Source: Springer Online Journal Archives 1860-2000
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics
    Notes: Abstract The use of natural fibres instead of man made fibres, as reinforcements in thermoplastics, gives interesting alternatives for production of low cost and ecologically friendly composites. In this work different commercially available semi-finished natural fibre mat reinforced thermoplastics (NMT) composites have been studied. Mechanical properties and microstructure of different NMT composites were investigated and compared to conventional GMT (glass fibre mat reinforced thermoplastic) composites and pure polypropylene (PP). The study included also NMT composites manufacturing processing parameters as processing temperatures and pressure during compression moulding. The results showed that NMT composites have a high stiffness compared to pure polymer and the NMT with a high fibre content (50% by weight) showed even better stiffness than the GMT. The GMT composites had superior strength and impact properties compared to the NMT which might be due to the relatively low strength of the natural fibres but also to poor adhesion to the PP matrix. The NMT materials showed a large dependence on direction and are therefore believed to have more fibres oriented in one direction. The stronger direction (0°) of the NMT was in some cases as much as 45% better than the 90° direction.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1023/A:1026546426764
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  • 7
    Electronic Resource
    Electronic Resource
    MoSx Thin Films by Thermolysis of a Single-Source Precursor (2000)
    Springer
    Journal of sol gel science and technology 19 (2000), S. 821-824 
    Details
    ISSN: 1573-4846
    Keywords: MoS x ; thin film ; liquid film coating ; thermolysis ; morphology
    Source: Springer Online Journal Archives 1860-2000
    Topics: Chemistry and Pharmacology
    Notes: Abstract Thin films of MoS x have been prepared on silicon substrates by spin coating and thermolysis of 0.5 M solutions of alkyldiammonium tetrathiomolybdates in 1,2-ethanediamine (EDA) and 1,2-propanediamine (12PDA). The films have been heat treated in air at temperatures between 80 and 250°C and under N2 atmosphere at temperatures between 300 and 800°C. X-ray diffraction shows a restricted crystallisation and amorphous residues in both kind of films. EDA-based films exhibit a high tendency to crystallise whereas 12PDA-based films form associated structures with the solvent preventing precursor crystallisation. An insight into the processes occurring in film formation is gained by infrared spectroscopy which indicates a beginning of the decomposition of the 12PDA-based film at temperatures as low as 80°C with incorporation of the diamine solvent. In contrast, the EDA-based films show first signs of a decomposition at 150°C. The decomposition of the intermediate MoS3 in both cases starts between 250 and 300°C. By means of SNMS depth profiles carbon contents up to 21 and 32 atom-% were found in EDA- and 12PDA-based films, respectively. The films show a significant deficit of sulphur which is compensated by the carbon. Near the surface of the coatings a loss of carbon is observed.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1023/A:1008728604305
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  • 8
    Electronic Resource
    Electronic Resource
    Influence of the Layer Morphology on the Electrical Properties of Sol Gel Transparent Conducting Oxide Coatings (2000)
    Springer
    Journal of sol gel science and technology 19 (2000), S. 435-439 
    Details
    ISSN: 1573-4846
    Keywords: morphology ; electrical properties ; transparent conductive coatings
    Source: Springer Online Journal Archives 1860-2000
    Topics: Chemistry and Pharmacology
    Notes: Abstract Tranparent conducting coatings have been prepared by sol gel methods either by a conventional sol-gel process (Antimony doped Tin Oxide—ATO, Aluminium doped Zinc Oxide—AZO) or a new wet chemical process using fully dispersed crystalline nanoparticles (ATO, Indium Tin Oxide—ITO). The dip coating technique has been used as deposition technique with single coating thickness varying from a few nanometer to ca. 400 nm. The layers have been fired in a furnace. Structural properties have been determined by x-ray diffraction and TEM analysis and the electrical properties by the van der Pauw/Hall measurement. Three different coating procedures have been used to investigate the effect on the structure, morphology and the electrical properties of the coatings. It is shown that the individual layer thickness in multilayer coatings influences dramatically the mentioned properties. Very thin individual layers favour a heterogeneous nucleation with dense columnar growth of the crystallites leading to low electrical resistivity (ρ ≈ 10−3Ω cm), while thick individual layers result in a porous morphology made of small crystallites leading to resistivities in the 10−2Ω cm range.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1023/A:1008747429862
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  • 9
    Electronic Resource
    Electronic Resource
    The First Finding of the Actinia Synandwakia hozawai in the Sea of Okhotsk (2000)
    Springer
    Russian journal of marine biology 26 (2000), S. 445-449 
    Details
    ISSN: 1608-3377
    Keywords: actinia ; Synandwakia hozawai ; Sea of Okhotsk ; morphology ; nematocysts
    Source: Springer Online Journal Archives 1860-2000
    Topics: Biology
    Notes: Abstract The finding of the actinia Synandwakia hozawai in the coastal waters of northern Sakhalin (Sea of Okhotsk) suggests a wider range of this species, which was previously only known to inhabit the coastal waters of eastern Japan. Data are presented on the morphology of the S. hozawai specimen from the Sea of Okhotsk and the types of its nematocysts.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1023/A:1009455007047
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  • 10
    Electronic Resource
    Electronic Resource
    A newLeptographium species associated withTomicus piniperda in south-western China (2000)
    Springer
    Mycoscience 41 (2000), S. 573-578 
    Details
    ISSN: 1618-2545
    Keywords: China ; Leptographium ; morphology ; taxonomy ; Tomicus piniperda
    Source: Springer Online Journal Archives 1860-2000
    Topics: Biology
    Notes: Abstract Tomicus species (Coleoptera: Scolytidae) are serious pests of pines with a wide distribution in Europe, Asia and America. In Yunnan, south-western China,T. piniperda has destroyed more than 0.5 million ha ofPinus yunnanensis in the past 15 years. A blue stain fungus belonging to the genusLeptographium is associated with both the shoot-feeding and trunk-attacking stages of the beetle's life cycle. The fungus is morphologically similar to the anamorph ofOphiostoma crassivaginatum and toL. pyrinum, which are both characterised by short robust conidiophores and hyphae covered by a granular layer. Both these species have been isolated from conifers and are associated with insects. After comparing the fungus fromT. piniperda with similarLeptographium species, using light and scanning electron microscopy, we concluded that it represents a new taxon, which is described here asL. yunnanense sp. nov.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1007/BF02460923
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