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  • Polymer and Materials Science  (1,063)
  • 1980-1984  (1,063)
  • 1
    Electronic Resource
    Electronic Resource
    Synthesis of fibre-forming copolymers of acrylonitrile with acrylates in systems based on lithium alkoxides (1984)
    Weinheim : Wiley-Blackwell
    Acta Polymerica 35 (1984), S. 65-67 
    Details
    ISSN: 0323-7648
    Keywords: Chemistry ; Polymer and Materials Science
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology , Physics
    Description / Table of Contents: Die Copolymerisation von Acrylnitril und Acrylaten wurde in Dimethylformamid bei hohem Acrylnitril/Acrylat-Verhältnis im Temperaturbereich von -50 bis +10°C durch Lithiumalkoxide initiiert. Die Bedingungen zur direkten Präparation von Spinnlösungen der Copolymere wurden erarbeitet. Das Lösungsspinnen dieser Copolymere durch Orientierungsfällung ergab Fasern mit hohen Festigkeitswerten.
    Notes: The copolymerization of acrylonitrile with acrylates has been initiated by lithium alkoxides in dimethylformamide at a high acrylonitrile/acrylate ratio over the temperature range from -50 to 10°C. The conditions for a direct preparation of spinning solutions of the copolymers were determined. The solution-spinning of these copolymers by orientational precipitation yielded fibres exhibiting high strength properties.
    Additional Material: 3 Tab.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/actp.1984.010350115
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  • 2
    Electronic Resource
    Electronic Resource
    Low energy electron loss studies of cuInSe2 surfaces (1982)
    Chichester [u.a.] : Wiley-Blackwell
    Surface and Interface Analysis 4 (1982), S. 227-229 
    Details
    ISSN: 0142-2421
    Keywords: Chemistry ; Polymer and Materials Science
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Physics
    Notes: The low energy loss spectra (LELS) of clean and oxygen contaminated (111) p-type CuInSe 2 single crystals are reported. Losses due to interband transitions and plasmon excitations are observed. By varying the primary electron energy (100-500 eV) both surface and bulk features of the conduction bands are probed. As oxygen is adsorbed on the surface of the CuInSe 2 (at room temperature), the In and Se atoms seem to associate with themselves and with oxygen, whereas the Cu atoms do not seem to play a direct role in the oxidation process. LELS Spectra are presented as a function of primary beam energy and oxygen absorption.
    Additional Material: 3 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/sia.740040602
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  • 3
    Electronic Resource
    Electronic Resource
    Surface structure and NiO dispersion for NiO/γ-Al2O3 catalysts (1982)
    Chichester [u.a.] : Wiley-Blackwell
    Surface and Interface Analysis 4 (1982), S. 234-239 
    Details
    ISSN: 0142-2421
    Keywords: Chemistry ; Polymer and Materials Science
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Physics
    Notes: Chemisorption of CO at temperatures below 100°C has been used to evaluate the dispersion of NiO in a series of NiO/γ-Al2O3 catalysts. CO adsorption measurements were supplemented by i.r. spectroscopy to establish the CO/NiO stoichiometry. From monolayer coverage data derived from Freundlich's equation, the percentage of NiO dispersion and the average NiO crystallite size were calculated. The crystallite size of supported NiO was found to be practically constant for NiO loadings from 1 to 8 wt%, experimenting an abrupt increase for higher NiO contents. These results were consistent with additional information on the surface structure of the catalysts obtained by IR spectroscopy, X-ray diffraction, magnetic susceptibility, and reduction with H2.
    Additional Material: 6 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/sia.740040604
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  • 4
    Electronic Resource
    Electronic Resource
    Kinetics of epoxy resin synthesis on the basis of GPC measurements (1981)
    New York, NY [u.a.] : Wiley-Blackwell
    Journal of Applied Polymer Science 26 (1981), S. 2783-2786 
    Details
    ISSN: 0021-8995
    Keywords: Chemistry ; Polymer and Materials Science
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology , Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics , Physics
    Additional Material: 2 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/app.1981.070260827
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  • 5
    Electronic Resource
    Electronic Resource
    Storage hardening and “abnormal” groups in guayule rubberThis article was presented at the 27th IUPAC Congress, Helsinki, Finland, August 1979. (1981)
    New York, NY [u.a.] : Wiley-Blackwell
    Journal of Applied Polymer Science 26 (1981), S. 1511-1517 
    Details
    ISSN: 0021-8995
    Keywords: Chemistry ; Polymer and Materials Science
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology , Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics , Physics
    Notes: The hardening process of natural (Hevea brasiliensis) rubber, that takes place when this rubber is stored in dry conditions over long periods of time, has been correlated with the presence of reactive “abnormal” groups directly grafted on the polymeric chain and in the serum of the latex. In the present work, natural Hevea (HR) and Guayule (Parthenium argentatum) rubber (GR) were stored under accelerated conditions and the changes in Mooney viscosity and molecular weight measured. The results showed that while HR undergoes hardening, GR keeps its Mooney viscosity constant, as does a constant viscosity (CV) Hevea rubber. These results are explained by the absence of functional “abnormal” groups that sustain the hardening reactions.
    Additional Material: 4 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/app.1981.070260508
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  • 6
    Electronic Resource
    Electronic Resource
    Effect of fibronectin on the adhesion of an established cell line to a surface reactive biomaterial (1982)
    Hoboken, NJ : Wiley-Blackwell
    Journal of Biomedical Materials Research 16 (1982), S. 195-207 
    Details
    ISSN: 0021-9304
    Keywords: Chemistry ; Polymer and Materials Science
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Medicine , Technology
    Notes: We have demonstrated that an established hamster cell line (NIL 8 M-2) will adhere to the bioceramic bioglass. The rate at which the NIL 8 M-2 cells assume a spread morphology on bioglass is density dependent and the morphology displayed by NIL 8 M-2 cells attached to bioglass is much more elongated than that displayed by NIL 8 M-2 cells attached to nonreactive glass. Precoating the bioglass with the plasma form of human fibronectin significantly reduces the density dependent nature of cell spreading. Coating the bioglass with fibronectin also reduces the time required for cell spreading and changes the morphology of the attached cells from an elongated to an extremely flattened shape. Our work raises the possibility that bone-implant adhesion might be improved by introducing molecules relevant to cell-substrate attachment into the biomaterial prior to implantation.
    Additional Material: 5 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/jbm.820160303
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  • 7
    Electronic Resource
    Electronic Resource
    Untersuchungen zur Belastbarkeit von Polybutylenterephthalat (1981)
    Weinheim : Wiley-Blackwell
    Acta Polymerica 32 (1981), S. 465-466 
    Details
    ISSN: 0323-7648
    Keywords: Chemistry ; Polymer and Materials Science
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology , Physics
    Description / Table of Contents: The deformation stability of polybutylene terephthalate in dependence on stress and temperature was determined. The lifetime of the polymer is described as a function of these parameters. The results are compared with the values obtained with other polymers.
    Notes: Die Deformationsstabilität von Polybutylenterephthalat wurde in Abhängigkeit von der Spannung und der Temperatur bestimmt. Die Lebensdauer des Polymers kann als eine Funktion dieser Parameter angegeben werden. Die Ergebnisse werden mit den an anderen Polymeren erhaltenen Werten verglichen.
    Additional Material: 4 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/actp.1981.010320806
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  • 8
    Electronic Resource
    Electronic Resource
    Corrosion fatigue behaviour of nitrogen-implanted steel in water (1980)
    Weinheim [u.a.] : Wiley-Blackwell
    Materials and Corrosion/Werkstoffe und Korrosion 31 (1980), S. 783-789 
    Details
    ISSN: 0947-5117
    Keywords: Chemistry ; Polymer and Materials Science
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics
    Description / Table of Contents: Schwingungskorrosionsverhalten von nitriertem Stahl in WasserDas Schwingungskorrosionsverhalten von nitriertem Stahl in neutralen Lösungen wurde unter Verwendung von schwingenden, einseitig eingespannten Proben (cantilever beam method) elektrochemisch (Ekorr/Zeit, Rp-Messung) und mittels Rasterelektronenmikroskopie untersucht.Die Korrosionsgeschwindigkeit in stagnierenden Flüssigkeiten ist bei dem nitrierten Stahl, unabhängig von der Stickstoffkonzentration, niedriger als bei unbehandeltem Stahl; die an der Oberfläche entstehenden Oxidschichten besitzen deutlich bessere Schutzwirkung.Bei einer zyklischen Belastung (25,4 kg/mm-2, 16,6 Hz) ist die Rißauslösung verzögert. Die Zeit bis zum Bruch ist beträchtlich kürzer als bei nicht nitrierten Proben (zumindest unter den verwendeten Versuchsbedingungen). Die Erhöhung der Rißausbreitungsgeschwindigkeit läßt sich erklären durch die Gefügeschädigungen, die durch das Nitrieren hervorgerufen werden. Die Bruchmorphologie wird ebenfalls erörtert.
    Notes: The corrosion fatigue behaviour of nitrogen implanted iron in neutral solutions has been investigated utilizing the oscillating cantilever beam method, by means of electrochemical (Ecorr vs. time plots, Rp measurements) and S. E. M. techniques.The calculated corrosion rate under stagnant conditions is lowered for the implanted iron at all nitrogen doses with respect to untreated iron. The surface oxide layers achieve enhanced protecting capacity.Consequently under a cyclic load of 25.4 kg mm-2, at a frequency of 16.6 Hz, cracks nucleation is delayed. The time to breaking of implanted specimens is considerably lower in our experimental conditions compared to untreated iron. The increase in the crack growth rate is consistent with the detrimental action of structural damage following implantation. The fracture morphology is also discussed.
    Additional Material: 11 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/maco.19800311006
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  • 9
    Electronic Resource
    Electronic Resource
    Effect of mineral filler sepiolite on sulphur-free thiuram vulcanization of natural rubber (1982)
    Weinheim : Wiley-Blackwell
    Angewandte Makromolekulare Chemie 104 (1982), S. 189-201 
    Details
    ISSN: 0003-3146
    Keywords: Chemistry ; Polymer and Materials Science
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology , Physics
    Description / Table of Contents: Der Einfluß von Sepiolit auf die schwefelfreie Vulkanisation von Naturkautschuk durch Tetramethylthiuramdisulfid, mit und ohne Aktivator (Triethanolamin), wurde untersucht. Dabei wurde der Sepioliteinfluß auf die a) kinetischen Vulkanisations-Parameter, b) Vernetzungsdichte, c) Art der Vernetzungsbrücken, d) Vernetzungs-ausbeute E und e) Bildung von Zinksulfid studiert. Mit zunehmendem Sepiolit-Anteil wächst die Vulkanisationsgeschwindigkeit, während die Vernetzungsdichte abnimmt. Aufgrund dieser Ergebnisse wird der Mechanismus der Vulkanisation diskutiert.
    Notes: The effect of sepiolite on the sulphurless vulcanization of NR by tetramethylthiuram disulphide, with and without activator (triethanolamine) was studied. The influence on: a) kinetic vulcanization parameters, b) crosslinking density, c) crosslinking types, d) efficiency factor E and e) zinc sulphide formation was considered. The vulcanization rate increases with increasing sepiolite level but crosslinking density is reduced. Based on these results a vulcanization mechanism is proposed and discussed.
    Additional Material: 3 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/apmc.1982.051040116
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  • 10
    Electronic Resource
    Electronic Resource
    Study of the structure and properties of phosphorinated segmented polyurethanes (1984)
    Weinheim : Wiley-Blackwell
    Angewandte Makromolekulare Chemie 121 (1984), S. 159-169 
    Details
    ISSN: 0003-3146
    Keywords: Chemistry ; Polymer and Materials Science
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology , Physics
    Description / Table of Contents: Der Einfluß einer Folge von gestreckten physikalischen Bindungen in steifen Polyurethanblöcken wurde durch Röntgenstreuungs-, thermographische und thermomechanische Messungen untersucht. Es wurde gezeigt, daß durch Variieren der Art und Struktur des quaternierenden Agens die Struktur und Eigenschaften von Polyurethanblöcken gezielt geändert werden kann, Hitzebehandlung (Tempern) des Polyurethans und der Polyurethanionomerproben hat bewiesen, daß das Wachsen der harten Bereiche vor allem darauf beruht, daß steife Segmente sich an schon vorhandene Hart-Domänen anlagern.
    Notes: The effect of an expanded set of physical bonds in rigid polyurethane segments has been studied by X-ray measurements, thermography, thermomechanics, etc. It has been shown that, by varying the nature and structure of quaternizing agent, the structure and properties of the segmented polyurethanes can be purposefully varied. Heat treatment (annealing) of polyurethanes, and polyurethane-ionomer samples has proved that the growth of hard domains is first of all due to the rigid segments associating with hard domains already existing.
    Additional Material: 4 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/apmc.1984.051210115
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