ISSN:
0749-1581
Keywords:
2D NMR
;
Gibberellin A3
;
3,13-diacetylgibberellin A3
;
Chemistry
;
Analytical Chemistry and Spectroscopy
Source:
Wiley InterScience Backfile Collection 1832-2000
Topics:
Chemistry and Pharmacology
Notes:
The complete analysis of the 1H NMR spectra of the phytohormone gibberellin A3 and its 3,13-diacetyl derivative has been performed. ASIS and 2D J-resolved spectroscopy were used to disentangle the complex spin systems, which were further analysed by 1H-1H homocorrelated spectroscopy and spin decoupling. 2D 1H-13C shift correlated spectra not only supported the identification of individual protons but also allowed the clarification of some controversial 13C assignments.
Additional Material:
5 Ill.
Type of Medium:
Electronic Resource
URL:
http://dx.doi.org/10.1002/mrc.1260250312
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