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  • 1
    Electronic Resource
    Electronic Resource
    Four-, Five- and Six-Membered Silylhydrazine-Ring Systems (1994)
    s.l. : American Chemical Society
    Organometallics 13 (1994), S. 3985-3989 
    Details
    ISSN: 1520-6041
    Source: ACS Legacy Archives
    Topics: Chemistry and Pharmacology
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1021/om00022a039
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  • 2
    Electronic Resource
    Electronic Resource
    Characterization of AlN powder produced by the reaction of AlCl3 with hexamethyldisilazane (1990)
    Springer
    Journal of materials science 9 (1990), S. 222-224 
    Details
    ISSN: 1573-4811
    Source: Springer Online Journal Archives 1860-2000
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1007/BF00727723
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  • 3
    Electronic Resource
    Electronic Resource
    Reaktion von Alkyl- und Arylchlorsilanen mit Phosph(III) en-imidamiden (1976)
    Springer
    Monatshefte für Chemie 107 (1976), S. 939-943 
    Details
    ISSN: 1434-4475
    Source: Springer Online Journal Archives 1860-2000
    Topics: Chemistry and Pharmacology
    Notes: Abstract The reaction of RSiCl3 (R=CH3, C2H5, C6H5) and R2SiCl2 (R=CH3) with one mole of the phosphenimidous amides R2N−P=NR′ [R=R′=Si(CH3)3; R=Si(CH3)3, R′=C(CH3)3] yieds a four membered PN2Si-ring system under elimination of (CH3)3SiCl.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1007/BF00904481
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  • 4
    Electronic Resource
    Electronic Resource
    Zur Reaktion von Fluorsilanen mit lithiierten Aminen (1977)
    Springer
    Monatshefte für Chemie 108 (1977), S. 1099-1104 
    Details
    ISSN: 1434-4475
    Source: Springer Online Journal Archives 1860-2000
    Topics: Chemistry and Pharmacology
    Notes: Abstract The reaction of fluorosilanes with lithium salts of bulky amines like tetramethyl-piperidine and di-tert. butylamine leads to stable aminofluorosilanes of the type R-SiF2-NR′R″ [R=F, C(CH3)3, C6H5, C6H4N(CH3)2]. Lithium salts of silylamines react analogously: R2Si(NR′-SiF2R″)2 (R=R′= =CH3, R″=C6H5). An eight membered Si−N-ring is obtained in the reaction of a disubstituted silylaminofluorosilane with the dilithium salt of a silylamine. The mass-,1H-, and19F-NMR spectra of the above mentioned compounds are reported.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1007/BF00897691
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  • 5
    Electronic Resource
    Electronic Resource
    Intramolekulare Cyclisierung von Aminofluorsilanen (1978)
    Springer
    Monatshefte für Chemie 109 (1978), S. 1067-1073 
    Details
    ISSN: 1434-4475
    Source: Springer Online Journal Archives 1860-2000
    Topics: Chemistry and Pharmacology
    Notes: Abstract Aminofluorosilanes react with lithiated amines undergoing LiF-elimination and substitution (1). The acyclic silicon-nitrogen-compound2 is isolated in the reaction with a difluorosilane after renewed lithiation.2 is cyclisated in the reaction with butyllithium by butane- and LiF-elimination (3). Aminofluorosilanes with bulky (4) or mesomeric stabilized (5) ligands form stable lithioaminofluorosilanes, which react with fluorosilanes giving substitution products (6, 7).6 and7 react with the lithium salt oftert-butylamin in a molar ratio of 1∶2 to give8 and9 by intramolecular cyclisation.—The mass,1H and19F nmr spectra of the compounds are reported.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1007/BF00913009
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  • 6
    Electronic Resource
    Electronic Resource
    Zur Reaktion von Hydrazinen mit Fluorsilanen und lithiierten Aminen (1979)
    Springer
    Monatshefte für Chemie 110 (1979), S. 289-296 
    Details
    ISSN: 1434-4475
    Keywords: Fluorosilylhydrazines ; 19 F nmr ; 29 Si nmr ; 1,3,4-Triaza-2,5-disilacyclopentanes
    Source: Springer Online Journal Archives 1860-2000
    Topics: Chemistry and Pharmacology
    Notes: Abstract Lithium salts of hydrazines react with fluorosilanes under formation of fluorosilylhydrazines and LiF. Five membered rings are obtained in the reaction of bis(fluorosilyl)-hydrazines with lithiated amines. The mass,1H-and19F-nmr spectra of the compounds are reported.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1007/BF00911916
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  • 7
    Electronic Resource
    Electronic Resource
    Synthese neuer Aminofluorsilane, sowie Alkoxylierung von Bis (trimethylsilyl)-amino-fluorsilanen (1975)
    Springer
    Monatshefte für Chemie 106 (1975), S. 459-471 
    Details
    ISSN: 1434-4475
    Source: Springer Online Journal Archives 1860-2000
    Topics: Chemistry and Pharmacology
    Notes: Abstract The reaction of aminofluorsilanes of the type (R=H,F) (Me 3Si)2N−SiF2R with two moles of ammonia, or of a mono- or dialkylamine, yields the corresponding amino-compounds, e.g. (Me 3Si)2N−Si(F)R−NH2, (Me 3Si)2N−Si(F)R−NHR′ and (Me 3Si)2N−Si(F)R−NR2′ (R′=Me, Et). Analogous products are obtained by reaction of the aminofluorosilanes with lithium salts of amines with bulky organic substituents in a 1 : 1 molar ratio. Alkoxy- and aryloxyaminofluorosilanes are prepared by the reaction of sodium alcoholates and sodium phenolate with (Me 3Si)2N−Si(F2)R (R=H, C2H3, C2H5, C6H5). The i.r.-, mass-,1H- and19F-NMR spectra of the above compounds are reported.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1007/BF01150527
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  • 8
    Electronic Resource
    Electronic Resource
    Zur Reaktion des N.N′-Bis(trichlorphosphoranyliden)-sulfamids (1971)
    Weinheim : Wiley-Blackwell
    Berichte der deutschen chemischen Gesellschaft 104 (1971), S. 3804-3809 
    Details
    ISSN: 0009-2940
    Keywords: Chemistry ; Inorganic Chemistry
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology
    Description / Table of Contents: On the Reaction of N.N′-Bis(trichlorophosphoranylidene)sulfamideSO2(NPCl3)2 reacts with silylamines (CH3)3SiNR2 (R=CH3, C2H5) in a molar ratio of 1 : 2 to give 1 and 2, in a molar ratio of 1 : 4 to give 3. From 1 and disilylamines the cyclic compounds 6 and 7 can be obtained as a mixture of cis.trans-isomers. The reaction of SO2(NPCl3)2 with [(CH3)3Si]2 NC2H5 yields the heterocyclic compound 5.  -  The i.r., mass, 1H and 31P n.m.r. spectra of the above mentioned compounds are reported.
    Notes: SO2(NPCl3)2 reagiert mit Silylaminen (CH3)3SiNR2 (R=CH3, C2H5) im Moleverhältnis 1 : 2 zu 1 und 2, im Molverhältnis 1 : 4 zu 3. Aus 1 und Disilylaminen sind die cyclischen Verbindungen 6 und 7 als cis.trans-Isomerengemisch zugänglich. Schließlich konnte aus SO2(NPCl3)2 und [(CH3)3Si]2NC2H5 der Heterocyclus 5 gewonnen werden.  -  Die IR-, Massen- und 1H- bzw. 31P-NMR-Spektren dieser Verbindungen werden mitgeteilt.
    Additional Material: 2 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/cber.19711041210
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  • 9
    Electronic Resource
    Electronic Resource
    Reaktionen des 3,3-Dichlor-1,5,2,4,6,3-dithiatriazaphosphor(V)-in-S,S′-bis(oxidfluorids), eines cyclischen Phosphornitrilsulfanurhalogenids (1974)
    Weinheim : Wiley-Blackwell
    Berichte der deutschen chemischen Gesellschaft 107 (1974), S. 592-597 
    Details
    ISSN: 0009-2940
    Keywords: Chemistry ; Inorganic Chemistry
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology
    Description / Table of Contents: Reactions of 3,3-Dichloro-1,5,2,4,6,3-dithiatriazaphosphor(V)in-S,S′-bis(oxide fluoride), of a Cyclic Phosphornitrilsulfanur Halogenide(NSOF)2NPCl2 reacts with ammonia in a molar ratio of 1:2 to give 1, with silylamines (CH3)3SiNHR (R=CH3, C2H5) in a molar ratio 1:1 to yield 2 and 3, and with (CH3)3SiNR2 (R=CH3, C2H5) to form 4 and 5. The reaction of (NSOF)2NPCl2 with disilylamines [(CH3)3Si]2NR (R=H, CH3, C2H5) yields the compounds 6, 7, and 8. The i.r., mass, 1H, 19F, and 31P n.m.r. spectra of the above mentioned compounds are reported.
    Notes: (NSOF)2NPCl21 reagiert mit Ammoniak im Molverhältnis 1:2 zu 1, mit Silylaminen (CH3)3SiNHR (R=CH3, C2H5) im Molverhältnis 1:1 zu 2 und 3, mit (CH3)3SiNR2 (R=CH3, C2H5) zu 4 und 5. Schließlich konnten aus (NSOF)2NPCl 2 und Disilylaminen [(CH3)3Si]2NR (R=H, CH3, C2H5) die Verbindungen 6, 7 und 8 isoliert werden. Die IR-, Massen- und 1H-, 19F-und 31P-NMR-Spektren dieser Verbindungen werden mitgeteilt.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/cber.19741070227
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  • 10
    Electronic Resource
    Electronic Resource
    Darstellung neuer [Bis(trimethylsilyl)amino]fluorsilane (1975)
    Weinheim : Wiley-Blackwell
    Berichte der deutschen chemischen Gesellschaft 108 (1975), S. 155-158 
    Details
    ISSN: 0009-2940
    Keywords: Chemistry ; Inorganic Chemistry
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology
    Description / Table of Contents: Preparation of New [Bis(trimethysilyl)amino]flourosilanesAlkyl- and phenyl-substituted silicon fluorides react with lithium or sodium bis(trimethylsilyl)-amide in a molar ratio 1:1 to give compounds like RSiF2N(SiR3)2 and R2SiFN(SiR3)2 (R=H, CH3, C2H5, CH2=CH, C6H5) (1-7). Spectral data of these compounds are reported.
    Notes: Alkyl- und phenylsubstituierte Siliciumfluoride reagieren mit Lithium- bzw. Natrium-bis(trimethylsilyl)amid im Molverhältnis 1:1 zu Verbindungen des Typs RSiF2N(SiR3)2 und R2SiFN(SiR3)2 (R=H, CH3, C2H5, CH2=CH, C6H5) (1-7), deren Spektren kurz diskutiert werden.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/cber.19751080119
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