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  • 1
    Electronic Resource
    Electronic Resource
    (Alkylthio)- bzw. (Arylthio)thiocarbonyl-thiocyanate und -isothiocyanate (1973)
    Weinheim : Wiley-Blackwell
    Berichte der deutschen chemischen Gesellschaft 106 (1973), S. 1487-1495 
    Details
    ISSN: 0009-2940
    Keywords: Chemistry ; Inorganic Chemistry
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology
    Description / Table of Contents: (Alkylthio)- or (Arylthio)thiocarbonyl Thiocyanates and IsothiocyanatesDithiocarbonic ester chlorides 1 afforded with NaSCN the thiocyanates of the title (2), which reacted with imines to give the compounds 3. The thiocyanates rearranged thermally with low yields to the isomeric isothiocyanates 5, which were characterized by the addition of amines, imines, and diphenylketene (6, 7, 10).
    Notes: Dithiokohlesäureester-chloride 1 ergaben mit NaSCN die Thiocyanate der überschrift (2), die mit Iminen zu den Verbindungen 3 reagierten. Thermische Umlagerung der Thiocyanate führte verlustreich zu den isomeren Senfölen 5, die durch Amin-, Imin- und Diphenylketen-Addukte (6, 7, 10) charakterisiert wurden.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/cber.19731060514
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  • 2
    Electronic Resource
    Electronic Resource
    Unerwartete und gezielte Synthese von 2-Alkyl(bzw.Aryl)thio-4λ4-[1,2,4]dithiazolo[1,5-b][1,2,4]dithiazolen (1976)
    Weinheim : Wiley-Blackwell
    Berichte der deutschen chemischen Gesellschaft 109 (1976), S. 3108-3114 
    Details
    ISSN: 0009-2940
    Keywords: Chemistry ; Inorganic Chemistry
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology
    Description / Table of Contents: Unexpected and Intended Synthesis of 2-Alkyl(Aryl)thio-4λ4-[1, 2,4]dithiazolo[1,2,4]-dithiazolesAlkyl(aryl)dichloromethyl disulfides (1) react with sodium thiocyanate to give to the title compounds 2, which were obtained also by alkylation and sulfuration of 5-formylamino-1,2,4-dithiazole-3-thione (3). Probably alkyl dithiocyanatomethyl disulfides (6), which could be isolated under other conditions, are intermediates of the first mentioned reaction.
    Notes: Aus dur Umsetzung einiger Alkyl(Aryl)-dichlormethyl-disulfide (1) mit Natriumthiocyanat einerseits, der Alkylierung und Schwefelung von 5-Formylamino-1,2,4-dithiazol-3-thion (3) andererseits wurden die Titelverbindungen 2 erhalten. Der erstgenannte Weg verläuft wahrscheinlich über Alkyl-dithiocyanatomethyl-disulfide (6), die unter anderen Bedingungen isolierbar sind.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/cber.19761090915
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