ISSN:
1572-8854
Keywords:
calix[4]arene
;
acetone
;
inclusion complex
Source:
Springer Online Journal Archives 1860-2000
Topics:
Geosciences
,
Physics
Notes:
Abstract Crystal structure of inclusion complex of 5, 17-di-t-butyl-26, 28-disubstituted calix[4]arene 3 with acetone, [(C54H58N2O6·CH3COCH3)·2CH3COCH3], was determined by X-ray crystallographic analysis. It possesses space group C2/c, with a = 26.277(8), b = 12.967(5), c = 20.355(4) Å, β = 124.845(14)°, and D calc = 1.173 mg/m3 for Z = 4. Crystal data indicate that action of one molecule of compound 3 upon three molecules of acetone forms a clathrate intermolecular inclusion complex.
Type of Medium:
Electronic Resource
URL:
http://dx.doi.org/10.1023/A:1009514026129
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