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  • Springer Nature  (64)
  • American Institute of Physics (AIP)  (34)
  • Springer  (27)
  • Nature Publishing Group  (8)
  • 1
    Electronic Resource
    Electronic Resource
    [S.l.] : American Institute of Physics (AIP)
    Review of Scientific Instruments 70 (1999), S. 1756-1760 
    ISSN: 1089-7623
    Source: AIP Digital Archive
    Topics: Physics , Electrical Engineering, Measurement and Control Technology
    Notes: We discuss practical aspects of Kelvin probe force microscopy (KFM) which are important to obtain stable images of the electric surface potential distribution at high spatial resolution (〈100 nm) and high potential sensitivity (〈1 mV) on conducting and nonconducting samples. We compare metal-coated and semiconducting tips with respect to their suitability for KFM. Components of the metal coating can become detached during scanning, introducing sudden offset jumps in the potential maps (typically up to 350 mV between adjacent scan lines). However, n-doped silicon tips show no substantial tip alterations and, therefore, provide a stable reference during the experiment (offset jumps typically up to 40 mV between adjacent scan lines). These semiconducting tips must be electrically connected via contact pads. We use InGa and colloidal silver pads which are easily applied to the substrate supporting the cantilever and have a low enough differential contact resistance (350 Ω and 2.2 kΩ, respectively). Furthermore, we introduce a simple procedure to fine tune the feedback which detects the electric surface potential and show how the basic KFM setup has to be modified to gain access to the necessary control signals. © 1999 American Institute of Physics.
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  • 2
    Electronic Resource
    Electronic Resource
    [S.l.] : American Institute of Physics (AIP)
    Journal of Applied Physics 77 (1995), S. 3725-3728 
    ISSN: 1089-7550
    Source: AIP Digital Archive
    Topics: Physics
    Notes: The article presents a study of the interaction of iron with a grain boundary in boron-doped multicrystalline silicon. The sample was intentionally contaminated with iron to a few 1014 cm−3 and investigated by the electron-beam-induced-current technique (measurement of minority-carrier diffusion length, quantitative imaging) in the temperature range 80–300 K. The measurements were carried out for two different states of iron in the sample: (i) iron paired with boron, i.e., as FeB, and (ii) iron as interstitial iron Fei. The differences between diffusion lengths for these two states were used to estimate the iron concentration. The analysis of the data revealed a pronounced iron profile around the grain boundary, indicating gettering of about 4×1011 iron atoms per cm2. The recombination velocity of the grain boundary is about 5×105 cm s−1 at 300 K and is not changed by the FeB destruction treatment. The temperature dependence of the iron-related diffusion length components is discussed and found to be in satisfactory agreement with what is expected from Shockley–Read–Hall theory. Further, the diffusion length analysis revealed also a strong recombination channel of unidentified origin. © 1995 American Institute of Physics.
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  • 3
    Electronic Resource
    Electronic Resource
    Woodbury, NY : American Institute of Physics (AIP)
    Applied Physics Letters 74 (1999), S. 2432-2434 
    ISSN: 1077-3118
    Source: AIP Digital Archive
    Topics: Physics
    Notes: We have investigated the microstructural accommodation of nonstoichiometry in (BaxSr1−x)Ti1+yO3+z thin films grown by chemical vapor deposition. Films with y=0.04 and y=0.15 were studied by high-spatial resolution electron energy-loss spectroscopy, revealing changes in chemistry and local atomic environment both at grain boundaries and within grains as a function of titanium content. We find that excess titanium in the samples with y=0.15 segregates to the grain boundaries in addition to being partially accommodated in the grain interior. © 1999 American Institute of Physics.
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  • 4
    Electronic Resource
    Electronic Resource
    [S.l.] : American Institute of Physics (AIP)
    Journal of Applied Physics 84 (1998), S. 1168-1173 
    ISSN: 1089-7550
    Source: AIP Digital Archive
    Topics: Physics
    Notes: The combination of atomic force microscopy and Kelvin probe technology is a powerful tool to obtain high-resolution maps of the surface potential distribution on conducting and nonconducting samples. However, resolution and contrast transfer of this method have not been fully understood, so far. To obtain a better quantitative understanding, we introduce a model which correlates the measured potential with the actual surface potential distribution, and we compare numerical simulations of the three-dimensional tip–specimen model with experimental data from test structures. The observed potential is a locally weighted average over all potentials present on the sample surface. The model allows us to calculate these weighting factors and, furthermore, leads to the conclusion that good resolution in potential maps is obtained by long and slender but slightly blunt tips on cantilevers of minimal width and surface area. © 1998 American Institute of Physics.
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  • 5
    Electronic Resource
    Electronic Resource
    [S.l.] : American Institute of Physics (AIP)
    Journal of Applied Physics 90 (2001), S. 3319-3324 
    ISSN: 1089-7550
    Source: AIP Digital Archive
    Topics: Physics
    Notes: High-resolution transmission electron microscopy (HRTEM), electron energy-loss spectroscopy (EELS), and electron diffraction were used to study the microstructure of epitaxial La0.5Sr0.5CoO3−∂ thin films grown on (001) oriented LaAlO3 substrates. Films were characterized before and after annealing treatments under different oxygen partial pressures. EELS shows that annealing reduces the valence state of cobalt due to loss of oxygen. HRTEM image simulations show that the superstructure contrast observed in HRTEM can be explained by shifts of cations in planes containing ordered oxygen vacancies. The as-deposited film showed weak, short-range ordering of oxygen vacancies within nanometer-sized domains. The annealed film showed long-range order and a strong anisotropy in ordering, with the oxygen-deficient planes aligned parallel to the film/substrate interface. We propose that the anisotropy in ordering is a mechanism of stress relief in these films. Implications of the observed microstructure on the oxygen transport and surface oxygen exchange properties are discussed. © 2001 American Institute of Physics.
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  • 6
    Electronic Resource
    Electronic Resource
    [S.l.] : American Institute of Physics (AIP)
    Journal of Applied Physics 87 (2000), S. 3526-3531 
    ISSN: 1089-7550
    Source: AIP Digital Archive
    Topics: Physics
    Notes: Epitaxial, perovskite Pb(Mg1/3Nb2/3)O3–PbTiO3 films were grown by metalorganic chemical vapor deposition under various deposition conditions and characterized by x-ray diffraction and transmission electron microscopy. Pyrochlore free films were obtained under all deposition conditions used in this study. Magnesium-rich growth conditions lead to the formation of a Mg-rich impurity phase in the films, embedded as coherent lamellae parallel to the growth direction. Depending on the growth conditions, a wide variation in the stoichiometry and volume fraction of this impurity phase was found between samples, whereas morphology and crystal structure were found to be very similar. © 2000 American Institute of Physics.
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  • 7
    Electronic Resource
    Electronic Resource
    Woodbury, NY : American Institute of Physics (AIP)
    Applied Physics Letters 66 (1995), S. 1261-1263 
    ISSN: 1077-3118
    Source: AIP Digital Archive
    Topics: Physics
    Notes: A new theoretical expression is derived for the internal quantum efficiency of solar cells homoepitaxially grown on highly doped monocrystalline substrates. This expression is used to characterize our thin-layer silicon cells grown by chemical vapor deposition. These cells reach a confirmed efficiency of 17.3% although the active layer thickness is only 48 μm. The internal quantum efficiency analysis demonstrates that the open circuit voltage is limited by carrier injection into the highly doped substrate. Carrier generation in the substrates accounts for 0.7% of the short circuit current. © 1995 American Institute of Physics.
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  • 8
    Electronic Resource
    Electronic Resource
    Woodbury, NY : American Institute of Physics (AIP)
    Applied Physics Letters 65 (1994), S. 564-566 
    ISSN: 1077-3118
    Source: AIP Digital Archive
    Topics: Physics
    Notes: High-resolution transmission electron microscopy (TEM) shows that MgO films, grown on (001) GaAs by magnetron sputtering, are single crystal with a cube-on-cube relationship with the substrate, even though they are separated from the substrate by an amorphous interlayer. Scanning TEM–energy dispersive x-ray and scanning TEM–electron energy loss spectroscopy analysis of the interlayer shows that it consists of the native oxide of GaAs as well as nanocrystalline MgO. It is proposed that epitaxial MgO nucleated at pin holes produced by volatilization of the native oxide.
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  • 9
    Electronic Resource
    Electronic Resource
    Woodbury, NY : American Institute of Physics (AIP)
    Applied Physics Letters 68 (1996), S. 2678-2680 
    ISSN: 1077-3118
    Source: AIP Digital Archive
    Topics: Physics
    Notes: Lattice defects in GaN epilayers grown on 6H–SiC(0001) by metalorganic vapor phase epitaxy (MOVPE) have been characterized by transmission electron microscopy (TEM). The predominant defects in the film were threading dislocations and half-loops with Burgers vectors 1/3〈112¯0〉, [0001], and 1/3〈112¯3〉. Planar faults were also observed in the film that are thought to be inversion domain boundaries (IDBs). © 1996 American Institute of Physics.
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  • 10
    Electronic Resource
    Electronic Resource
    Woodbury, NY : American Institute of Physics (AIP)
    Applied Physics Letters 81 (2002), S. 712-714 
    ISSN: 1077-3118
    Source: AIP Digital Archive
    Topics: Physics
    Notes: We use electron energy-loss spectroscopy in scanning transmission electron microscopy to investigate interfacial reactions of chemical vapor deposited Y2O3 films with the Si substrate and with in situ polycrystalline Si ("poly-Si") capping layers after postdeposition annealing. We find that in situ capping layers significantly reduce the formation of SiO2 at the interface with the substrate, but silicates form at the substrate and the capping layer interfaces. Predeposition nitridation of the Si surface can impede the reaction at the substrate interface, resulting in crystallization of Y2O3 in the film interior. Possible mechanisms of the silicate formation are discussed. © 2002 American Institute of Physics.
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