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  • Column liquid chromatography  (54)
  • Coleoptera  (46)
  • Springer  (100)
  • Annual Reviews
  • Springer Science + Business Media
  • 2000-2004  (2)
  • 1995-1999  (70)
  • 1980-1984  (28)
Collection
Keywords
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  • Springer  (100)
  • Annual Reviews
  • Springer Science + Business Media
Years
Year
  • 1
    Electronic Resource
    Electronic Resource
    Development of a universal Raman detector for microchromatography (1997)
    Springer
    Chromatographia 44 (1997), S. 257-262 
    Details
    ISSN: 1612-1112
    Keywords: Column liquid chromatography ; Microchromatography ; Raman spectroscopy ; Deuterated solvents
    Source: Springer Online Journal Archives 1860-2000
    Topics: Chemistry and Pharmacology
    Notes: Summary A detector for microchromatography in which Raman spectroscopy is used to identify the eluted species has been developed. The detector is designed to be applicable to a wide range of compounds without requiring the presence of a chromophore. Its use is illustrated in the analysis of nitro compounds on a 250 μm i.d. column. Raman spectra of each of the compounds could be identified as they passed the detector. The advatages of the use of fully deuterated solvents are demonstrated by the analysis of nitrobenzenes in methanol/water mobile phases. The detection limit for nitrobenzene using the Raman line at 1342 cm−1 was 75ng.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1007/BF02466391
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  • 2
    Electronic Resource
    Electronic Resource
    Physiology and costs of resistance to herbivory and disease in Brassica (1996)
    Springer
    Entomologia experimentalis et applicata 80 (1996), S. 231-237 
    Details
    ISSN: 1570-7458
    Keywords: Leptosphaeria maculans ; Peronospora parasitica ; fungal pathogens ; Phyllotreta cruciferae ; flea beetles ; Coleoptera ; Chrysomelidae ; Cruciferae ; chitinase ; myrosinase ; allocation costs ; plant defense mechanisms
    Source: Springer Online Journal Archives 1860-2000
    Topics: Biology
    Notes: Abstract We used artificial selection experiments to study genetic allocation costs and physiological mechanisms of resistance to herbivory and fungal disease. Genetic costs to resistance were present in some instances and absent in others. Genetic resistance to the fungal pathogen, Leptosphaeria maculans was cost-free, while resistance to Peronospora parasitica showed a negative genetic correlation between disease resistance and growth rate. Leptosphaeria resistant genotypes had 13% higher chitinase activity. Genetic increases in myrosinase activity were correlated with increased resistance to flea beetles (Phyllotreta cruciferae), but resulted in lower plant fecundity, presumably due to production costs of myrosinase. Genetic costs of resistance may maintain genetic variation in natural plant populations. These studies demonstrate the predictive and explanatory power of a functional approach to plant-herbivore and plant-pathogen interactions.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1007/BF00194764
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  • 3
    Electronic Resource
    Electronic Resource
    Ecdysteroids during pupal development of female Xyleborus ferrugineus (1981)
    Springer
    Entomologia experimentalis et applicata 30 (1981), S. 151-156 
    Details
    ISSN: 1570-7458
    Keywords: Xyleborus ferrugineus ; pupae ; ecdysteroids ; pharate adult ; radioimmunoassay ; Coleoptera ; Scolytidae
    Source: Springer Online Journal Archives 1860-2000
    Topics: Biology
    Description / Table of Contents: Zusammenfassung Der Ecdysteroidtiter weiblicher Puppen von Xyleborus ferrugineus (Fabr.) wurde geschätzt, indem ganze Tiere homogenisiert und radioimmunologisch untersucht wurden. Ein ausgeprägtes Maximum an Ecdysteroiden wurde bei 36 Stunden Puppenent-wicklung beobachtet (743 pg/mg Körpergewicht). Der Titer nahm ab auf 299 pg/mg im Pharatstadium und auf 193 pg/mg unmittelbar vor Schlüpfen der Adulten. Qualitative Studien mit HPLC ergaben in frischen Puppen ein Verhältnis von 3:1 Ecdyson zu 20-Hydrooxyecdyson. Pharatstadien enthielten vor allem 20-Hydrooxyecdyson. Das beobachtete einzige Maximum im Titer stimmt überein mit den Resultaten bei andern untersuchten Coleopteren.
    Notes: Abstract Ecdysteroid titers were estimated on the whole body homogenates of Xyleborus ferrugineus (Fabr.) female pupae during development by radioimmunoassay. A distinct peak of ecdysteroids was observed at 36-hr pupal development (743 pg/mg body wt). Titer declined to 299 pg/mg by the pharate adult stage and to 193 pg/mg body wt just before adult emergence. Qualitative studies by HPLC revealed a ratio of 3:1 ecdysone to 20-hydroxyecdysone in the initial pupal stage. Pharate adults had mainly 20-hydroxyecdysone. The observed single peak in ecdysteroid titer agrees with findings in other studied coleopteran species.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1007/BF00300880
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  • 4
    Electronic Resource
    Electronic Resource
    Geographic Variation in Response of Pine Engraver, Ips pini, and Associated Species to Pheromone, Lanierone (1997)
    Springer
    Journal of chemical ecology 23 (1997), S. 2013-2031 
    Details
    ISSN: 1573-1561
    Keywords: Ips pini ; Ips integer ; Coleoptera ; Scolytidae ; aggregation pheromone ; lanierone ; ipsdienol ; geographic variation ; synergism ; Enoclerus lecontei ; Cleridae ; kairomone
    Source: Springer Online Journal Archives 1860-2000
    Topics: Biology , Chemistry and Pharmacology
    Notes: Abstract Lanierone strongly synergized the attraction of male and female Ips pini (Say) to ipsdienol in New York and Wisconsin. Synergy was only weakly significant in Montana and British Columbia and not significant in California. Catches of I. pini in ipsdienol-baited traps were increased 0% ( i.e., nonsignificant) to 9942% by lanierone, with the highest increases in eastern North America. Lanierone had the least effect in California. The effects of lanierone on sex ratios of I. pini in trap catches varied significantly between regions. The addition of lanierone to ipsdienol-baited traps resulted in a general increase in male representation at nine of 12 sites. Ips integer (Eichhoff) was attracted to lanierone alone. Ipsdienol reduced the response of I. integer to lanierone. Enoclerus lecontei (Wolcott) (Cleridae) preferred traps baited with the combination of ipsdienol and lanierone. (R)-(–)-Ipsdienol was attractive to E. sphegeus (F.), Thanasimus undatulus (Say) (Cleridae), and Temnochila chlorodia (Mannerheim) (Trogositidae), while racemic ipsdienol was attractive to E. nigrifrons var. gerhardi Wolc. and Thanasimus dubius (F.). Lanierone had no effect on these species.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1023/B:JOEC.0000006486.39056.48
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  • 5
    Electronic Resource
    Electronic Resource
    Defensive adaptations of eggs and adults ofGastrophysa cyanea (Coleoptera: Chrysomelidae) (1982)
    Springer
    Journal of chemical ecology 8 (1982), S. 453-462 
    Details
    ISSN: 1573-1561
    Keywords: Defensive secretions ; oleic acid ; hydrocarbons ; terpenoids ; eggs ; deterrents ; ants ; predation ; Chrysomelidae ; Coleoptera ; Gastrophysa cyanea ; reflex bleeding ; elytral glands
    Source: Springer Online Journal Archives 1860-2000
    Topics: Biology , Chemistry and Pharmacology
    Notes: Abstract Egg clusters and adults ofGastrophysa cyanea are conspicuous and, like their larvae, are chemically protected. The eggs owe their bright yellow color primarily to β-carotene and, in addition, contain substantial quantities of oleic acid. At natural concentrations oleic acid effectively deters many species of ants from feeding. The use of fatty acids as deterrents against ants is discussed as a possible widespread phenomenon among insects. During defensive confrontations, adults ofG. cyanea exhibit avoidance behavior and may also feign death. In addition, the adults may autohemmorhage or secrete a fluid from elytral or pronotal pores in response to traumatic stimuli. The secretions are effective against ants and contain a mixture of hydrocarbons as well as terpenoid components. The pattern of ontogenetic modification in the defensive chemical repertoire ofG. cyanea is discussed.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1007/BF00987793
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  • 6
    Electronic Resource
    Electronic Resource
    Retention behavior of morphine and its metabolites on a porous graphitic carbon column (1998)
    Springer
    Chromatographia 47 (1998), S. 667-672 
    Details
    ISSN: 1612-1112
    Keywords: Column liquid chromatography ; Porous graphitic carbon ; Optimization ; Morphine and metabolites
    Source: Springer Online Journal Archives 1860-2000
    Topics: Chemistry and Pharmacology
    Notes: Summary The chromatographic behaviour of a series of morphine-based opiates has been investigated using a porous graphitic carbon packing material at acid and alkaline pH. The effects of mobile phase pH, mobile phase organic percentage, column temperature and ionpairing agents were studied. All six opiates were separated within a close retention window despite large differences in measured lipophilicities of the individual opiates. The retention order was not related to the log P values of the opiates and strong retention of the fully ionised compounds was observed, particularly those with acidic functional groups. The effect of pH on the retention of the compounds indicated that the degree of ionisation of the individual compounds was important in the separation mechanism, suggesting that hydrophobic interactions were present in addition to the polar retentive effects observed above. The strong retention of the ionised glucuronide and sulphate conjugates of morphine is a particularly useful feature of the porous graphitic carbon packing material which has general applicability to the analysis of polar or ionised drug metabolites.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1007/BF02467451
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  • 7
    Electronic Resource
    Electronic Resource
    Simultaneous determination of triprolidine, pseudoephedrine, paracetamol and dextromethorphan by HPLC (1996)
    Springer
    Chromatographia 43 (1996), S. 496-500 
    Details
    ISSN: 1612-1112
    Keywords: Column liquid chromatography ; Pharmaceutical formulations ; Triprolidine ; Pseudoephedrine ; Paracetamol ; Dextromethorphan
    Source: Springer Online Journal Archives 1860-2000
    Topics: Chemistry and Pharmacology
    Notes: Summary A simple, rapid and specific HPLC method has been developed for the determination of triprolidine, pseudoephedrine, paracetamol and dextromethorphan, in combination, in different pharmaceutical dosage forms, using a reversed-phase C18 column, gradient elution, and UV detection at 254 and 280 nm. No preliminary extraction procedure is required for liquid formulations and a very simple extraction procedure is required for tablets and creams. The recovery of the drugs ranged from 96.0 to 98.7%. The assay results obtained for eight commercially available formulations were in agreement with the amounts declared. The linearity and precision of the method have been assessed.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1007/BF02293000
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  • 8
    Electronic Resource
    Electronic Resource
    HPLC analysis of boldine in pharmaceuticals (1997)
    Springer
    Chromatographia 44 (1997), S. 619-622 
    Details
    ISSN: 1612-1112
    Keywords: Column liquid chromatography ; Boldine in pharmaceuticals
    Source: Springer Online Journal Archives 1860-2000
    Topics: Chemistry and Pharmacology
    Notes: Summary A method is proposed for extraction, separation, identification and quantitative measurement of boldine (I) in pharmaceuticals. The extraction of (I) from the matrix (syrups, tablets, extracts) was realized with aqueous ammonium chloride (0.02 M, pH=3.0 with perchloric acid) and the clean-up of the extract was performed by solid-phase extraction by means of cartridges containing a strong cation-exchange sorbent, from which (I) was eluted with aqueous ammonium chloride (1 M, pH=10.0 with ammonia). The final eluate was examined by HPLC. Chromatography was performed on a C-8 column with a gradient elution from 15:85 to 30:70 of acetonitrile-water containing 0.1 M sodium perchlorate (pH=3.0), in 20 min. A diode array detector was used at 302 nm for detection. The method gives recovery values greater than 98% and the reproducibility is within 6.0%.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1007/BF02466665
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  • 9
    Electronic Resource
    Electronic Resource
    Optimisation and validation of an automated solid phase extraction technique coupled on-line to enzyme-based biosensor detection for the determination of phenolic compounds in surface water samples (1995)
    Springer
    Chromatographia 41 (1995), S. 207-215 
    Details
    ISSN: 1612-1112
    Keywords: Column liquid chromatography ; Solid phase extraction ; Enzyme-based biosensor detection ; Tyrosinase ; Phenols
    Source: Springer Online Journal Archives 1860-2000
    Topics: Chemistry and Pharmacology
    Notes: Summary A fully integrated screening system for phenolic compounds was developed incorporating on-line solid phase extraction, fractionation and biosensor detection. Two different types of biosensors, solid graphite and carbon paste electrodes incorporating the enzyme tyrosinase, were compared and used in the screening system. Interfacing of the solid phase extraction and fractionation with the biosensor detection was given special attention since the biosensors were not compatible with the organic modifier used for desorption of phenols from the solid phase extraction step. The system was validated with conventional analytical techniques. Surface water samples from the Ebro river were spiked with 1,10, and 25μg L−1 of catechol, phenol,p-cresol, respectively. Three out of seven samples were spiked and the correct samples were identified, containing phenols equivalent to the spiked concentrations.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1007/BF02267957
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  • 10
    Electronic Resource
    Electronic Resource
    HPLC determination of rhodamine B (C.I. 45170) in cosmetic products (1996)
    Springer
    Chromatographia 43 (1996), S. 76-78 
    Details
    ISSN: 1612-1112
    Keywords: Column liquid chromatography ; Rhodamine B in cosmetics
    Source: Springer Online Journal Archives 1860-2000
    Topics: Chemistry and Pharmacology
    Notes: Summary A method is proposed for the extraction, separation, identification and quantitative measurement of rhodamine B in cosmetics samples The colour is extracted with a solution of orthophosphoric acid in either water or DMF (depending on the type of cosmetic) adsorbed on a polyamide column, and then eluted with water and methanol. Further clean-up of the extract is performed by means of a Bond Elut C-18 cartridge, from which rhodamine B is eluted with methanol-water (8∶2). The final eluate is examined by HPLC. Chromatography is performed on a C-18 column with a gradient elution from 50∶50 to 70∶30 of acetonitrile-water, containing 0.1 M sodium perchlorate, in 15 min. A diodearray detector enables peak purity analysis. The method gives recovery values of approximately 90%, or better, and the reproducibility is within 4%.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1007/BF02272825
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