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  • Polymer and Materials Science  (207)
  • FLUID MECHANICS AND HEAT TRANSFER
  • 1980-1984  (239)
  • 1981  (239)
  • 1
    Electronic Resource
    Electronic Resource
    Kinetics of epoxy resin synthesis on the basis of GPC measurements (1981)
    New York, NY [u.a.] : Wiley-Blackwell
    Journal of Applied Polymer Science 26 (1981), S. 2783-2786 
    Details
    ISSN: 0021-8995
    Keywords: Chemistry ; Polymer and Materials Science
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology , Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics , Physics
    Additional Material: 2 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/app.1981.070260827
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  • 2
    Electronic Resource
    Electronic Resource
    Storage hardening and “abnormal” groups in guayule rubberThis article was presented at the 27th IUPAC Congress, Helsinki, Finland, August 1979. (1981)
    New York, NY [u.a.] : Wiley-Blackwell
    Journal of Applied Polymer Science 26 (1981), S. 1511-1517 
    Details
    ISSN: 0021-8995
    Keywords: Chemistry ; Polymer and Materials Science
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology , Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics , Physics
    Notes: The hardening process of natural (Hevea brasiliensis) rubber, that takes place when this rubber is stored in dry conditions over long periods of time, has been correlated with the presence of reactive “abnormal” groups directly grafted on the polymeric chain and in the serum of the latex. In the present work, natural Hevea (HR) and Guayule (Parthenium argentatum) rubber (GR) were stored under accelerated conditions and the changes in Mooney viscosity and molecular weight measured. The results showed that while HR undergoes hardening, GR keeps its Mooney viscosity constant, as does a constant viscosity (CV) Hevea rubber. These results are explained by the absence of functional “abnormal” groups that sustain the hardening reactions.
    Additional Material: 4 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/app.1981.070260508
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  • 3
    Electronic Resource
    Electronic Resource
    Untersuchungen zur Belastbarkeit von Polybutylenterephthalat (1981)
    Weinheim : Wiley-Blackwell
    Acta Polymerica 32 (1981), S. 465-466 
    Details
    ISSN: 0323-7648
    Keywords: Chemistry ; Polymer and Materials Science
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology , Physics
    Description / Table of Contents: The deformation stability of polybutylene terephthalate in dependence on stress and temperature was determined. The lifetime of the polymer is described as a function of these parameters. The results are compared with the values obtained with other polymers.
    Notes: Die Deformationsstabilität von Polybutylenterephthalat wurde in Abhängigkeit von der Spannung und der Temperatur bestimmt. Die Lebensdauer des Polymers kann als eine Funktion dieser Parameter angegeben werden. Die Ergebnisse werden mit den an anderen Polymeren erhaltenen Werten verglichen.
    Additional Material: 4 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/actp.1981.010320806
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  • 4
    Electronic Resource
    Electronic Resource
    Thermodynamics and equilibrium sedimentation analysis of the close approach of DNA molecules and a molecular ordering transition (1981)
    New York : Wiley-Blackwell
    Biopolymers 20 (1981), S. 1305-1328 
    Details
    ISSN: 0006-3525
    Keywords: Chemistry ; Polymer and Materials Science
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology
    Notes: Measurement of the equilibrium distribution of persistence length fragments of DNA in high concentration in the ultracentrifuge shows that the reduced osmotic pressure rises much faster than linearly. From analysis of the data in terms of the Zimm cluster integral we infer that the net interactions between helices are purely repulsive at all distances. A theoretical equation of state derived from scaled particle theory with one adjustable parameter is in excellent agreement with the experimental data so long as the salt concentration is not excessively low. The parameter represents the hard-core radius in a simplified approximation to the potential function for the electrostatic repulsion between helices. Its value depends on the salt concentration, and it shrinks at high salt to a radius in close agreement with direct structural estimates. At a particular value of the osmotic pressure that is only slightly salt dependent, the solution undergoes a reversible transition to a denser, turbid, optically anisotropic phase. The relation between DNA volume fraction, including the electrostatic radius, at the transition point and the effective asymmetry of the molecules as a function of salt is in approximate correspondence with various theoretical treatments. However, the experimental function extrapolates to the correct limit for spherical particles. The work needed to bring DNA to a high concentration is estimated. The results suggest that the phase transition is first order.
    Additional Material: 7 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/bip.1981.360200615
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  • 5
    Electronic Resource
    Electronic Resource
    Calculated microwave absorption of double-helical B-conformation poly(dG)·poly(dC) (1981)
    New York : Wiley-Blackwell
    Biopolymers 20 (1981), S. 853-864 
    Details
    ISSN: 0006-3525
    Keywords: Chemistry ; Polymer and Materials Science
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology
    Notes: We have estimated the absorption of microwave radiation by the four acoustic modes of poly(dG)·poly(dC) in B conformation. The eigenvectors used in this calculation are those obtained from a refined normal coordinate analysis by fitting the velocity of the longitudinal acoustic mode to that observed by Brillouin scattering. The acoustic modes couple to the radiation field when translational invariance is broken such as for finite segments of helix and as may be the case in vivo. Calculations for various helix lengths show that the estimated absorption is greater than that of water by at least two to three orders of magnitude in some cases.
    Additional Material: 5 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/bip.1981.360200415
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  • 6
    Electronic Resource
    Electronic Resource
    Analysis of the ionization constants and heats of ionization of reduced and oxidized horse heart cytochrome c (1981)
    New York : Wiley-Blackwell
    Biopolymers 20 (1981), S. 2253-2261 
    Details
    ISSN: 0006-3525
    Keywords: Chemistry ; Polymer and Materials Science
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology
    Notes: Simultaneous curve fitting for the ionization parameters of oxidized and reduced horse heart cytochrome c in 0.15M KCl and 20°C yields values for the ionization constants (as pK′) and the heats of ionization (ΔHi) which can reconstruct either the potentiometric or thermal titration curves. Reduced cytochrome c requires 8 sets of groups, whereas oxidized cytochrome c requires 10 sets of groups. The additional groups in the oxidized preparation appear to involve the ferriheme (pK′, 9.25; ΔHi, 13.7 kcal/mol) and a tyrosine (pK′ ≃ 10.24) that is not present in the reduced form. The potentiometric and thermal difference curves (reduced - oxidized) involve the appearance of 17 kcal/mol centered at pH 9.7 and 5.8 kcal/mol centered at pH 4.9. The carboxyl groups in both species appear to be normal for the hydrogen-bonded form. Only one histidine has normal ionization properties (pK′, 6.7; ΔHi, 7.5 kcal/mol), as do 17 of the lysine residues (pK′, 10.8; ΔHi, 11.5 kcal/mol).
    Additional Material: 4 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/bip.1981.360201017
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  • 7
    Electronic Resource
    Electronic Resource
    Acoustic modes and nonbonded interactions of the double helix (1981)
    New York : Wiley-Blackwell
    Biopolymers 20 (1981), S. 833-852 
    Details
    ISSN: 0006-3525
    Keywords: Chemistry ; Polymer and Materials Science
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology
    Notes: Observations of acoustic velocities in DNA fibers have been used to refine nonbonded force constants for the DNA double helix. Long-range forces are found to be needed for A conformation and are likely to dominate in B conformation as well. The acoustic dispersion curves are described and calculated. A correction due to the effects of water is calculated. The effect of nonbonded interaction on other vibrational modes is calculated.
    Additional Material: 8 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/bip.1981.360200414
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  • 8
    Electronic Resource
    Electronic Resource
    Model networks of end-linked polydimethylsiloxane chains. XII. Dependence of ultimate properties on dangling-chain irregularities (1981)
    New York, NY [u.a.] : Wiley-Blackwell
    Journal of Applied Polymer Science 26 (1981), S. 1829-1836 
    Details
    ISSN: 0021-8995
    Keywords: Chemistry ; Polymer and Materials Science
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology , Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics , Physics
    Notes: Elastomeric networks were prepared by end-linking vinyl-terminated polydimethylsiloxane (PDMS) chains having number-average molecular weights of 11.3 × 103 g mol-1. The tetra-functional end-linking agent, Si[OSi(CH3)2H]4, was used in varying amounts smaller than that corresponding to a stoichiometric balance between its active hydrogen atoms and the chain vinyl groups. The number of dangling-chain irregularities thus introduced into the networks was directly determined by iodometric titration for unreacted vinyl groups. The (unfilled) PDMS networks thus obtained were studied in elongation to their rupture points at 25°C (a temperature sufficiently high to prevent complications from strain-induced crystallization), and in swelling equilibrium in benzene at room temperature. Small to moderately large proportions of dangling chains were found to have less of an effect on the elongation modulus than might be expected, and similarly a relatively small effect on the degree of equilibrium swelling. Most importantly, comparisons of constant values of the high deformation modulus show that dangling-chain irregularities decrease both the maximum extensibility of a network and its ultimate strength.
    Additional Material: 5 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/app.1981.070260608
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  • 9
    Electronic Resource
    Electronic Resource
    Dimensional stability and tensile properties of drawn polystyrene composites (1981)
    New York, NY [u.a.] : Wiley-Blackwell
    Journal of Applied Polymer Science 26 (1981), S. 129-139 
    Details
    ISSN: 0021-8995
    Keywords: Chemistry ; Polymer and Materials Science
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology , Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics , Physics
    Notes: Recovery experiments above Tg and tensile tests have been performed on glass bead and short glass fiber-polystyrene composite sheets obtained from extrusion and subsequent hot drawing. A shift procedure has been applied to the recoil data using a WLF equation. The data reported show that both dimensional stability and mechanical properties are enhanced by adding rigid fillers to the drawn thermoplastic matrix. The presence of short fibers reduces strongly the recoverable strain of the oriented material. A simple model able to predict the equilibrium values of the length reversion ratio of glass bead composites is developed and compares well with the experimental data.
    Additional Material: 10 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/app.1981.070260111
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  • 10
    Electronic Resource
    Electronic Resource
    Interpenetrating polymer networks based on ionically crosslinked polymers: Reacidification and annealing as morphological variables (1981)
    New York, NY [u.a.] : Wiley-Blackwell
    Journal of Applied Polymer Science 26 (1981), S. 141-147 
    Details
    ISSN: 0021-8995
    Keywords: Chemistry ; Polymer and Materials Science
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology , Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics , Physics
    Notes: A carboxylic elastomer based on butadiene, styrene, and methacrylic acid was polymerized and neutralized to form an ionomeric network I. Sequential IPNs were formed by synthesizing in situ polystyrene crosslinked with divinylbenzene as network II. Annealing studies were carried out, with and without reacidification, to ascertain the role played by ionic crosslinks in influencing morphology and mechanical behavior. Finally, the product is reneutralized, resulting in are arranged, relaxed structure. Ionic crosslinks in polymer I provide an in situ decrosslinking mechanism which permits molecular rearrangements to be induced. By annealing the material, a more cocontinuous phase morphology with concomitant modulus increases is attained. This investigation suggests an alternative method of inducing dual phase continuity in multipolymer combinations.
    Additional Material: 4 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/app.1981.070260112
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