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  • 11
    Electronic Resource
    Electronic Resource
    Blends of biodegradable polyesters by reactive blending: preparation, characterisation and properties (1999)
    Springer
    Journal of materials science 34 (1999), S. 1625-1639 
    Details
    ISSN: 1573-4803
    Source: Springer Online Journal Archives 1860-2000
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics
    Notes: Abstract Blends of poly-ε-caproIactone (PCL) and poly-β-hydroxybutyrate (PHB) were prepared by mixing the two polymers in the presence of dicumylperoxide (DCPO) in solution of chlorobenzene. Similarly blends were obtained by mixing the two polymers with no peroxide added. The blends were prepared in a break of composition, from 85% wt PHB/15% wt PCL to 15% wt PHB/85% wt PCL, respectively. Also pure polymers were reacted with DCPO in the same way of the blends. Thermal (DSC), spectroscopic, mechanical (tensile tests) and morphological SEM)analyses were performed on the blends and on the pure polymers. Significant differences were found in the chemical-physical characteristics of the blends with and without peroxide.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1023/A:1004584802030
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  • 12
    Electronic Resource
    Electronic Resource
    Impact behaviour and fractographic analysis of rubber-modified polybutyleneterephthalate obtained by reactive blending concurrently with polymerization process (1990)
    Weinheim : Wiley-Blackwell
    Angewandte Makromolekulare Chemie 174 (1990), S. 141-150 
    Details
    ISSN: 0003-3146
    Keywords: Chemistry ; Polymer and Materials Science
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology , Physics
    Description / Table of Contents: Die Modifizierung von Polybutylenterephthalat mit Gummi wurde durch Zugabe geeignet funktionalisierter Copolymerer aus Ethylen und Propylen (EPR) und gleichzeitiger Hochtemperaturpolykondensation von 1,4-Butandiol mit Dimethylterephthalat erreicht. Die Schlagzähigkeit der Blends, die reines oder mit Ester- oder Hydroxylgruppen modifiziertes EPR enthielten, wurde mit Hilfe von Schlagbiegeversuchen nach Charpy bei verschiedenen Temperaturen bestimmt. Die morphologischen Merkmale der Bruchflächen wurden auch untersucht. Es wurde ein Versuch unternommen, die Morphologie dieser Flächen mit den Bruchanalysenergebnissen zu korrelieren.
    Notes: Rubber modification of polybutyleneterephthalate was accomplished by the addition of suitable functionalized ethylene-propylene copolymers (EPR) concurrently with the high temperature polycondensation of 1,4-butanediol and dimethylterephthalate.The impact properties of blends obtained with plain EPR, with ester or hydroxyl groups modified EPR were analyzed by Charpy tests performed at different temperatures with a Ceast fracture pendulum. The morphological features of fracture surfaces have also been investigated. An attempt has been made to correlate the morphology of the surfaces with the fracture analysis results.
    Additional Material: 2 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/apmc.1990.051740112
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  • 13
    Electronic Resource
    Electronic Resource
    Poly-ε-caprolactone/poly(Methylmethacrylate) reactive blends: Correlation between synthesis, morphology and physical properties (1993)
    Weinheim : Wiley-Blackwell
    Angewandte Makromolekulare Chemie 210 (1993), S. 47-59 
    Details
    ISSN: 0003-3146
    Keywords: Chemistry ; Polymer and Materials Science
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology , Physics
    Description / Table of Contents: Blends aus Poly-ε-caprolacton (PCL) und Polymethylmethacrylat (PMMA) wurden durch Polymerisation von Methylmethacrylat in Gegenwart von PCL hergestellt. Die thermeischen, morphologischen, dynamisch-mechanischen und mechanischen Eigenschaften der Blends wurden ermittelt. Zum Vergleich wurden Blends durch mechanisches Mischen von PCL-und PMMA-Homopolymerschmelzen hergestellt und charakterisiert. Die nach beidenMethoden hergestellten Blends unterscheiden sich wesentlich in der phasenstrukturund den mechanischen eigenschafte, was wahrscheinlich auf die bildung von gepfropften Anteilen bei der erstgenannten Methode zuräuckgefäuhrt werden kann.
    Notes: Blends of poly-ε-caprolactone (PCL) and poly(methylmethacrylate) (PMMA) were prepared by a reactive method and characterized by thermal, morphological, dynamic mechanical and mechanical analyses. For comparison, “mechanical” blends, obtained by melt-mixing of preformed polymers, have been prepared and characterized. The two series of blends are different in phase structure and in mechanical tensile properties, probably due to the formation of grafted species during reactive blending.
    Additional Material: 9 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/apmc.1993.052100105
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  • 14
    Electronic Resource
    Electronic Resource
    Blends of polyamide 6 and poly(etheraroylhydrazide)s prepared concurrently with polyhydrazide polymerization (1994)
    Weinheim : Wiley-Blackwell
    Angewandte Makromolekulare Chemie 214 (1994), S. 101-113 
    Details
    ISSN: 0003-3146
    Keywords: Chemistry ; Polymer and Materials Science
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology , Physics
    Description / Table of Contents: Polyhydrazid/Polyamid-Blends (PEHZ12/PA6) wurden durch Niedrigtemperatur-Polykondensation von 4,4′-Dichlorformyl-α,ω-diphenoxydodecan und Terephthaloyldihydrazid (TDH) zu Poly(etheraroylhydrazid) in Gegenwart von Polyamid 6 synthetisiert. Die DSC-Analysen lassen vermuten, daß die zwei Polymerkomponenten nicht wechselwirken. Bei der Extraktion des PA6-Anteils der Blends mit Ameisensäure zeigt die Charakterisierung des PEHZ12-Extraktionsrückstands aber, daß zumindest bei bestimmten Zusammensetzungen Wechselwirkungen zwischen den Komponenten auftreten. Modellreaktionen erlauben die Annahme, daß die PEHZ12-Polymerisation zwischen den Amino-Endgruppen des PA6 und den wachsenden PEHZ12-Polymerketten abläuft.
    Notes: Poly(etheraroylhydrazide) is synthesized in the presence of PA6 by means of low-temperature condensation polymerization of 4,4′-dichloroformyl-α,ω-diphenoxydodecane with terephthaloyl dihydrazide (TDH) in order to prepare polyhydrazide/poly-amide 6 (PEHZ12/PA6) blends. The thermal analysis of the blends by DSC seems to indicate that the two polymers are not interacting. Nevertheless, when the blends are subjected to an extraction process with formic acid in order to remove the PA6, the characterization of the residual PEHZ12 reveales that some interactions do occur between the constituent polymers, at least for selected compositions. Model experiments permit to hypothesize that the polymerization of PEHZ12 proceeds with a chemical interaction between amino end groups of PA6 and growing PEHZ12 chains.
    Additional Material: 7 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/apmc.1994.052140110
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  • 15
    Electronic Resource
    Electronic Resource
    Thermal and structural analysis and crystallization behavior of new poly(ether-alkyl) oxadiazoles (1994)
    Bognor Regis [u.a.] : Wiley-Blackwell
    Journal of Polymer Science Part B: Polymer Physics 32 (1994), S. 1643-1651 
    Details
    ISSN: 0887-6266
    Keywords: polyoxadiazoles ; structural analysis ; cristallinity behavior ; cyclodehydration reaction ; Chemistry ; Polymer and Materials Science
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology , Physics
    Notes: A new series of poly(ether-alkyl)oxadiazoles of general formula: with m = 3, 4, and 5 has been obtained from the corresponding polyhydrazides through thermal cyclization reaction. The polymers were characterized by infrared spectroscopy, differential scanning calorimetry, wide-angle x-ray analysis, and optical microscopy. The polymers were crystalline, with a crystalline texture and structural parameters strongly dependent on the value of m. The Tm's and Tg's value decreased with increasing number of CH2. © 1994 John Wiley & Sons, Inc.
    Additional Material: 12 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/polb.1994.090320907
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  • 16
    Electronic Resource
    Electronic Resource
    Synthesis and structure-property relationships of a new class of rubber-toughened PMMA (1992)
    New York, NY [u.a.] : Wiley-Blackwell
    Journal of Applied Polymer Science 44 (1992), S. 1883-1892 
    Details
    ISSN: 0021-8995
    Keywords: Chemistry ; Polymer and Materials Science
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology , Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics , Physics
    Notes: In the present work, blends between poly(methyl methacrylate) (PMMA) and poly(ethylene-co-vinyl acetate) (EVA) rubbers obtained by in situ polymerization of the acrylic monomer in the presence of the rubber have been investigated by linear elastic fracture mechanics (LEFM), by Charpy impact tests, and by scanning electron microscopy (SEM). Particularly, a correlation among molecular weight and composition of the EVA rubbers, phase structure development, and, consequently, mechanical impact properties of the resulting blends has been drawn.
    Additional Material: 13 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/app.1992.070441102
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  • 17
    Electronic Resource
    Electronic Resource
    A new class of aromatic polyetheraroylhydrazides. I. Synthesis and chemical-physical characterization (1993)
    Bognor Regis [u.a.] : Wiley-Blackwell
    Journal of Polymer Science Part A: Polymer Chemistry 31 (1993), S. 2415-2415 
    Details
    ISSN: 0887-624X
    Keywords: Chemistry ; Polymer and Materials Science
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/pola.1993.080310931
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  • 18
    Electronic Resource
    Electronic Resource
    A new class of aromatic polyetheraroylhydrazides. I. Synthesis and chemical-physical characterization (1993)
    Bognor Regis [u.a.] : Wiley-Blackwell
    Journal of Polymer Science Part A: Polymer Chemistry 31 (1993), S. 1315-1322 
    Details
    ISSN: 0887-624X
    Keywords: aromatic polyhydrazides ; heat-resistant polymers ; synthesis ; thermal analysis ; structure ; Chemistry ; Polymer and Materials Science
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology
    Notes: A series of new aromatic polyetheraroylhydrazides incorporating 4-oxybenzoyl units has been synthesized, whose general formula was [CONHNHCO—O—O-(CH2)x—O—phenyl O-CONHNHCOO]n with x values in the range of 2 to 12. The increasing number of methylene units in the backbone gave rise to polymers which melted before the hydrazidic linkage underwent thermal cyclation to oxadiazole. Moreover, many polymers showed multiple endotherms on melting. X-ray diffraction studies confirmed a crystalline organization of polyhydrazides for methylene units above 4. © 1993 John Wiley & Sons, Inc.
    Additional Material: 12 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/pola.1993.080310527
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  • 19
    Electronic Resource
    Electronic Resource
    A new class of aromatic poly-ether-aroyl-oxadiazoles. II. Studies on the cyclization reaction, infrared, structural, and morphological characterization (1994)
    Bognor Regis [u.a.] : Wiley-Blackwell
    Journal of Polymer Science Part B: Polymer Physics 32 (1994), S. 1249-1256 
    Details
    ISSN: 0887-6266
    Keywords: polyoxadiazoles ; IR ; structure ; morphology ; Chemistry ; Polymer and Materials Science
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology , Physics
    Notes: Poly-ether-aroyl-oxadiazoles (PEODZ) of general formula: are reported.Thermal cyclization of the starting polyhydrazides, infrared, thermal, and structural characterization are discussed as function of the number of methylene spacers in the range 2-12.It is found that the position of melting is strongly dependent upon the number of—CH2—, and that moldable polyoxadiazoles are obtained at × values 〉 7. The spherulitic nature of PEODZ is clearly revealed by thermal-optical microscopy which, together with isothermal crystallizations at the differential scanning calorimeter, gives a close insight into the crystalline organization of such polymers. © 1994 John Wiley & Sons, Inc.
    Additional Material: 9 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/polb.1994.090320712
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  • 20
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    Phase transition kinetics in the case of nonrandom nucleation (2002)
    American Physical Society
    Details
    Publication Date: 2002-03-28
    Print ISSN: 0163-1829
    Electronic ISSN: 1095-3795
    Topics: Physics
    Published by American Physical Society
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