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Accurate Measurement of Heat Capacity by Differential Scanning Calorimetry (1984)

In: CASI

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Publication Date: 2014-09-16

Description: Experience with high quality heat capacity measurement by differential scanning calorimetry is summarized and illustrated, pointing out three major causes of error: (1) incompatible thermal histories of the sample, reference and blank runs; (2) unstable initial and final isotherms; (3) incompatible differences between initial and final isotherm amplitudes for sample, reference and blank runs. Considering these problems, it is shown for the case of polyoxymethylene that accuracies in heat capacity of 0.1 percent may be possible.

Keywords: COMPOSITE MATERIALS

Type: Composite Struct. Mater.; p 127-145

Format: text

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