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Crystallization and preliminary X-ray analysis of two new crystal forms of calmodulin (1996)

Rupp, B. ; Marshak, D. R. ; Parkin, S.

Copenhagen : International Union of Crystallography (IUCr)

Acta crystallographica 52 (1996), S. 411-413

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ISSN: 1399-0047

Source: Crystallography Journals Online : IUCR Backfile Archive 1948-2001

Topics: Chemistry and Pharmacology , Geosciences , Physics

Notes: Two new crystal forms of calmodulin from Gallus gallus are reported. Crystals in space group P1 (cell dimensions a = 59.7, b = 53.1, c = 24.6 Å, α = 93.2, β = 96.7, γ = 89.2 and Z = 2), grow as long thin needles. Water content on density considerations is \sim50%. They diffract to \sim2.0 Å but give wide multiply peaked spot profiles. Crystals in space group P212121 (cell dimensions a = 32.2, b = 56.0, c = 67.3 Å and Z = 4), grow as clusters of thin tablets and contain \sim30% water by volume. These small crystals (\sim0.4 × 0.15 × 0.1 mm) diffracted well to \sim 1.4 Å and some appreciable intensities were observed at resolutions better than 1.2 Å.

Type of Medium: Electronic Resource

URL: http://dx.doi.org/10.1107/S0907444995011826

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