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Tris{bis[N-(2-aminoethyl)-1,2-ethanediamine-κ3N]nickel(II)} bis(tetrathioantimonate) (2001)

Stähler, Ralph ; Näther, Christian ; Bensch, Wolfgang

Oxford [u.a.] : International Union of Crystallography (IUCr)

Acta crystallographica 57 (2001), S. 26-27

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ISSN: 1600-5759

Source: Crystallography Journals Online : IUCR Backfile Archive 1948-2001

Topics: Chemistry and Pharmacology , Geosciences , Physics

Notes: Yellow crystals of [Ni(deta)2]3[SbS4]2 (deta is diethylenetriamine, C4H13N3) were synthesized under solvothermal conditions by reacting elemental Ni, Sb and S in a solution of diethylenetriamine. The structure is composed of tetrahedral [SbS4]3− anions in general positions and octahedral [Ni(deta)2]2+ cations located at centres of inversion. In the crystal structure, the anions and cations are stacked in the direction of the a axis in a pseudo-hexagonal arrangement.

Type of Medium: Electronic Resource

URL: http://dx.doi.org/10.1107/S0108270100014359

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