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Nickel(II) complexes of 4-acetamidobenzaldehyde N(4)-substituted thiosemicarbazones (1999)

West, Douglas X. ; Beraldo, Heloisa ; Nassar, Amal A.

Springer

Transition metal chemistry 24 (1999), S. 25-28

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ISSN: 1572-901X

Source: Springer Online Journal Archives 1860-2000

Topics: Chemistry and Pharmacology

Notes: Abstract Nickel(II) complexes with five 4-acetamidobenzaldehyde N(4)- substituted thiosemicarbazones have been prepared in EtOH solution and characterized by physical and spectral methods. N.m.r., i.r. and electronic spectra of the thiosemicarbazones and their complexes, along with physical properties of the complexes, have been recorded. These thiosemicarbazones coordinate as anionic ligands via the thiosemicarbazone moiety's azomethine nitrogen and thiolate sulfur [upon loss of the N(2) hydrogen] when reacted with NiCl2 in the presence of Et3N or with Ni(OAc)2.

Type of Medium: Electronic Resource

URL: http://dx.doi.org/10.1023/A:1006975910459

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