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Coulometric determination of neptunium (1991)

Karelin, A. I. ; Semenov, E. N. ; Mikhailova, N. A.

Springer

Journal of radioanalytical and nuclear chemistry 147 (1991), S. 33-40

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ISSN: 1588-2780

Source: Springer Online Journal Archives 1860-2000

Topics: Chemistry and Pharmacology , Energy, Environment Protection, Nuclear Power Engineering

Notes: Abstract A coulometric titration method with controlled current and amperometric end-point detection with two indicator electrodes was worked out to determine neptunium in solutions which were obtained while treating the spent nuclear fuel. This method allows to determine in presence of 1000-fold quantities and more of Pu, Ce, Cr, Fe, Mn, 1000-fold quantities and more of U. The error of determination is 0.2% for pure Np solutions and increases up to some precent in presence of large amounts of impurity.

Type of Medium: Electronic Resource

URL: http://dx.doi.org/10.1007/BF02039563

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