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The synthesis of a macromolecular ligand by the modification of polystyrene (1981)

Phillips, Hodge H. ; Kinstle, James F. ; Adcock, James L.

New York : Wiley-Blackwell

Journal of Polymer Science: Polymer Chemistry Edition 19 (1981), S. 175-194

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ISSN: 0360-6376

Keywords: Physics ; Polymer and Materials Science

Source: Wiley InterScience Backfile Collection 1832-2000

Topics: Chemistry and Pharmacology

Notes: Uncrosslinked atactic polystyrene was chemically modified first by acetylation then by a Claisen condensation with ethyl perfluoropropanoate to produce three crosslinked chelating polymers that contained a phenyl, perfluoroethyl, beta-diketone chelating group in 10, 20, and 63 mole % compositions. Cu(II), Ni(II), and uranyl chelates of the macromolecular ligands were prepared and analyzed. The macromolecular ligands and their chelates were compared with the model ligating species 4,4,5,5,5-pentafluoro-1-phenyl-1,3-pentanedione with infrared and mass spectroscopy and proton nuclear magnetic resonance.

Additional Material: 4 Ill.

Type of Medium: Electronic Resource

URL: http://dx.doi.org/10.1002/pol.1981.170190117

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