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  • 1
    Electronic Resource
    Electronic Resource
    Zur präparativen Bildung des Tri-tert.-butyl-nonaphosphans(3); P9(CMe3)3 (1990)
    Weinheim : Wiley-Blackwell
    Zeitschrift für anorganische Chemie 585 (1990), S. 49-50 
    Details
    ISSN: 0044-2313
    Keywords: Chemistry ; Inorganic Chemistry
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology
    Description / Table of Contents: Formation of Tri-tert.-butyl-nonaphosphane (3); P9(CMe3)3P9(CMe3)3 1 is formed by the reaction of “Na3P/K3P” with (Me3C)PCl2 [maximum yield 20% with regard to (Me3C)PCl2]. The molar ratio of the reactants used on this synthesis is Na/K:P4:(Me3C)PCl2 is 4:1:2. The method of preparation is described.
    Notes: P9(CMe3)3 1 läßt sich durch Umsetzung von „Na3P/K3P“ mit (Me3C)PCl2 präparativ darstellen (Ausbeute bis 20% bezogen auf Me3CPCl2), wenn die Reaktanden Na/K:P4:(Me3C)PCl2 im Molverhältnis 4:1:2 eingesetzt werden. Die Arbeitsvorschrift wird angegeben.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/zaac.19905850106
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