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Zur Reaktion von Imidodiphosphoryltetrachlorid mit Phosphorpentachlorid (1974)

Riesel, L. ; Mauck, M. ; Herrmann, E.

Weinheim : Wiley-Blackwell

Zeitschrift für anorganische Chemie 405 (1974), S. 109-112

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ISSN: 0044-2313

Keywords: Chemistry ; Inorganic Chemistry

Source: Wiley InterScience Backfile Collection 1832-2000

Topics: Chemistry and Pharmacology

Description / Table of Contents: Reaction of Imidodiphosphoryl Tetrachloride with Phosphorus PentachlorideImidodiphosphoryl tetrachloride quantitatively reacts with PCl5 to form, HCl, POCl3, and Cl3P=N—POCl2. The mechanism of the reaction is discussed. Using 32P-labeled PCl5 was proved that the attack of the PCl5 to imidodiphosphoryl tetrachloride does occur about an oxygen atom.

Notes: Imidodiphosphoryltetrachlorid reagiert mit PCl5 quantitativ zu HCl, POCl3 und Cl3P=N—POCl2. Der mögliche Reaktionsmechanismus wird diskutiert. Mit 32P-markiertem PCl5 gelang der Nachweis, daß der Angriff des PCl5 am Imidodiphosphoryltetrachlorid über ein Sauerstoffatom erfolgt.

Type of Medium: Electronic Resource

URL: http://dx.doi.org/10.1002/zaac.19744050112

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