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Elektrochemische Synthesen, XX. Die Synthese von S4N4 und (S5N5)Cl (1984)

Fritz, Heinz P. ; Bruchhaus, Rainer

Weinheim : Wiley-Blackwell

Berichte der deutschen chemischen Gesellschaft 117 (1984), S. 1920-1925

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ISSN: 0009-2940

Keywords: Chemistry ; Inorganic Chemistry

Source: Wiley InterScience Backfile Collection 1832-2000

Topics: Chemistry and Pharmacology

Description / Table of Contents: Electrochemical Syntheses, XX1). The Syntheses of S4N4 and (S5N5)ClThe cathodic reduction of S3N3Cl3 in 0.1 M (Ph3P=N=PPh3)[PF6]/CH2Cl2 or 0.15 M (Bu4N)-[BF4]/CH2Cl2 yields S4N4 at room temperature and (S5N5)Cl at - 20°C with current efficiencies of 90% and 49%, respectively.

Notes: Die kathodische Reduktion von S3N3Cl3 in 0.1 M (Ph3P=N=PPh3)[PF6]/CH2Cl2 oder 0.15 M (Bu4N)[BF4]/CH2Cl2 ergibt bei Raumtemperatur S4N4 und bei - 20°C (S5N5)Cl mit Stromausbeuten von 90% bzw. 49%.

Additional Material: 1 Ill.

Type of Medium: Electronic Resource

URL: http://dx.doi.org/10.1002/cber.19841170520

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