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Principal components regression for routine multicomponent UV determinations: A validation protocol (1989)

Gemperline, Paul J. ; Salt, Alger

New York, NY : Wiley-Blackwell

Journal of Chemometrics 3 (1989), S. 343-357

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ISSN: 0886-9383

Keywords: Principal components regression ; Factorial design ; Hypothesis testing ; Assay validation ; Chemistry ; Analytical Chemistry and Spectroscopy

Source: Wiley InterScience Backfile Collection 1832-2000

Topics: Chemistry and Pharmacology

Notes: A validation protocol for multicomponent spectroscopic assays based on principal components regression is described. Factorial design and hypothesis tests are used to establish the linearity and absence of interaction between components in the regression model. Testing considers multiple response variables simultaneously so that correlation between residuals is properly treated. Assay reproducibility and sensitivity to related substances are evaluated.

Additional Material: 2 Ill.

Type of Medium: Electronic Resource

URL: http://dx.doi.org/10.1002/cem.1180030204

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