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19F NMR study of 1-halo-F-adamantanes (1993)

Adcock, James L. ; Luo, Huimin ; Dai, Sheng

Chichester : Wiley-Blackwell

Organic Magnetic Resonance 31 (1993), S. 969-971

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ISSN: 0749-1581

Keywords: F-adamantanes ; 1-Halo-F-adamantanes ; Perfluoroadamantyl halides ; 19F NMR ; Adamantyl halides ; 1-Haloadamantanes ; Chemical shifts ; Chemistry ; Analytical Chemistry and Spectroscopy

Source: Wiley InterScience Backfile Collection 1832-2000

Topics: Chemistry and Pharmacology

Notes: An ‘anomalous’ variation of β-fluorine chemical shifts with respect to the inductive effect in the 19F NMR of a series of 1-halo-F-adamantanes is reported. These fluorine chemical shifts are similar to the hydrogen chemical shift anomaly found in the corresponding hydrocarbon halides. Whereas the γ-hydrogen chemical shifts can be rationalized by the inductive effect, the γ-fluorine chemical shifts have the same ‘anomalous’ variation as found in the β-fluorine chemical shifts.

Additional Material: 2 Ill.

Type of Medium: Electronic Resource

URL: http://dx.doi.org/10.1002/mrc.1260311103

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