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  • Articles  (58)
  • 61.70  (58)
  • Springer  (58)
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  • 1980-1984  (39)
  • 1975-1979  (19)
  • Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics  (58)
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  • Articles  (58)
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  • Springer  (58)
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  • Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics  (58)
  • Physics  (60)
  • 1
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    Applied physics 20 (1979), S. 135-140 
    ISSN: 1432-0630
    Keywords: 78.70 ; 71.60 ; 61.70
    Source: Springer Online Journal Archives 1860-2000
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics , Physics
    Notes: Abstract The technique of the coincidence count rate at the peak of the angular correlation curve (CCR) in positron annihilation has been applied to the investigation of vacancy formation energies in thermal equilibrium in nickel, cobalt, and iron. The monovacancy formation energyE 1v/F has been determined to (1.55±0.05) eV and (1.34±0.07) eV for nickel and cobalt, and (1.60±0.10) eV for α-iron, and (1.40±0.15) eV for γ-iron, respectively. The structural phase transformations in cobalt (693 K) and iron (1183 K, 1663 K) are exhibited by discontinuities of the CCR. In the case of cobalt the CCR follows exactly the change of the thermal expansion at the transition temperature. The temperature dependence of the CCR in the prevacancy region is found to be proportional to the thermal expansion for all metals investigated.
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  • 2
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    Applied physics 13 (1977), S. 171-173 
    ISSN: 1432-0630
    Keywords: 61.70 ; 61.80 ; 62
    Source: Springer Online Journal Archives 1860-2000
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics , Physics
    Notes: Abstract Ultrasonic pulsed-echo patterns in AC-cut quartz crystals cooled to 4.2 K have been studied over the frequency range 0.2〈f〈0.6 [GHz]. The observed beats, superimposed on the exponential decay, have been identified as resulting from diffraction of the waves in the finite-size crystals. Furthermore, it has been found that irradiation with 1 MeV γ-rays yields samples with both a smaller attenuation constant and less pronounced beats. The significance of the reported results lies mainly in the potential application of the procedure of γ-ray irradiation, and subsequent bleaching with ultraviolet light, in order to obtain quartz crystals with improved acoustic patterns.
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  • 3
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    Applied physics 23 (1980), S. 303-309 
    ISSN: 1432-0630
    Keywords: 42.80 ; 61.70 ; 61.80 ; 78.20
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    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics , Physics
    Notes: Abstract A significant contribution to the degradation of GaAs-based lasers and light-emitting diodes arises from the formation of so-called dark line defects. It is shown that these defects are accumulations of non-radiative recombination centres around dislocations. The centres are identified as As vacancies, which are emitted by climbing dislocations, concomitantly with the absorption of Ga interstitials. From scanning deep-level transient spectroscopy observations it is concluded that the so-called DX centres are Ga interstitials. The driving force for dislocation climb and thus for dark-line-defect formation is a supersaturation of Ga interstitials originating from the growth of the GaAs crystals under Ga-rich conditions as a consequence of the high volatility of As. Phenomena in other III–V compound semiconductors related to the formation of dark line defects in GaAs are also discussed.
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  • 4
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    Applied physics 30 (1983), S. 117-122 
    ISSN: 1432-0630
    Keywords: 61.70 ; 72.70
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    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics , Physics
    Notes: Abstract Fluctuations in the number of vacancies in metals in thermal equilibrium lead to resistivity fluctuations. Analysis of these fluctuations permits measurement of both formation and migration enthalpy of the vacancies. The power spectrum of the fluctuations is calculated using a series of statistically independent pulses. It can be derived from the diffusion equation for any geometry of the vacancy sinks. Vacancy diffusion to the surface of a thin plate or of a sphere are treated as examples. The measurability of vacancy noise is assessed. It should also be possible to measure vacancy noise during irradiation. It is predicted that correlated vacancy creation, which may occur during irradiation, will cause an increase in the power spectrum.
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  • 5
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    Applied physics 26 (1981), S. 107-113 
    ISSN: 1432-0630
    Keywords: 61.70 ; 78.70
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    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics , Physics
    Notes: Abstract The isothermal recovery rates of vacancy-impurity complexes in an aluminium-1% magnesium alloy are measured in situ at eight temperatures from variations of colinear annihilation γ-rays versus time. These data analysed in terms of a time dependant β+-trapping model yield two apparent migration energies of 0.8 eV±0.1 eV and 0.9 eV±0.05 eV. The nature of the complexes is discussed and their binding energy is estimated.
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  • 6
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    Applied physics 32 (1983), S. 45-53 
    ISSN: 1432-0630
    Keywords: 66.33 ; 61.70 ; 82.65
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    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics , Physics
    Notes: Abstract The proton conductivity in H3OUO2AsO4·3H2O (HUAs) has been measured below the transition temperature at 299 K. A consistent picture of the elementary process taking place is developed from separate electrochemical, spectroscopic and calorimetric measurements. The conductivity is proposed to occur by the “vehicle mechanism” of proton transport, i.e. the cooperative motion of H3O+ and H2O. This mechanism is compared with the Grotthuss and the simple ion hopping mechanism.
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  • 7
    ISSN: 1432-0630
    Keywords: 61.70 ; 66.30 ; 85.3085.30
    Source: Springer Online Journal Archives 1860-2000
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics , Physics
    Notes: Abstract In- and out-diffusion of gold in silicon were investigated with the aid of a neutronactivation analysis in combination with mechanical sectioning or by the spreadingresistance technique. In-diffusion profiles in the range 1371–1073 K show that Au diffuses in Si mainly via the so-called kick-out mechanism. From the Au diffusion and solubility measurements the interstitialcy contributionD I SD to the Si self-diffusion coefficient was determined, which shows that the self-diffusion occurs to a considerable extent via selfinterstitials. Out-diffusion profiles at 1173 K were measured on wafers homogeneously supersaturated with Au. The observed decrease of the electrical activity of Au in the bulk indicates that during the out-diffusion anneal the majority of Au atoms originally dissolved substitutionally changes its configuration.
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  • 8
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    Applied physics 27 (1982), S. 167-169 
    ISSN: 1432-0630
    Keywords: 61.70 ; 68 ; 74
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    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics , Physics
    Notes: Abstract A simple method is presented to prepare very low pinning niobium foils on which geometrically well defined Nb3Sn-pinning structures of arbitrary shape are deposited. This facilitates the fabrication of samples for guided vortex motion experiments some of which are reported.
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  • 9
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    Applied physics 34 (1984), S. 231-236 
    ISSN: 1432-0630
    Keywords: 68.55 ; 61.70
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    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics , Physics
    Notes: Abstract Antiphase domains occur in thin GaAs epitaxial films grown on Ge(001) by molecular beam epitaxy. The domains have been imaged by transmission electron microscopy using 200-type reflections in dark field. The carefully chosen imaging conditions with convergent illumination ensure that doubly diffracted beams from a pair of first order Laue zone discs contribute to the singly diffracted 200-type beams. The three Bragg reflections may add in or out of phase to give domains in either light or dark contrast depending on their polarity.
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  • 10
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    Applied physics 35 (1984), S. 119-124 
    ISSN: 1432-0630
    Keywords: 61.70 ; 66 ; 85.30 ; 79.20
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    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics , Physics
    Notes: Abstract The gettering efficiency for Au induced by Ne+ and Ar+ implantation has been studied. The depth distribution of gettered Au as a function of annealing temperature and dose of implanted Ne+ and Ar+ ions are presented. The experiment shows that the maximum efficiency of gettering occurs when the implantation doses are comparable with amorphization dose.
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  • 11
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    Applied physics 28 (1982), S. 99-102 
    ISSN: 1432-0630
    Keywords: 61.70 ; 81.40
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    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics , Physics
    Notes: Abstract Supersaturated surface alloys produced by very high dose (0.8−2.6×1017cm−2) implantation of As-ions into silicon and subsequent pulsed electron-beam annealing have been investigated by means of the channeling technique. The maximum solubility limit of 7×1021 As/cm3 has been determined. It exceeds the equilibrium solubility limit by more than a factor of 4. Angular scan measurements indicated that for doses above 1×1017cm−2 As atoms are displaced by about 0.12 Å from the regular lattice sites.
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  • 12
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    Applied physics 28 (1982), S. 179-187 
    ISSN: 1432-0630
    Keywords: 78.70 ; 61.70
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    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics , Physics
    Notes: Abstract Positron annihilation measurements of the coincidence count rate at the peak of the angular correlation curve (CCR) have been performed as a function of temperature for the alloy systemFeTi in a concentration range up to about 1.3 at. %. The concentration dependence of the effective vacancy formation enthalpy (H 1V F )eff suggests the existence of an attractive interaction between vacancies and the impurity atoms. It will be shown that the description of the vacancy concentration in an alloy according to the Lomer model is not valid in this case, because it neglects binding of vacancies to solute atom pairs and to higher agglomerates. The application of a model proposed by Dorn and Mitchell gives evidence that beyond the binding of a vacancy to a single solute atom in the concentration range investigated also aggregates of a vacancy bound to two and three foreign atoms must be taken into account. The analysis of the measurements according to the method of Hehenkamp and Sander gives values for the respective vacancy-solute-atom(s) binding enthalpies H 1 B =0.25eV, H 2 B =0.53eV and H 3 B =0.91eV. The discussion of the temperature and solute-atoms concentration dependence of the vacancy concentration suggests a much more complicated behaviour than for pure metals even at low solute-atom concentrations.
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  • 13
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    Applied physics 12 (1977), S. 217-218 
    ISSN: 1432-0630
    Keywords: 78.70 ; 61.70
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    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics , Physics
    Notes: Abstract Published data on positron annihilation lifetime in copper as a function of grain size have been analyzed to show that there is a linear relationship between the internal grain boundary surface area, per unit volume,S v, and the positron lifetime, τ. The analysis indicates that grain boundaries are important in the trapping of positrons. It is suggested that the slope of the resulting straight line,dS v/dτ, can be used to determine the annihilation rate of the grain boundaries.
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  • 14
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    Applied physics 12 (1977), S. 341-345 
    ISSN: 1432-0630
    Keywords: 61.70 ; 66 ; 68.20
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    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics , Physics
    Notes: Abstract Hillocks and voids (vacancy crystals) which were formed by electromigration on ultrapure gold and silver wires, showed only the combined crystal forms {111} and {100}. These planes are identical with the equilibrium planes GI, calculated by Stranski and Kaishew for nonpolar substances under the assumption of only nearest neighbor interaction. Hillock and void nucleation occurred on crystal imperfections (heterogeneous nucleation). Hillocks and vacancy crystals (voids) on gold showed twin formation obeying the spinel law.
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  • 15
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    Applied physics 13 (1977), S. 51-54 
    ISSN: 1432-0630
    Keywords: 78.70 ; 61.70 ; 81
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    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics , Physics
    Notes: Abstract The positron annihilation lineshape was measured in indium in the temperature range between 74 K and the melting point (430 K). A model based on self-trapping of positrons and trapping by vacancies was fitted through the data. A vacancy formation enthalpy of (0.48±0.03) eV was obtained.
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  • 16
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    Applied physics 13 (1977), S. 105-106 
    ISSN: 1432-0630
    Keywords: 61.70 ; 64 ; 81
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    Notes: Abstract Precision measurements of positron lifetime spectra in Fe-29.5at.%Ni alloy specimens were performed to clarify the nature of the martensitic transformation in this alloy. The forward transformation did not introduce any defects which behave as strong trapping sites for positrons. On the other hand, the reverse transformation accompanied the production of defects, to which the positron lifetime is sensitive, maybe dislocations. From the present results, the nature of the transformation was discussed.
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  • 17
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    Applied physics 21 (1980), S. 195-198 
    ISSN: 1432-0630
    Keywords: 61.70 ; 76.80 ; 81.40
    Source: Springer Online Journal Archives 1860-2000
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics , Physics
    Notes: Abstract Polycrystalline samples of LiNbO3 doped by the enriched57Fe isotope have been studied at room and liquid nitrogen temperatures by nuclear γ-resonance (NGR). Iron impurity concentrations were 0.07, 0.30, 1.02, 2.06 at.%, the Li/Nb ratio being 0.935, 0.990, 1.000. An asymmetry of the quadrupole doublet of NGR experimental spectra has been found. Acceptable hypotheses are discussed to explain the nature of the asymmetry: the Goldanskii-Karyagin effect, the effect of sample texture, and the electron and nuclear spin-lattice relaxation effect. On the basis of computed NGR spectra and thorough analysis of the models we can conclude that there is tendency to form coupled pairs of Fe2+ cations in neighbour lithium and niobium sites. The probability of the formation of such pairs exceeds considerably the statistical value.
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  • 18
    ISSN: 1432-0630
    Keywords: 61.70 ; 64 ; 81
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    Notes: Abstract The effect of lattice defects on positron annihilation in semiconductors was studied. In silicon, any detectable doping effect could not be found. In germanium, the thermal equilibrium measurements of annihilation lineshapes showed no vacancy effect. From these experimental facts, the interaction of positrons with lattice defects was discussed.
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  • 19
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    Applied physics 17 (1978), S. 89-97 
    ISSN: 1432-0630
    Keywords: 61.80 ; 68.20 ; 61.70
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    Notes: Abstract This paper describes blistering of rhenium following 21 keV He+-ion irradiation at temperatures between 300 K and 1200 K. Blistering starts at 300 K at a dose of 3×1017 ions/cm2. The most probable blister diameter varies from 4400 Å at 300 K to 10100 Å at 1200 K. The blister depth τ bl , the blister diameter φ bl and the blister heighth bi show a distribution. From the observations one could derive the following relationships:h bl = 0.35φ bl ; τ bl =3.43φ bl 2/3 . The erosion yieldE y due to blistering is function of doseE y =0.51 atoms/ion at 3×1017 ions/cm2,E y =0.56 atoms/ion at 6×1017 ions/cm2 andE y =0.14 atoms/ion at 3×1018 ions/cm2. The sputtering yieldS (21 keV) is estimated to be ∼0.1 atom/ion. The corresponding surface regression is 44Å at 3×1017 ions/cm2 and 1323 Å at 9×1018 ions/cm2. Surface regression has therefore little influence on the observations at low doses.
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  • 20
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    Applied physics 20 (1979), S. 29-35 
    ISSN: 1432-0630
    Keywords: 76 ; 61.70
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    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics , Physics
    Notes: Abstract It is shown that lattice deformations around interstitial atoms may give a significant contribution to the local magnetic dipolar field at the interstitial site. An analysis of the dipole field measured for mouns on octahedral interstitial sites in Co shows that 1/4 of the dipole field results from lattice deformations. The double force tensor of the muon is found to be nearly isotropic and of the order of magnitude of 4eV.
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  • 21
    ISSN: 1432-0630
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    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics , Physics
    Notes: Abstract Transmission electron microscopy, optical reflection and channeling effect measurements are employed to investigate disorders in 30 keV, high dose (3×1016ions/cm2) and high current (≦5 mA) phosphorus as-implanted silicon with (111), (100), and (110) orientation as a function of temperature rise (100–850°C) by the beam heating effect during implantation. Temperature rise below 400°C results in continuous amorrphous layer formation. This contrasts with results of the recovery into single crystals for temperature rise samples above 500°C, regardless of wafer orientation. Secondary defects (black-dotted defects, dislocation loops and rodlike defects) are formed in singlecrystal recovery samples, having a deeper distribution in (110) wafers and a shallower distribution in (111) and (100) wafers. Rodlike defects observed in 850°C samples are of “vacancy” type and have the largest density in (110) wafers.
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  • 22
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    Applied physics 22 (1980), S. 415-419 
    ISSN: 1432-0630
    Keywords: 61.70 ; 61.60 ; 78.70
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    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics , Physics
    Notes: Abstract The positron lifetime in electron-irradiated undoped and doped silicon crystals is studied as a function of temperature between 90 and 300 K. We show that the temperature dependence of the two lifetime components does not arise from the escape, but from the trapping rate at defects. The temperature dependences of the capture cross sections are deduced. It is concluded that in undoped crystals the positrons interact with negatively charged and neutral defects, probably divacancies and vacancy-oxygen complexes, respectively. In strongly P-doped crystals positron trapping occurs preferably in negatively charged centers.
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  • 23
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    Applied physics 23 (1980), S. 361-368 
    ISSN: 1432-0630
    Keywords: 61.70 ; 66 ; 85.30
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    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics , Physics
    Notes: Abstract The diffusion of Au in Si is known to take place via the interchange of Au atoms between substitutional (Au s ) and interstitial (Au i ) sites. So far it has generally been believed that this interchange involves lattice vacancies (V) and that it occurs via the Frank-Turnbull mechanism V+Au i ⇆Au s . It is stated in the literature that this model explains the observation that the Au s concentrationC s m in the centre of Au-diffused Si wafers increases with timet according to $$C_s^m \propto \sqrt t $$ . We show that this statement is incorrect, i.e., the Frank-Turnbull model cannot account for the $$C_s^m \propto \sqrt t $$ law. Such a dependence is expected in the case of Si wafers with a sufficiently low density of internal sinks for self-interstitials if the Au i −Au s interchange is controlled by the so-called kick-out mechanism Au i ⇆Au s +1. Since this mechanism involves self-interstitials (I) the present result is in accordance with the fact that under high-temperature equilibrium conditions the dominating intrinsic point defects in Si are self-interstitials and not vacancies as in Ge or metals.
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  • 24
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    Applied physics 22 (1980), S. 155-160 
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    Keywords: 76 ; 61.70
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    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics , Physics
    Notes: Abstract The high-field susceptibility of a cylindrical EuS single crystal was measured in the temperature range between 2.5 K and 16.5 K with applied magnetic fields up to 45 kOe. The measured field dependence of the susceptibility was explained by taking into consideration thermally excited spin waves and the influence of microstructural defects on the spin arrangement. The exchange integral with nearest neighbour and next-nearest neighbour atoms,J=J 1+J2, was determined to be (0.14±0.02)k B(K). This result is in good agreement with the value derived from neutron scattering experiments. The analysis of the influence of different types of crystal defects on the law of approach to ferromagnetic saturation shows that the nonmagnetic inclusions play a dominant role in our case. The deduced density of nonmagnetic inclusions according to the micromagnetic theory agrees well with the result of scanning elecron microscope (SEM) observations.
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  • 25
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    Applied physics 22 (1980), S. 185-187 
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    Keywords: 06 ; 07 ; 61.70
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    Notes: Abstract New methods for thermal-equilibrium investigations of atomic vacancies or of dislocation movements in metals require measurements of minute resistance fluctuations. The accuracy of such measurements is limited by thermal noise from the resistor. The present paper proposes a method for analysing resistance fluctuations independent of voltage noise.
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  • 26
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    Applied physics 22 (1980), S. 385-388 
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    Notes: Abstract The effects of pulsed electron-beam annealing of high-dose As implanted {111} Si single crystals has been studied. The depth distributions and lattice location of the As atoms were obtained using MeV4He+ backscattering and channeling technique. The implantation energy was 100 keV with a total dose of 3.5·1016/cm2. Above the threshold energy of 0.9 J/cm2 the single-crystal transition was observed with about 95% of the As atoms on substitutional lattice sites. This leads to an As concentration of 2·1021/cm3 which was demonstrated to be a metastable one.
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  • 27
    ISSN: 1432-0630
    Keywords: 78.70 ; 61.70 ; 61.80
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    Notes: Abstract The sensitivity of positrons to point defects created by the irradiation of V3Si with neutrons is demonstrated. We found no indication of thermal vacancies by thermal equilibrium measurement up to 1273 K which indicates that the monovacancy formation enthalpy for V3Si isH 1V F ≧(1.84±0.14) eV. Investigations within the range of homogeneity for excess vanadium suppot the idea that substitutional defects are the dominating defect type, whereas for excess silicon a direct confirmation of existing structural vacancies as the dominating defect type is given.
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  • 28
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    Applied physics 30 (1983), S. 195-211 
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    Keywords: 61.70 ; 81.10 ; 66.30
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    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics , Physics
    Notes: Abstract The rapid solidification of silicon layers melted by high-power laser pulses lead to an enhanced incorporation of implanted dopants in substitutional lattice sites. A review of experimental results, heat and mass transport calculations, is presented together with the latest models for solute redistribution during rapid solidification. Interfacial instabilities, leading to cell structure and other factors limiting the maximum concentration of incorporated dopants are also presented.
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  • 29
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    Applied physics 30 (1983), S. 233-235 
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    Keywords: 61.70 ; 71.55
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    Notes: Abstract It is found from DLTS measurements that plastic deformation of GaAs single crystal creates a new kind of electron traps with an activation energy of 0.37 eV, and gives rise to an increase in the concentration of main electron traps with an energy of 0.80 eV. By comparing the concentrations of the main electron traps before and after deformation with analogous concentrations of AsGa paramagnetic centers, found by EPR experiments, it is concluded that the centers observed in both cases are of the same origin. A nonstandard feature of the main traps is discovered: linear dependence of the DLTS-peak amplitude on the logarithm of the filling-pulse duration time. This feature can be explained in terms of the barrier-limited capture rate, assuming the traps are arranged in rows.
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  • 30
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    Applied physics 32 (1983), S. 155-158 
    ISSN: 1432-0630
    Keywords: 66.30 ; 61.70 ; 82.65
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    Notes: Abstract The proton conductivity in tetragonal H3OUO2AsO4·(3-δ)H2O has been measured above the transition temperature at 299 K. The conductivity, calorimetric and spectroscopic data depend on the water content and the transition is suggested to be a peritectic reaction setting free a small amount of solution, which stays strongly adsorbed between the layers of the structure and gives rise to the high conductivity.
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    Applied physics 27 (1982), S. 257-261 
    ISSN: 1432-0630
    Keywords: 78.70 ; 61.70 ; 81
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    Notes: Abstract The positron lifetime was measured in cadmium in the temperature range between 80 K and 500 K. For the first time a plateau was observed by this method in polycrystalline samples. The obtained data are well explained by depletion of shallow traps forT≤180 K and by self-trapping in the prevacancy region.
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  • 32
    ISSN: 1432-0630
    Keywords: 61.70 ; 81
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    Notes: Abstract By means of an integrated source-specimen technique the temperature dependence of positron lifetimes and annihilation lineshapes has been measured, on the same specimens of gold and cadmium from 4.2K to the melting points, and also in electronirradiated and quenched gold. The anomalous temperature dependence of positron annihilation at intermediate temperatures (200 to 350 K in Cd, 270 to 750 K in Au) discovered by Lichtenberger, Schulte, and MacKenzie is confirmed. The data are incompatible with the idea that the intermediate temperature dependence is due to thermal expansion. They are well explained by an extension of the trapping model which includes the formation of metastable self-trapped positrons. From lineshape measurements after electron irradiation at 180 K and after quenching it is deduced that the trapping rate of positrons at vacancy-type defects in Au is temperature independent below room temperature.
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  • 33
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    Applied physics 20 (1979), S. 353-356 
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    Keywords: 61.70 ; 61.80
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    Notes: Abstract The effects of single-pulse ruby laser irradiation have been investigated in Si samples with disorder layers located at a depth of 2000 Å from the crystal surface and extending up to 8000 Å. This disorder was obtained by implantation with 350 keV N+ to a fluence of 2×1016/cm2. Channeling, diffraction and transmission electron microscopy were used to characterize the structure of the irradiated layers. After 1.5 J/cm2 irradiation the damaged layer reorders partially, while for about 2.0J/cm2 the surface single crystal becomes polycrystalline. At a higher energy density all the material undergoes the transition to single crystal. Calculations based on the liquid model accounts in part for the experimental results.
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  • 34
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    Applied physics 18 (1979), S. 29-33 
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    Keywords: 61.70 ; 62.20
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    Notes: Abstract The defect structure in EuS single crystals grown form the melt is studied by etch pitting, scanning and high-voltage electron microscopy. Circular and square etch pits and a second phase in the shape of thin hexagonal platelets are observed by etching. Microprobe analysis indicates the platelets to consist of Eu metal. In the transmission electron microscope, smoothly curved dislocations and helical dislocations, small dislocation loops and inclusions associated with dislocations are observed. The possible origin of the detected dislocation structure is considered with reference to climb and glide processes occurring during cooling down the grown crystals. The results corroborate the glide geometry of the NaCl lattice for EuS.
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  • 35
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    Keywords: 68.50 ; 61.70
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    Notes: Abstract A summary of the theoretical and experimental investigations carried out to understand the problem of epitaxy is given. The effect of deposition conditions and the nature of the substrate-deposit combination on the orientation of the final film is discussed. The importance of the nucleation and growth stages, reorientation and recrystallization effects and the influence of the impurities and defects in the substrate surface on the quality of the films deposited are presented.
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  • 36
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    Applied physics 30 (1983), S. 161-167 
    ISSN: 1432-0630
    Keywords: 61.70 ; 61.80 ; 68.55
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    Notes: Abstract In this paper we want to show by means of Reflection High Energy Electron Diffraction (RHEED) techniques that the recrystallization processes taking place on amorphous germanium films irradiated with low-power superimposed ruby laser pulses occur gradually. Furthermore, in implanted α-Ge films the amorphous-crystalline front moves from the surface of the specimen towards the substrate, while the opposite occurs for glow-discharge deposited films. Moreover, electron microscope observations carried out with a double-stage carbon replica technique at different depths in the specimen show that defect migration is one of the competitive mechanisms in low-power laser annealing.
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  • 37
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    Applied physics 29 (1982), S. 105-111 
    ISSN: 1432-0630
    Keywords: 71.55F ; 61.70 ; 73.40Q
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    Notes: Abstract The annealing behavior of trap-centers was studied in float-zone silicon wafers containing A-swirl defects. Samples from areas of high and low A-swirl density were annealed in nitrogen ambient between 100° and 900 °C, and analysed using the Deep Level Transient Spectroscopy. The results indicate, that two levels atE c }-0.07 eV,σ n=4.6×10−16 cm2, andE c−0.49eV,σ n=6.6×10−16cm2 are caused by one defect, for which the silicon di-selfinterstitial is a likely interpretation. A level atE c }-0.11 eV was assigned to interstitial carbon. Both defects annealed out at about 170 °C. After 600 °C annealing an additional level atE c−0.2 eV was detected, which was attributed to an interstitial silicon carbon complex. Heat treatment at 800 °C generated a new level atE c−0.49 eV,σ n=2.9×10−16cm2 only in the area of high A-swirl defect density. This level was also observed after oxidation and subsequent annealing of silicon.
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  • 38
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    Applied physics 35 (1984), S. 249-253 
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    Keywords: 61.70 ; 61.80 ; 71.35 ; 78.55
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    Notes: Abstract The topograms revealing the anisotropic distribution of defects in the volume of monocrystalline YAG samples have been obtained by the thermoluminescence (TL) technique. It has also been shown that the anisotropic distribution of the lattice defects affects strongly the shape of the TL curves. The greatest changes in the TL intensity were observed in the areas of the samples distributed symmetrically every 120°. It was noted that the selective distribution of the TL intensity is caused mainly by the presence of the (211) facets as well as growth striations formed during the growth process. The groups of lines observed in the TL spectrum have been ascribed to the Tb3+ ions, excited owing to the radiationless energy transfer from the bound exciton states (BES).
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  • 39
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    Applied physics 11 (1976), S. 191-192 
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    Keywords: 61.70 ; 71.55 ; 81
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    Notes: Abstract The isochronal annealing of two plastically deformed irons of 99.998% and 99.86% purities is studied by positron lifetime and annihilation line shape measurements. The results show that trapping of positrons is caused by dislocations. At around 300° C a recovery process attributed to a rearrangement of dislocation structure is observed in the pure but not in the impure iron. The positron lifetime in deformed and recrystallized state is found to be 167 ps and 117 ps, respectively.
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  • 40
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    Applied physics 20 (1979), S. 305-312 
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    Keywords: 63 ; 61.70
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    Notes: Abstract An analysis of possible transformations of moments of force by a diamond lattice has been made. The conditions of resonance transformations of moments of force by this lattice have been found. The dynamics symmetry of the diamond lattice has been determined in terms of the Shubnikov group Fd3m'. Besides, it has been found that resonance librationally deformed configurations are oneperiodic and have cores 〈110〉 two times more deformed than the surrounding area. As a result of the action of resonance phonons of the librational mode it is possible to generate a new kind of defects-bidislocations with Burgers vector components+[110]/2 and −[110]/2. It has been shown that bidislocations can play an essential role in plastic deformation of a diamond lattice and other related lattices.
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  • 41
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    Applied physics 17 (1978), S. 31-39 
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    Keywords: 61.70 ; 61.80
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    Notes: Abstract The growth, movement and nature of outside dislocation, which propagate from heavily phosphorus (〉1015 ions/cm2) implanted (111), (100), and (110) silicon layers into unimplanted outside regions by a compressive strain induced during 1100° C wet O2 annealing, are investigated using transmission electron microscopy and x-ray diffraction topography. Outside dislocations are formed, mainly on (111) planes., by the glide motion of dislocation networks formed in implanted layers during early annealing. This results in dislocations extending into the unimplanted areas to different degrees, in the order of, from the largest to smallest, (111), (110), and (100) wafers. In (110) wafers, the [001] oriented dislocations in the implanted regions rise to the surface at the implant and unimplant boundary. On the other hand, the [110] dislocations penetrate into the unimplanted region. Two sets of orthogonal 〈110〉 oriented dislocations generated in (100) implanted wafers behave in the same manner as the [001] dislocations in (110) wafers. Some sources of the compressive strain related to the generation of these dislocations are discussed.
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  • 42
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    Notes: Abstract High-voltage electron microscopy in combination with a large-area thinning technique has been applied to thin epitaxial Ge layers on GaAs substrates. These layers exhibit 60° misfit dislocations along the 〈110〉 directions parallel to the interface. Various dislocation reactions are evaluated from the electron micrographs, e.g. the formation of non-glissile 90° dislocations from two nearly parallel 60° dislocations and the annihilation reaction of two crossing 60° dislocations with identical Burgers vectors. The latter reaction occasionally leads to a dislocation multiplication. The misfit dislocations in very thin layers (∼0.5 μm thickness and a linear dislocation density of less than 100 dislocation lines/cm) tend to be arranged in groups rather than being equidistant. Consequences for the interpretation of x-ray topograms are discussed.
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  • 43
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    Notes: Abstract The anisotropy of the local magnetic dipole field is calculated for interstitial lattice sites of tetragonal, trigonal, or orthorhombic symmetry in bcc and hep crystals. In addition, for interstitial sites of uniaxial symmetry the effects of lattice deformations on the magnetic dipole field are investigated. A discussion of experimental results obtained from muon spin rotation experiments on Co and Gd shows that in these metals lattice-deformation effect may influence the local dipole fields significantly.
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  • 44
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    Applied physics 20 (1979), S. 265-273 
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    Notes: Abstract The paper re-examines the effect of oxidation on the diffusion of phosphorus and boron in silicon as well as recent results on redistribution phenomena of these dopants under irradiation and on the emitter-push effect. It is shown that at high temperatures phosphorus and boron diffuse via a defect mechanism involving silicon self-interstitials. These results support the view-point that self-interstitials are the dominating point defects in silicon under thermal equilibrium conditions. Possible generation mechanisms for the self-interstitial supersaturation causing the emitter-push effect are suggested.
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  • 45
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    Applied physics 21 (1980), S. 257-261 
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    Keywords: 61.70 ; 71.55
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    Notes: Abstract Deformation-produced deep levels, both of electron and hole traps, have been studied using deep level transient capacitance spectroscopy (DLTS) for an undopedn-type GaAs (HB grown) compressed at 440°C. Concentrations of two grown-in electron trap levels (E c −0.65eV andE c −0.74eV) and one grown-in hole trap level (E v +∼0.4eV) increase with plastic deformation, while that of a grown-in electron trap level (E c −∼0.3eV) decreases in an early stage of deformation. While no new peak appeared in the electron trap DLTS spectrum after plastic deformation, in the hole trap DLTS spectrum a broad spectrum, seemingly composed of many peaks, newly appeared in a middle temperature range, which may be attributed to electronic energy levels of dislocations with various characters.
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  • 46
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    Applied physics 30 (1983), S. 123-126 
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    Notes: Abstract The displacement field around a dislocation loop had been calculated to give the diminishing factor of X-ray diffraction intensity from a fatigued Al sample. Experimentally had been measured this factor on the samples fatigued at room temperature and at low temperature. From these the size and density of dislocation loops can be deduced. Results show that in the sample fatigued at room temperature there is no significant change in dislocation structure while at low temperature in fatigued sample occurs a large amount of dislocation loops whose density is 1014−1017cm−3 while their radii are between 100 and 1000 Å.
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  • 47
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    Notes: Abstract An extensive analysis of the substitutional dopant diffusion phenomena in silicon during oxidation is presented. The analysis covers qualitative as well as quantitative aspects of the oxidation-enhanced and -retarded diffusion (OED and ORD) phenomena, and examines three different possible assumptions that can be made on the nature of the silicon thermal equilibrium point defect species: silicon self-interstitials (I) only, vacancies (V) only, coexistence of I and V. The only consistent way to interpret all properly documented OED/ORD data is to assume that I and V coexist under oxidation as well as under thermal equilibrium conditions at high temperatures.
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  • 48
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    Applied physics 31 (1983), S. 109-114 
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    Keywords: 61.70 ; 65
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    Notes: Abstract Distribution and morphology for dislocations introduced in (001) Si wafers subjected to bending stress at 800°, 900°, and 1100°C were investigated. For wafers bent around a [110] axis at 900° and 1100°C, straight dislocations appeared along the [110] direction only near the neutral plane, and were absent at the surfaces where bending stress is greatest. However, for wafers bent at 800 °C, such straight dislocations were not formed. Dependence of the dislocation distribution and morphology on heat treatment temperature is explained on the basis of interaction between bending stress and SiO2 precipitates introduced in bulk. Also, it was found that the straight [110] dislocations remained still near the neutral plane, even when additional reverse bending stress was applied around an axis parallel to the dislocations, but were transfered toward the tensile surface by bending around an axis normal to the dislocation direction.
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    Applied physics 32 (1983), S. 159-161 
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    Keywords: 66.30 ; 61.70 ; 42.60
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    Notes: Abstract The entire sodium ion content of sodiumβ″ alumina (Na1.67Mg0.67Al10.33O17) can be replaced with a variety of lanthanide ions by simple diffusion reactions at moderate temperatures (500–700°C). Lanthanideβ″ alumina crystals are hard, clear, chemically stable, and have well-defined crystal structures. The fluorescence spectrum of Nd3+ inβ″ alumina is similar to that in YAG. The lifetime of the4 F 3/2 state of Nd3+ in completely-exchangedβ″ alumina (350μs at 1021 Nd3+ cm−3) is about 45% longer than in YAG (240μs at 1020Nd3+ cm−3). The lanthanideβ″ aluminas may be of considerable interest as new phosphor and laser host materials.
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  • 50
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    Notes: Abstract For the first time the positron lifetimes in polycrystalline tin have been measured as a function of temperature in the whole range from 80 K to the melting point. The temperature dependence of the mean lifetime could be divided into four regions which can be attributed to the depletion of shallow traps, normal thermal expansion, prevacancy effects, and trapping by vacancies, respectively. In one of the samples the phase transition fromβ- toα-Sn clearly could be detected at 230 K by a sharp increase in the mean lifetime.
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    Notes: Abstract Trapping of positrons at vacancy-type defects in magnesium was studied by positron lifetime and Doppler-broadening measurements. Vacancy defects were produced by quenching, electron irradiation and deformation at low temperatures as well as by thermal agitation at elevated temperatures. In the first three cases we observed trapping at multiple vacancies, which anneal out between 77...400 K. Thermal equilibrium measurements show S-shape behaviour originating from positron trapping at magnesium monovacancies. However, changes in the positron parameters were very small, which is due to the weakness of the positron-vacancy interaction. A detrapping analysis yielded a positron-vacancy binding energy of the order of 0.3...0.4 eV.
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    Notes: Abstract In (100)p-Si radiation damage was produced by implanting B+ ions with an energy of 80keV, 90keV and 1.6MeV. The specimens were annealed by scanned electronbeam irradiation (20keV, 1–2mAcm−2). The formation, evolution and annihilation of defects during the irradiation process were investigated by employing DLTS and RBS measuring techniques. The results show a minimum of defect concentration and an efficiency of the electrical activation of B higher than 80% at an annealing time of 4.5 s. For irradiation times longer than 5 s it becomes evident, that the crystal surface acts as source of defects and contributes to an increase in defect concentration.
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    Notes: Abstract Positron-annihilation lineshape parameter measurements were performed during isothermal annealing of room temperature deformed iron. An isothermal annealing effect is seen in impure iron while in pure iron no effect is measured.
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    Applied physics 27 (1982), S. 149-152 
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    Notes: Abstract A simple model is developed for the trapping of positrons at grain boundaries. It is shown that there is a linear relationship between any linear annihilation parameter and the inverse grain size. An effective grain boundary width is defined, which depends on the positron diffusion length and on the strength of the grain boundary for positrons. The effect of detrapping on this effective width is also considered. The model is tested by using the experimental results available in the literature.
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    Applied physics 27 (1982), S. 171-176 
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    Keywords: 61.70 ; 66 ; 85.30
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    Notes: Abstract The paper presents a theoretical study of the diffusion of gold into dislocated silicon wafers in terms of the kick-out mechanism Au i ⇄Au s +I, where Au i , Au s , andI mean Au interstitials, substitutional Au atoms, and Si self-interstitials, respectively. In agreement with experiments it is found that the Au s concentration in the centre of a wafer,C s m , increases with the durationt of the diffusion anneal according toC s m =C s eq (k 0 t)1/2 except forC s m values in the vicinity of the solubility limitC s eq of Au s . Approximate analytical expressions fork 0 as a function of the densityN I of the dislocations acting asI sinks are given for the entire regime 0≦NI〈+t8.
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    Applied physics 35 (1984), S. 109-114 
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    Notes: Abstract Dislocation configurations and stacking faults in commercial copper rods after 20% and 70% cold-rolling, fatigue and unidirectional tension here studied by x-ray line profile analysis. The analysis of dislocation is based on the Stokes method, the Warren-Averbach analysis and the Wilkens theory for Gaussian or mixed type of strain broadening profiles. For the Cauchy type the range of stress field of dislocations is small, and a model of regular distribution of dislocation dipoles is proposed instead of the Wilkens model of a restrictedly random distribution of dislocations. Due to the obvious texture in all four kinds of deformed samples, the possible glide systems are obtained by using a biaxial stress system. The analysis of stacking faults is based on theories of Patterson, Warren, and Wagner by measuring profile peak shifts, asymmetry and broadening. The broadening due to perfect dislocations and stacking faults can easily be separated. The configuration parameters and density of dislocations, the probabilities of intrinsic, extrinsic and twin stacking faults were deduced in all cases.
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    Applied physics 29 (1982), S. 199-200 
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    Notes: Abstract Conditions are discussed under which an interstitial atom absorbed in the core of a gliding 60° dislocation belonging to the glide set can be transformed into an antisite defect. The mechanism considered may be responsible for an increase in the concentration of AsGa defects observed in GaAs single crystals after their plastic deformation.
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    Applied physics 28 (1982), S. 79-92 
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    Notes: Abstract The information available on the diffusion of oxygen and on the formation of thermal donors in silicon is critically reviewed. In this context the effects of intrinsic point defects on the diffusion-controlled growth of oxygen precipitates is investigated in some detail. Seemingly contradictory experimental results on the diffusivity of oxygen in silicon at temperatures around 400° C are explained in terms offast-diffusing gas-like molecular oxygen in silicon. The concept of molecular oxygen is also invoked in a newly suggested model of thermal donor formation in silicon. The diffusivity of molecular oxygen in silicon is estimated to be around 10−9cm2s−1 at 450° C, almost nine orders of magnitude higher than the diffusivity of atomic oxygen in interstitial position.
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