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  • Blank corrections
  • Dissolved organic carbon
  • Cambridge University Press  (3)
  • GFZ Data Services  (1)
  • Periodicals Archive Online (PAO)
  • 2020-2023  (4)
  • 1935-1939
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  • 1
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    Radiocarbon in dissolved organic carbon by UV oxidation: an update of procedures and blank characterization at NOSAMS (2022)
    Cambridge University Press
    Details
    Publication Date: 2022-10-26
    Description: © The Author(s), 2022. This article is distributed under the terms of the Creative Commons Attribution License. The definitive version was published in Xu, L., Roberts, M., Elder, K., Hansman, R., Gagnon, A., & Kurz, M. Radiocarbon in dissolved organic carbon by UV oxidation: an update of procedures and blank characterization at NOSAMS. Radiocarbon, 64(1), (2022): 195-199, https://doi.org/10.1017/rdc.2022.4.
    Description: This note describes improvements of UV oxidation method that is used to measure carbon isotopes of dissolved organic carbon (DOC) at the National Ocean Sciences Accelerator Mass Spectrometry Facility (NOSAMS). The procedural blank is reduced to 2.6 ± 0.6 μg C, with Fm of 0.42 ± 0.10 and δ13C of –28.43 ± 1.19‰. The throughput is improved from one sample per day to two samples per day.
    Description: We gratefully acknowledge support from the U.S. National Science Foundation, via NSF-OCE-1755125.
    Keywords: Blank ; Dissolved organic carbon ; Radiocarbon ; UV-oxidation
    Repository Name: Woods Hole Open Access Server
    Type: Article
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  • 2
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    Marine organic carbon and radiocarbon – present and future challenges (2022)
    Cambridge University Press
    Details
    Publication Date: 2022-10-26
    Description: © The Author(s), 2022. This article is distributed under the terms of the Creative Commons Attribution License. The definitive version was published in Druffel, E., Beaupre, S., Grotheer, H., Lewis, C., McNichol, A., Mollenhauer, G., & Walker, B. Marine organic carbon and radiocarbon – present and future challenges. Radiocarbon, (2022): 1-17, https://doi.org/10.1017/RDC.2021.105.
    Description: We discuss present and developing techniques for studying radiocarbon in marine organic carbon (C). Bulk DOC (dissolved organic C) Δ14C measurements reveal information about the cycling time and sources of DOC in the ocean, yet they are time consuming and need to be streamlined. To further elucidate the cycling of DOC, various fractions have been separated from bulk DOC, through solid phase extraction of DOC, and ultrafiltration of high and low molecular weight DOC. Research using 14C of DOC and particulate organic C separated into organic fractions revealed that the acid insoluble fraction is similar in 14C signature to that of the lipid fraction. Plans for utilizing this methodology are described. Studies using compound specific radiocarbon analyses to study the origin of biomarkers in the marine environment are reviewed and plans for the future are outlined. Development of ramped pyrolysis oxidation methods are discussed and scientific questions addressed. A modified elemental analysis (EA) combustion reactor is described that allows high particulate organic C sample throughput by direct coupling with the MIniCArbonDAtingSystem.
    Keywords: CSRA ; Dissolved organic carbon ; Methodology ; Organic carbon ; Radiocarbon
    Repository Name: Woods Hole Open Access Server
    Type: Article
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  • 3
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    Dissolved organic compounds in geothermal fluids used for energy production (2022)
    GFZ Data Services
    Details
    Publication Date: 2022-06-07
    Description: Abstract
    Description: This data was collected to write an extensive review on organic compounds in geothermal fluids as part of the REFLECT (Redefining geothermal fluid properties at extreme conditions to optimize future geothermal energy extraction). The data is mainly focussed on geothermal sites were organic compound data was reported in the literature. It includes data from the literature (Feldbusch, 2016; Vetter, 2012; Brehme et al., 2019; Westphal et al., 2019; Sanjuan et al., 2016) as well as own data that was analysed at the GFZ German Research Centre for Geosciences in section 3.2 (Organic Geochemistry). It comprises 130 samples from 19 different sites including DOC, organic acid anion as well as main inorganic anion concentrations, well depths, and reservoir temperatures of various geothermal sites in Europe. Due to confidentiality agreements Site names are all given in ID’s which are fully explained in the publication “Organic compounds in geothermal fluids – a review” when available. Sample ID’s are also given if the samples, both from the literature or own samples were measured at GFZ German Research Centre for Geosciences. This project has received funding from the European Union’s Horizon 2020 research and innovation programme under grant agreement nº 850626 (REFLECT).
    Keywords: Geothermal fluids ; Brine ; Dissolved organic matter ; Dissolved organic carbon ; Inhibitor ; EARTH SCIENCE 〉 SOLID EARTH 〉 GEOCHEMISTRY ; EARTH SCIENCE 〉 SOLID EARTH 〉 GEOCHEMISTRY 〉 GEOCHEMICAL PROPERTIES 〉 CHEMICAL CONCENTRATIONS ; EARTH SCIENCE 〉 SOLID EARTH 〉 GEOTHERMAL DYNAMICS 〉 GEOTHERMAL ENERGY
    Type: Dataset , Dataset
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  • 4
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    C-14 Blank Corrections for 25-100 mu G samples at the National Ocean Sciences AMS Laboratory (2020)
    Cambridge University Press
    Details
    Publication Date: 2022-10-26
    Description: © The Author(s), 2019. This article is distributed under the terms of the Creative Commons Attribution License. The definitive version was published in Roberts, Mark L., Elder, Kathryn L., Jenkins, William J., Gagnon, Alan R., Xu, Li, Hlavenka, Joshua D., & Longworth, Brett E. C-14 Blank Corrections for 25-100 mu G samples at the National Ocean Sciences AMS Laboratory. Radiocarbon, 61(5), (2019): 1403-1411, Doi: 10.1017/RDC.2019.74.
    Description: Replicate radiocarbon (14C) measurements of organic and inorganic control samples, with known Fraction Modern values in the range Fm = 0–1.5 and mass range 6 μg–2 mg carbon, are used to determine both the mass and radiocarbon content of the blank carbon introduced during sample processing and measurement in our laboratory. These data are used to model, separately for organic and inorganic samples, the blank contribution and subsequently “blank correct” measured unknowns in the mass range 25–100 μg. Data, formulas, and an assessment of the precision and accuracy of the blank correction are presented.
    Description: This work is supported by a Cooperative Agreement (OCE-1755125) with the U.S. National Science Foundation.
    Keywords: AMS ; AMS dating ; Blank corrections
    Repository Name: Woods Hole Open Access Server
    Type: Article
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