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  • Artikel  (44)
  • Column liquid chromatography  (26)
  • Wheat
  • Springer  (44)
  • Cell Press
  • International Union of Crystallography
  • 2020-2024
  • 2005-2009
  • 1985-1989
  • 1980-1984  (44)
  • 1984  (44)
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  • Artikel  (44)
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  • Springer  (44)
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  • 2020-2024
  • 2005-2009
  • 1985-1989
  • 1980-1984  (44)
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  • 1
    Digitale Medien
    Digitale Medien
    Springer
    Theoretical and applied genetics 67 (1984), S. 249-255 
    ISSN: 1432-2242
    Schlagwort(e): Wheat ; Plant regeneration ; Chromosome variation
    Quelle: Springer Online Journal Archives 1860-2000
    Thema: Biologie
    Notizen: Summary A cytological study has been made of plants regenerated from cultured immature embryos of four wheat cultivars (Triticum aestivum, 2n = 6x = 42). In total, 29% of the 192 plants examined were aneuploid with a range in chromosome numbers of 38–45. Evidence of chromosome structural changes was also found. This variation occurred in regenerants of all four cultivars, but there were large differences in the proportions of aneuploids arising from individual cultures which meant that no significant differences could be demonstrated between cultivars. Chromosome abnormalities were present in plants regenerated both from embryogenic cultures and from cultures in which the origin of shoots could not be distinctly defined.
    Materialart: Digitale Medien
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  • 2
    Digitale Medien
    Digitale Medien
    Springer
    Theoretical and applied genetics 67 (1984), S. 439-442 
    ISSN: 1432-2242
    Schlagwort(e): Wheat ; Multicellular pollen grains ; Embryos ; Cytology
    Quelle: Springer Online Journal Archives 1860-2000
    Thema: Biologie
    Notizen: Summary Cytological analysis of microspore embryogenesis during in vitro culture reveals a high mortality in the first week and a latency phase of about one week before the first embryogénic mitosis. Genotypic differences observed during our wheat anther culture do not seem to originate at the induction level but are linked to the different abortion rates.
    Materialart: Digitale Medien
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  • 3
    Digitale Medien
    Digitale Medien
    Springer
    Theoretical and applied genetics 67 (1984), S. 525-528 
    ISSN: 1432-2242
    Schlagwort(e): Cryopreservation ; Embryo culture ; Haploids ; Wheat ; Rice ; Germplasm bank
    Quelle: Springer Online Journal Archives 1860-2000
    Thema: Biologie
    Notizen: Summary Anther culture derived pollen embryos and immature zygotic embryos of wheat and rice, frozen in liquid nitrogen in the presence of dimethyl sulfoxide, sucrose and glycerol, have been revived. The retrieved cultures proliferated and/or regenerated shoots and plantlets. The prospects of the cryopreservation of embryos for the conservation and multiplication of germplasm and the possibility of the establishment of ‘Germplasm Banks’ are discussed.
    Materialart: Digitale Medien
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  • 4
    Digitale Medien
    Digitale Medien
    Springer
    Theoretical and applied genetics 68 (1984), S. 219-226 
    ISSN: 1432-2242
    Schlagwort(e): Hexaploid genotypes ; Allelic variation ; Esterase ; Isozymes ; Isoelectric focusing ; Wheat
    Quelle: Springer Online Journal Archives 1860-2000
    Thema: Biologie
    Notizen: Summary Analysis of grain esterase isozymes in Chinese Spring aneuploid genotypes by IEF confirmed that genes on the long arms of chromosomes 3A, 3B and 3D (Est-5) control the production of 19 isozymes. Allelic variants have been found for the isozyme pattern controlled by each chromosome. Segregational data involving null alleles and complex phenotypic differences indicate that the wheat grain esterases are encoded by three compound and probably homoeoallelic loci, each capable of producing at least six different isozymes. In a sample of 138 hexaploid genotypes, seven alleles were distinguished.
    Materialart: Digitale Medien
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  • 5
    ISSN: 1432-2242
    Schlagwort(e): Electrophoresis ; Endosperm ; Proteins ; Emmer ; Wheat
    Quelle: Springer Online Journal Archives 1860-2000
    Thema: Biologie
    Notizen: Summary Triticum turgidum L. var. dicoccoides (wild emmer) is an important genetic resource for increasing the protein content of common wheat (Triticum aestivum L.). Many studies have shown that the presence or absence of bands in sodium dodecyl sulfate polyacrylamide (SDS-PAGE) electrophoregrams of wheat storage proteins to be of a purely genetic character. A total protein extraction and SDS-PAGE technique was used to estimate the storage protein genetic variability among 841 accessions of wild emmer collected from various ecological regions in the Middle East. In addition, a computer data bank was developed, recording the onedimension electrophoregram bands for each accession by molecular weight (MW) and relative Coomassie Blue staining intensity as determined from densitometer scans. Analyses of this information are being used to identify specific accessions for further study by two dimension electrofocusing-electrophoresis and breeding and genetic analyses. The computer-assisted analyses indicated that the greatest genetic variability occurs for proteins in the high MW region (above 70,000 MW) followed by those in the medium range (70,000 to 33,300 MW). Comparatively little variability was revealed for protein subunits of below 33,300 MW.
    Materialart: Digitale Medien
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  • 6
    ISSN: 1432-2242
    Schlagwort(e): Chromosomal location ; Genetic control ; Salt soluble proteins ; Wheat ; Barley ; Rye
    Quelle: Springer Online Journal Archives 1860-2000
    Thema: Biologie
    Notizen: Summary Salt-soluble proteins from the endosperms of wheat, barley, and rye have been separated by nonequilibrium electrofocusing x electrophoresis. Genes encoding 14 of the 25 components observed in wheat have been unambiguously assigned to 10 different chromosomes (1B, 3B, 3D, 4A, 4D, 5B, 6B, 6D, 7B, 7D) by analysis of the compensated nulli-tetrasomic series. Five more wheat proteins seem to be controlled by group 2 chromosomes. Analysis of wheat-barley and wheat-rye addition lines has led to the location of genes for 6 out of 20 barley proteins in 4 different chromosomes (1H, 3H, 4H, 6H; 1H is homoeologous to group 7 chromosomes of wheat) and of genes for 5 out of 20 rye proteins in two different chromosomes (2R, 4R). The relationship between the proteins reported here and previously characterized ones is discussed.
    Materialart: Digitale Medien
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  • 7
    ISSN: 1432-2242
    Schlagwort(e): Wheat ; Triticum ; Grain protein ; Grain weight ; Maternal effect ; Cytoplasmic effect
    Quelle: Springer Online Journal Archives 1860-2000
    Thema: Biologie
    Notizen: Summary Reciprocal crosses were made between cultivated wheat (Triticum turgidum var. ‘durum’) and a high-protein line of wild tetraploid wheat (T. turgidum var. ‘dicoccoides’). F1 grains (on maternal spikes) were very similar to the selfed grains on the maternal parent in protein percentage, weight and protein content. These traits were also analyzed in F3 grains developed on F2 spikes of segregating populations derived from reciprocal crosses between the same cultivated parent and another high-protein line of var. ‘dicoccoides’. No significant differences in the mean values of these traits were found between the reciprocal crosses, indicating no cytoplasmic effect. It has been concluded that these grain characteristics are largely determined by the maternal plant.
    Materialart: Digitale Medien
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  • 8
    Digitale Medien
    Digitale Medien
    Springer
    Theoretical and applied genetics 68 (1984), S. 21-23 
    ISSN: 1432-2242
    Schlagwort(e): Wheat ; Heritability ; Yield ; Height
    Quelle: Springer Online Journal Archives 1860-2000
    Thema: Biologie
    Notizen: Summary Grain yield, plant height and test weight were studied in a population of winter wheat (Triticum aestivum L.). The population consisted of F2 bulk populations of 42 crosses among 11 genotypes adapted to S. W. Ontario. Heritabilities were: 0.30±0.32 for yield, 0.77±0.15 for height and 0.98±0.08 for test weight. Predicted genetic gain with 10% selection intensity was 0.15 t/ha for yield, 10.1 cm for height and 3.00 kg/hl for test weight. The low heritability for yield indicates that effective selection would require pedigree information and progeny tests, while the high heritabilities for height and test weight indicate that selection for these traits using single plots would be appropriate.
    Materialart: Digitale Medien
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  • 9
    Digitale Medien
    Digitale Medien
    Springer
    Chromatographia 18 (1984), S. 633-636 
    ISSN: 1612-1112
    Schlagwort(e): Column liquid chromatography ; Aromatic acid isomers ; Low capacity ion-exchange resin ; Microbore packed columns
    Quelle: Springer Online Journal Archives 1860-2000
    Thema: Chemie und Pharmazie
    Notizen: Summary A low-capacity, anion-exchange, porous-polymer resin was used as the packing material in a microbore column. Using a phosphate buffer containing various organic modifiers, retention behavior of substituted benzoic acid isomers with amino, chloro, methyl, nitro and carboxylic groups was investigated. The effect of ethanol, acetonitrile and sodium dodecylsulfate used as organic modifiers on the retention behavior at various eluent pH values was studies and optimum separations of the positional isomers reported.
    Materialart: Digitale Medien
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  • 10
    Digitale Medien
    Digitale Medien
    Springer
    Chromatographia 18 (1984), S. 668-672 
    ISSN: 1612-1112
    Schlagwort(e): Column liquid chromatography ; Mixed eluents ; Preferential sorption of eluents ; Pressure effects
    Quelle: Springer Online Journal Archives 1860-2000
    Thema: Chemie und Pharmazie
    Notizen: Summary Pronounced base line perturbations were repeatably observed in LC both in alternating recycling and in backflushing experiments when binary eluents and refractometric detectors were used. The perturbations which we call eigenzones appeared immediately after operating the recycling or the backflushing valve, and their size and shape depended on the nature of both the column filling and the mixed mobile phase as well as on the pressure drop across the column. Experimental results presented confirm that the primary causes of the eigenzones were the pressure changes in the columns which influenced the sorption equilibrium of mixed eluent components within the column packing. Some practical consequences of this effect are briefly discussed.
    Materialart: Digitale Medien
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  • 11
    Digitale Medien
    Digitale Medien
    Springer
    Chromatographia 18 (1984), S. 677-679 
    ISSN: 1612-1112
    Schlagwort(e): Polycyclic aromatic hydrocarbons ; Column liquid chromatography ; Polyphenyl bonded phases ; Retention and carbon content
    Quelle: Springer Online Journal Archives 1860-2000
    Thema: Chemie und Pharmazie
    Notizen: Summary The relationship between the retention of PAHs having various molecular sizes and the carbon contents (%) of bonded stationary phases with various types of ligands were investigated. The examined stationary phases were phenyl, diphenyl, triphenyl and benzyl-bonded silicas. The data indicated that sometimes it is not true that the retention of any solute relates linearly to the carbon content of the stationary phase. As the result, it is suggested that the pore size distribution of the silica support, the bulkiness of the ligand bonded to the silica and the molecular size of solute should also be considered before any precise statement can be made.
    Materialart: Digitale Medien
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  • 12
    Digitale Medien
    Digitale Medien
    Springer
    Chromatographia 18 (1984), S. 175-182 
    ISSN: 1612-1112
    Schlagwort(e): Column liquid chromatography ; Fourier transform IR ; Polar compounds ; Coal products
    Quelle: Springer Online Journal Archives 1860-2000
    Thema: Chemie und Pharmazie
    Notizen: Summary Fourier-transform infrared spectrometry (FTIR) was utilized as a detection system for high-performance liquid chromatography of polar compounds on a normal bonded-phase system. In addition to FTIR, UV (254 nm) and refractive index detection were employed in the separation of model compounds containing oxygen and nitrogen atoms in their molecules (phenols, alcohols, neutral and weakly basic nitrogen compounds). A polar amino-cyano (PAC) bonded-phase column was employed with a binary mobile phase (98:2 CDCl3:CH3CN). The separations and the information gained from each detector is discussed, including interactions between sample material and mobile phase. A polar fraction of a coal-derived product is also chromatographed under identical conditions. The results based on FTIR detection and chromatographic retention behavior suggest the exclusive presence of hindered and unhindered phenols.
    Materialart: Digitale Medien
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  • 13
    Digitale Medien
    Digitale Medien
    Springer
    Chromatographia 18 (1984), S. 211-215 
    ISSN: 1612-1112
    Schlagwort(e): Column liquid chromatography ; Alkylbenzenes ; PAHs ; Retention prediction ; Microcomputer
    Quelle: Springer Online Journal Archives 1860-2000
    Thema: Chemie und Pharmazie
    Notizen: Summary The microcomputer-assisted retention prediction system in C18 reversed-phase HPLC is described. The system is based on the use of the hydrophobic parameter and the correlation factor of alkylbenzenes and polycyclic aromatic hydrocarbons (PAHs) which are highly correlated to their retention in reversed-phase HPLC. The system is evaluated by comparing the retention data between measured and predicted values. One of the typical examples applied for PAH analysis in the extracts of diesel particulate matter shows the high potential of the system investigated.
    Materialart: Digitale Medien
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  • 14
    Digitale Medien
    Digitale Medien
    Springer
    Chromatographia 18 (1984), S. 216-220 
    ISSN: 1612-1112
    Schlagwort(e): Cation exchangers ; Column liquid chromatography ; Exchange capacity, determination ; Organic peroxidation
    Quelle: Springer Online Journal Archives 1860-2000
    Thema: Chemie und Pharmazie
    Notizen: Summary Two oxidation procedures for the synthesis of silicabased aliphatic sulfonic acid cation-exchangers for HPLC are described. Several reaction conditions for oxidizing a terminal-bonded thiol with organic peroxides are provided along with their yields, capacities, reproducibility, and chromatographic behavior. Also, three methods for determining exchange capacity are discussed, and their relationship to the capacity factors of charged solutes is compared. The maximum capacity determined by the titration of the bonded silica was 0.34 meq/gram. The general problems of synthesizing cation-exchangers, measuring their efficiencies and exchange capacities, and evaluating their overall performances are outlined.
    Materialart: Digitale Medien
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  • 15
    Digitale Medien
    Digitale Medien
    Springer
    Chromatographia 18 (1984), S. 369-373 
    ISSN: 1612-1112
    Schlagwort(e): Column liquid chromatography ; Ion exchange ; dynamic ; Metal ions ; Equilibria effects
    Quelle: Springer Online Journal Archives 1860-2000
    Thema: Chemie und Pharmazie
    Notizen: Summary Equilibria occurring during the dynamic ion exchange separation of metal ions were examined, and their effect on the chromatography of the metal ions was evaluated. Bonded reversed-phase silica, pure organic reversed phase, and silica columns were used to differentiate between the role of silica and the reverse phase. The results show that system peaks had the most important influence on the applicability of dynamic exchangers to quantitative metal ion determinations. The response of system peaks to sample composition (pH, ionic strength, matrix effects) was complicated and could not be predicted easily. Equilibria effects that can cause analytical errors were identified and recommendations for elimination of such errors are given.
    Materialart: Digitale Medien
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  • 16
    ISSN: 1612-1112
    Schlagwort(e): Column liquid chromatography ; Amines ; Phenols ; Fourier transform I.R.
    Quelle: Springer Online Journal Archives 1860-2000
    Thema: Chemie und Pharmazie
    Notizen: Summary Several chromatographic parameters have been examined as to their effect on detectability for microbore high-performance liquid chromatography coupled with Fourier-transform infrared spectrometry. Detection limits for several compound classes are presented as amount injected. Improvements in detectability for this technique are discussed.
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  • 17
    ISSN: 1612-1112
    Schlagwort(e): Column liquid chromatography ; Polystyrene packings ; Pre-column derivatization ; Thiamine compounds ; UV and fluorescence detection
    Quelle: Springer Online Journal Archives 1860-2000
    Thema: Chemie und Pharmazie
    Notizen: Summary The chromatography of thiochrome and related phosphate esters was studied on two different polystyrene packing materials. The adsorbents were compared with respect to capacity factors, plate heights and resolution factors measured with different mixtures of phosphate buffer (pH 8.5) and methanol. In contrast with derivatized silica, these phases were found to be stable using an alkaline mobile phase and sample. Fast separations were possible with good peak symmetry at all organic modifier concentrations.
    Materialart: Digitale Medien
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  • 18
    Digitale Medien
    Digitale Medien
    Springer
    Chromatographia 18 (1984), S. 445-448 
    ISSN: 1612-1112
    Schlagwort(e): Column liquid chromatography ; Amino-bonded stationary phase ; Ion-exchange ; Fermentation solution ; Biomass
    Quelle: Springer Online Journal Archives 1860-2000
    Thema: Chemie und Pharmazie
    Notizen: Summary In this work the analytical separation of biomass hydrolysis and fermentation products is described. Aminobonded phase and ion exchange materials (HPX 87H, HPX 42A, μ Spherogel Carbohydrate) were used as HPLC stationary phases for the determination of monomeric and oligomeric carbohydrates, carbohydrate degradation and fermentation products. The HPX 42A and the amino-bonded phase columns are especially suitable for the analysis of the gluco oligomers. The HPX 87H column separates the monomeric sugars and their degradation and fermentation products (e.g. furfurals and ethanol) very well. Using the μ Spherogel Carbohydrate column the lower gluco-oligomers as well as the monomeric sugars and their degradation and fermentation products, can be determined within 35 minutes.
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  • 19
    ISSN: 1612-1112
    Schlagwort(e): Column liquid chromatography ; Chiral bonded phase ; Racemate resolution
    Quelle: Springer Online Journal Archives 1860-2000
    Thema: Chemie und Pharmazie
    Notizen: Summary A chiral stationary phase with an immobilized, optically active diamine was prepared for the separation of enantiomers. The synthesis of the phase was carried out by bonding (−)trans-1,2-cyclohexanediamine to microparticulate silica gel through the coupling agent 3-glycidoxypropylsilane. The resolution of the racemic compounds catechin, 2,2′-dihydroxy-1,1′binaphthyl and trans-1,2-cyclohexandiol, is reported.
    Materialart: Digitale Medien
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  • 20
    Digitale Medien
    Digitale Medien
    Springer
    Chromatographia 18 (1984), S. 495-498 
    ISSN: 1612-1112
    Schlagwort(e): Column liquid chromatography ; PAHs ; Molecular shape recognition
    Quelle: Springer Online Journal Archives 1860-2000
    Thema: Chemie und Pharmazie
    Notizen: Summary The molecular-shape recognition of polycyclic aromatic hydrocarbons has been studied on various stationary phases in reversed-phase high-performance liquid chromatography. The examined stationary phases were phenyl-, diphenyl-, triphenyl- and benzyl-bonded silicas. The results of regression analysis inidcated that triphenylsilica is the best packing material to recognize the difference in the molecular-shape of structural isomers. This fact was confirmed by the separation of 4-ring isomers.
    Materialart: Digitale Medien
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  • 21
    ISSN: 1612-1112
    Schlagwort(e): Column liquid chromatography ; Retention data ; Substituted benzene derivatives ; Correlations
    Quelle: Springer Online Journal Archives 1860-2000
    Thema: Chemie und Pharmazie
    Notizen: Summary The capacity factors of substituted benzene derivatives on bonded phases of various chain lengths in the reversed-phase mode have been measured and correlation of retention data between four stationary phases has been investigated by linear regression analysis. As a result, a difference in the retention mechanism between phases of shorter chain length and octadecylsilica was observed. In addition, it is also apparent that the multicombination treatment between retention data and descriptors such as π, HA, HD and σ promises the possibility of predicting the retention of substituted benzene derivatives on various reversed-phase stationary phases.
    Materialart: Digitale Medien
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  • 22
    Digitale Medien
    Digitale Medien
    Springer
    Chromatographia 18 (1984), S. 525-527 
    ISSN: 1612-1112
    Schlagwort(e): Column liquid chromatography ; Polyamines ; Dansyl derivatives ; Peak compression
    Quelle: Springer Online Journal Archives 1860-2000
    Thema: Chemie und Pharmazie
    Notizen: Summary Analytical conditions for the high-speed, reversed-phase, liquid chromatographic of a diamine (putrescine) and polyamines (spermine and spermidine) were determined. Various elution modes were employed using the same mobile phase constituents: 20mM sodium heptane sulfonate and 20mM acetic acid as solvent A and, pure acetonitrile as solvent B. Samples were derivatized with dansyl chloride before injection. Under isocratic conditions, the separation of the three polyamines was achieved in 7 min. The use of a linear elution gradient led to the same analytical time but with a better resolution of the putrescine peak from non-polyamine frontal peaks. For these measurements, the sample size was 5μl. This volume was increased to 20μl and the use of a steep gradient combined with the peak-compression technique allowed a fast analysis in 2–3 minutes, which may be compared with a 30 min run time necessary when a conventional column is used.
    Materialart: Digitale Medien
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  • 23
    Digitale Medien
    Digitale Medien
    Springer
    Plant and soil 77 (1984), S. 381-385 
    ISSN: 1573-5036
    Schlagwort(e): 14C-labelled plant material ; 14C-labelled soil ; Root exudation ; Sample oxidizer ; Scintillation counting ; Sutton series soil ; Tissue solubilization ; Wheat
    Quelle: Springer Online Journal Archives 1860-2000
    Thema: Land- und Forstwirtschaft, Gartenbau, Fischereiwirtschaft, Hauswirtschaft
    Notizen: Summary A comparison between a tissue solubilization method and a sample oxidizer technique to measure14C in plant and soil material is described. The solubilization method although not quantitative gives good recoveries and reproducible values of14C-content with soil samples not exceeding 10 mg and should be of value for estimating the14C-content of soils in laboratories without a sample oxidizer.
    Materialart: Digitale Medien
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  • 24
    Digitale Medien
    Digitale Medien
    Springer
    Plant and soil 77 (1984), S. 141-149 
    ISSN: 1573-5036
    Schlagwort(e): Cracks ; Crack width ; Lateral roots ; Pea ; Penetration ; Penetrometer ; Rape ; Remoulded soil ; Roots ; Safflower ; Seminal axes ; Soil strength ; Undisturbed soil ; Wheat
    Quelle: Springer Online Journal Archives 1860-2000
    Thema: Land- und Forstwirtschaft, Gartenbau, Fischereiwirtschaft, Hauswirtschaft
    Notizen: Summary Experimental methods are described for observing the behaviour of roots encountering cracks in soil. The proportions of roots which enter a second soil block after crossing a crack of known width were measured. Soil strength was measured with a penetrometer. Results are presented for the proportions of seminal roots of wheat and primary lateral roots of pea which enter moulded soil of various strengths after crossing cracks. Results are also presented for the proportions of seminal roots of pea, rape and safflower which enter undisturbed soil after crossing cracks. It was found that, in all cases, the proportion of roots penetrating the second soil block decreased with increasing crack width and increasing soil strength. Also, a smaller proportion of thinner roots penetrated the second soil block than thicker roots under similar conditions. Root diameter in the cracks was influenced by both crack width and soil strength, and an empirical equation is presented to describe this effect.
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  • 25
    ISSN: 1573-5036
    Schlagwort(e): Ammonium acetate extractable potassium ; Inceptisol soil ; Minimum level ; Non-exchangeable potassium ; Pearl millet ; Wheat
    Quelle: Springer Online Journal Archives 1860-2000
    Thema: Land- und Forstwirtschaft, Gartenbau, Fischereiwirtschaft, Hauswirtschaft
    Notizen: Summary Ammonium acetate extractable potassium in the soil reached a minimum value of 6.8 mg K/100g soil after 14 crops of wheat and pearl millet in the field without applying any potassium fertilizer. At this level of ammonium acetate extractable K both wheat and pearl millet utilized about, 90 per cent of the total K from non-exchangeable sources. Wheat and pearl millet were grown in this soil in the greenhouse at different levels of K. At K0 level wheat utilized 86 per cent of the total K uptake from the non-exchangeable source and pearl millet, 95 per cent. At K1 level, wheat utilized only 19 per cent but at higher levels of K, there was build up in the K status of soils. In the case of pearl millet at K1, K2 and K3 levels 59, 13 and 22 per cent of total uptake were contributed by non-exchangeable forms. The total K uptake by pearl millet was more than double that by wheat. Plant analysis showed that 83 per cent of the total K in wheat was contained in the shoot portion and the rest in the roots. The corresponding figures for pearl millet were 94 and 6 per cent.
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  • 26
    Digitale Medien
    Digitale Medien
    Springer
    Plant and soil 79 (1984), S. 249-254 
    ISSN: 1573-5036
    Schlagwort(e): Acid KMnO4 extraction ; Chemical index ; Incubation ; Mineralizable N ; Mineral N ; N uptake ; Soil ; Wheat
    Quelle: Springer Online Journal Archives 1860-2000
    Thema: Land- und Forstwirtschaft, Gartenbau, Fischereiwirtschaft, Hauswirtschaft
    Notizen: Summary A chemical measure of soil nitrogen (N) availability has been evaluated. The method involved the estimation of initial mineral N, plus mineralizable N released with 0.05N KMnO4 in 1NH2SO4. The results obtained correlated highly significantly with the N uptake by wheat plants (r=0.72,P〈0.01).
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  • 27
    Digitale Medien
    Digitale Medien
    Springer
    Plant and soil 76 (1984), S. 379-387 
    ISSN: 1573-5036
    Schlagwort(e): Actinomycetes ; Bacteria ; Chernozemic soil ; Fungi ; Rhizosphere ; Trifluralin herbicide ; Wheat
    Quelle: Springer Online Journal Archives 1860-2000
    Thema: Land- und Forstwirtschaft, Gartenbau, Fischereiwirtschaft, Hauswirtschaft
    Notizen: Summary This study examined the effects of trifluralin (α,α,α-trifluoro-2,6-dinitro-N,N-dipropyl-p-toluidine), a soil incorporated herbicide, on soil microflora both in the general soil environment and in the rhizosphere of trifluralin damaged wheat roots. Two Dark Brown Chernozemic soils were treated with various trifluralin rates in the growth chamber and wheat [Triticum aestivum L. ‘Neepawa’] was seeded. Trifluralin generally had no effect on fungi, bacteria, or actinomycete populations in either the general soil or in the rhizosphere. CO2 evolution was unchanged when trifluralin was added to the soil. In wheat plots, at two field locations, there were no significant effects of trifluralin (1.0 kg ha−1) on soil fungi, bacteria, actinomycete, denitrifying bacteria, and nitrifying Nitrobacter propulations. A pure culture study with 42 soil microorganisms showed that many isolates were inhibited at 400 to 100,000 μg g−1 but not at concentrations 〈16 μg g−1. Similar data were obtained from tests on four different soils. These studies indicate that trifluralin is unlikely to cause changes in the numbers of soil microorganisms when used at recommended levels.
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  • 28
    Digitale Medien
    Digitale Medien
    Springer
    Plant and soil 78 (1984), S. 417-428 
    ISSN: 1573-5036
    Schlagwort(e): Aphelenchoides spp ; Aphelenchus avenae ; Pinus radiata ; Soil fungi ; Wheat
    Quelle: Springer Online Journal Archives 1860-2000
    Thema: Land- und Forstwirtschaft, Gartenbau, Fischereiwirtschaft, Hauswirtschaft
    Notizen: Summary The soils of a wheat-field and pine-forest had different mycofloras and supported different populations ofAphelenchus avenae, a mycophagous nematode. The abundance ofA. avenae was correlated with the composition of the mycoflora in these soils; the greater abundance ofA. avenae in wheat-field soil being associated with a more diverse mycoflora.
    Materialart: Digitale Medien
    Standort Signatur Erwartet Verfügbarkeit
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  • 29
    Digitale Medien
    Digitale Medien
    Springer
    Plant and soil 79 (1984), S. 11-28 
    ISSN: 1573-5036
    Schlagwort(e): Beta distribution ; Buckling ; Cracks ; Crack width ; Lateral roots ; Pea ; Penetration ; Penetrometer ; Rape ; Remoulded soil ; Roots ; Safflower ; Seminal axes ; Soil strength ; Undisturbed soil ; Wheat
    Quelle: Springer Online Journal Archives 1860-2000
    Thema: Land- und Forstwirtschaft, Gartenbau, Fischereiwirtschaft, Hauswirtschaft
    Notizen: Summary It is shown that probabilities of root penetration across cracks in soil can be calculated effectively using a mathematical model involving root stress and soil distributions and penetrometer/root stress ratios. Penetration criteria are developed, and it is found that the effective penetrometer/root stress ratios take values of about 4 for crack widths smaller than about 2 mm and about 8 for wider cracks. Root swelling does not appear to contribute significantly to the probability of root penetration through any effect on root buckling stress. Suggestions are made for further work on the effects of soil structure and strength on root behaviour.
    Materialart: Digitale Medien
    Standort Signatur Erwartet Verfügbarkeit
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  • 30
    Digitale Medien
    Digitale Medien
    Springer
    Nutrient cycling in agroecosystems 5 (1984), S. 285-288 
    ISSN: 1573-0867
    Schlagwort(e): Wheat ; potassium chloride ; irrigation ; plant water potential
    Quelle: Springer Online Journal Archives 1860-2000
    Thema: Land- und Forstwirtschaft, Gartenbau, Fischereiwirtschaft, Hauswirtschaft
    Notizen: Abstract ‘The water potential of wheat plants increased during the mid-day noon, probably as an adaptation; the rise was greater with less frequent irrigation and was increased by KCl application.’
    Materialart: Digitale Medien
    Standort Signatur Erwartet Verfügbarkeit
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  • 31
    Digitale Medien
    Digitale Medien
    Springer
    Plant and soil 80 (1984), S. 135-138 
    ISSN: 1573-5036
    Schlagwort(e): Hardpans ; Root growth ; Soil compaction ; Subterranean clover ; Wheat
    Quelle: Springer Online Journal Archives 1860-2000
    Thema: Land- und Forstwirtschaft, Gartenbau, Fischereiwirtschaft, Hauswirtschaft
    Notizen: Summary Wheat crops with stunted chlorotic patches are widespread in northern Victoria, Australia, and are often associated with dense, compacted layers of soil. Poor growth of subterranean clover, with symptoms of cupped and reddened leaflets, is also a problem in these cropping regions during the pasture phase of the rotation. Artificially compacted soils were created to test the hypothesis that these symptoms of poor growth were caused by soil compaction. Soil compacted from 0–20 cm with a bulk density similar to that measured in problem fields reproduced these symptoms in wheat and subterranean clover. Surface compaction alone also reproduced the symptoms in clover.
    Materialart: Digitale Medien
    Standort Signatur Erwartet Verfügbarkeit
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  • 32
    ISSN: 1573-5036
    Schlagwort(e): Azospirillum brasilense ; Wheat ; Triticum aestivum ; N-fertilizer
    Quelle: Springer Online Journal Archives 1860-2000
    Thema: Land- und Forstwirtschaft, Gartenbau, Fischereiwirtschaft, Hauswirtschaft
    Notizen: Summary The yield response of a common spring wheat cultivar,Triticum aestivum, to inoculation withAzospirillum brasilense was studied at four levels of N fertilization. Plant yield increased due to the inoculation treatment only at medium and high levels of N fertilization, with a maximum yield increase of about 8.0 per cent at the highest level (approximately 1.0 g of pure N per plant). Yield increase was mostly due to an increase in the number of grains per spike, and at the highest level of fertilization, also due to a higher number of spikes per plant. At all N levels, the inoculation caused an increase of 0.5–1.4 per cent in the number of fertile spikelets per main spike. Grain protein percentage was unaffected by the inoculation, though significantly increase due to the fertilization treatments. The occurrence of maximum yield response at the highest N level, the response by early-determined yield components, i.e. spikelet number, and the unaffected grain protein content are in accord with the suggestion that the contribution ofAzospirillum brasilense to wheat yield is not through N2-fixation.
    Materialart: Digitale Medien
    Standort Signatur Erwartet Verfügbarkeit
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  • 33
    Digitale Medien
    Digitale Medien
    Springer
    Chromatographia 18 (1984), S. 574-578 
    ISSN: 1612-1112
    Schlagwort(e): Column liquid chromatography ; Microbore column ; Flow rate stability ; Performance ; Quantitative analysis
    Quelle: Springer Online Journal Archives 1860-2000
    Thema: Chemie und Pharmazie
    Notizen: Summary Some quantitative implications of the use of microbore columns in column liquid chromatography are investigated. Although for several pumps the flow rate stability at 50 μl min−1 is slightly worse than that of pumps operating at 1 ml min−1, the quantitative performance with respect to repeatability and reproducibility of response factors equals that of conventional liquid chromatography. Thermostatting is strongly recommended for microbore column operation.
    Materialart: Digitale Medien
    Standort Signatur Erwartet Verfügbarkeit
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  • 34
    Digitale Medien
    Digitale Medien
    Springer
    Chromatographia 18 (1984), S. 62-64 
    ISSN: 1612-1112
    Schlagwort(e): Column liquid chromatography ; Reversed phase ; Microparticulate packing ; Amino acids
    Quelle: Springer Online Journal Archives 1860-2000
    Thema: Chemie und Pharmazie
    Notizen: Abstract A procedure is described by which 20 commonly occurring amino acids may be separated by reversed-phase liquid chromatography at room temperature in a total time, including derivatisation with o-phthalaldehyde/2-mercaptoethanol reagent, of approximately 15 minutes. Further, an increase in column temperature enables increased resolution of certain amino acids to be obtained with small but acceptable losses in fluorescence intensity. The only major drawback to the method is that the derivatisation reagent does not react with proline or hydroxyproline.
    Materialart: Digitale Medien
    Standort Signatur Erwartet Verfügbarkeit
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  • 35
    Digitale Medien
    Digitale Medien
    Springer
    Chromatographia 18 (1984), S. 15-17 
    ISSN: 1612-1112
    Schlagwort(e): Column liquid chromatography ; Ion-pair ; Dynamic equillibrium ; Aqueous and aqueous alcohol eluents
    Quelle: Springer Online Journal Archives 1860-2000
    Thema: Chemie und Pharmazie
    Notizen: Summary This work describes the dynamic equilibrium of an ionpair, reverse-phase liquid chromatography system. A given adsorbed quantity of an anionic surfactant can lead to different capacity factors and selectivity for anionic solutes.
    Materialart: Digitale Medien
    Standort Signatur Erwartet Verfügbarkeit
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  • 36
    ISSN: 1612-1112
    Schlagwort(e): Column liquid chromatography ; Retention correlation ; Silica ; Normal and reversed phase
    Quelle: Springer Online Journal Archives 1860-2000
    Thema: Chemie und Pharmazie
    Notizen: Summary The correlation between the retention data of polyaromatic hydrocarbons (PAH) obtained in normal-and reversed-phase liquid chromatography is investigated in order to determine the dominant factors controlling the retention. It is clear that the separation of PAHs on various chemically-bonded packing materials in normal- and/or reversed-phase modes is primarily controlled by the molecular structure and shape. The π-electron interaction between the solute and the stationary phase also contributes to the retention, although pure silica shows a somewhat different behavior.
    Materialart: Digitale Medien
    Standort Signatur Erwartet Verfügbarkeit
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  • 37
    Digitale Medien
    Digitale Medien
    Springer
    Chromatographia 18 (1984), S. 600-602 
    ISSN: 1612-1112
    Schlagwort(e): Column liquid chromatography ; Sugars ; Copper (II) complex ; UV detection
    Quelle: Springer Online Journal Archives 1860-2000
    Thema: Chemie und Pharmazie
    Notizen: Summary A sensitive method of sugar analysis by HPLC is described in which a copper (II) modified silica gel as stationary phase is used. Detection is based on UV absorption of a complex formed between the sugar, copper, and ammonia.
    Materialart: Digitale Medien
    Standort Signatur Erwartet Verfügbarkeit
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  • 38
    Digitale Medien
    Digitale Medien
    Springer
    Chromatographia 18 (1984), S. 695-697 
    ISSN: 1612-1112
    Schlagwort(e): Column liquid chromatography ; Semi-microbore columns ; Reverse-phase ; 3 μm packing
    Quelle: Springer Online Journal Archives 1860-2000
    Thema: Chemie und Pharmazie
    Notizen: Summary The preparation and use of semi-microbore (2mm i.d.), reverse-phase columns in HPLC has been investigated and they have been compared with 5 mm bore analytical columns. Injection valve design, detector cell volume, column loading and column linking are considered for both semi-microbore and analytical systems. Mobile phase flow-rate, detector time constant and column lifetime are also evaluated for small-bore systems.
    Materialart: Digitale Medien
    Standort Signatur Erwartet Verfügbarkeit
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  • 39
    ISSN: 1612-1112
    Schlagwort(e): Column liquid chromatography ; Quantitative determination of L-alanine ; DABS-Cl ; Tryglycine sulphate
    Quelle: Springer Online Journal Archives 1860-2000
    Thema: Chemie und Pharmazie
    Notizen: Summary A method for the quantitative determination of L-alanine in triglycine sulphate crystals, in the presence of excess amounts of glycine, is described. L-alanine is determined after derivatization with 4-N,N-dimethyl-aminoazobenzene-4′-sulfonyl chloride (DABS-Cl) and in the presence of DABS-valine used as the internal standard. The results obtained indicate that the method permits the determination of alanine in triglycine sulphate crystals at concentrations of about 1%.
    Materialart: Digitale Medien
    Standort Signatur Erwartet Verfügbarkeit
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  • 40
    Digitale Medien
    Digitale Medien
    Springer
    Chromatographia 18 (1984), S. 73-80 
    ISSN: 1612-1112
    Schlagwort(e): Column liquid chromatography ; Microbore columns ; Performance ; High-speed separation
    Quelle: Springer Online Journal Archives 1860-2000
    Thema: Chemie und Pharmazie
    Notizen: Summary Microbore columns of 1 mm i.d. have turned out to be very suitable for the achievement of efficient columns. The packing procedure for stainless steel 1 mm i.d. columns from 5 to 100 cm in length was studied. Stationary phases used were: pure silica gel, octyl, octadecyl and amino bonded silicas. The main parameters (slurry composition, packing system, choice of materials) are discussed. Short columns packed with 3 or 5μm particles allow high speed separations. A separation in 18 seconds is described. Very high plate numbers can be obtained with long columns. With 7–8μm particles, a 1 m column can produce 50,000 plates (h=3). Columns can be joined without loss of efficiency. 270 000 theoretical plates were obtained on a 6 m adsorption column with a test mixture. In reversed-phase chromatography, bile acid sodium salts can be separated on a 1 m column. In adsorption chromatography, details are given of the separation of a polystyrene oligomer sample, as well as a light and a heavy petroleum distillate samples on a 2 m column with refractive index detection in the last-case.
    Materialart: Digitale Medien
    Standort Signatur Erwartet Verfügbarkeit
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  • 41
    Digitale Medien
    Digitale Medien
    Springer
    Chromatographia 18 (1984), S. 84-86 
    ISSN: 1612-1112
    Schlagwort(e): Column liquid chromatography ; Reversed phase ; Stationary phase evaluation
    Quelle: Springer Online Journal Archives 1860-2000
    Thema: Chemie und Pharmazie
    Notizen: Summary For the evaluation of reversed phase packing materials a mixture of acetylacetone, I-nitronaphthalene and naphthalene is proposed. This will reveal the usual optimum kinetic chromatographic parameters (the naphthalene peak), the degree of activity or endcapping status of the column (the ratio of the I-nitronaphthalene and naphthalene retention times) and trace metal activity (the shape and intensity of the acetylacetone peak).
    Materialart: Digitale Medien
    Standort Signatur Erwartet Verfügbarkeit
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  • 42
    Digitale Medien
    Digitale Medien
    Springer
    Chromatographia 18 (1984), S. 81-83 
    ISSN: 1612-1112
    Schlagwort(e): Column liquid chromatography ; Bonded phases ; Characterisation ; Toxicological screening
    Quelle: Springer Online Journal Archives 1860-2000
    Thema: Chemie und Pharmazie
    Notizen: Summary This paper describes a test (“DMD-test”) to determine chromatographic properties of C8- or C18-bonded phases. The test was developed to select HPLC columns, for clinical and forensic toxicological screening in particular. The three compounds for the DMD-test are: diphenhydramine, 5-(p-methylphenyl)-5-phenylhydantoin (=MPPH) and diazepam. The isocratic mobile phase (acetonitrile/buffer pH2.3) is suitable for analysis of biological samples. 24 commercially available columns were tested. From our work this test enables the selection of commercial HPLC columns with reproducible properties. In this way a reference LC retention list can be developed to identify analytical results on an inter- or intralaboratory basis.
    Materialart: Digitale Medien
    Standort Signatur Erwartet Verfügbarkeit
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  • 43
    Digitale Medien
    Digitale Medien
    Springer
    Chromatographia 18 (1984), S. 90-95 
    ISSN: 1612-1112
    Schlagwort(e): Column liquid chromatography ; Reversed phase ; Retention prediction ; Substituted benzenes ; Molecular parameters
    Quelle: Springer Online Journal Archives 1860-2000
    Thema: Chemie und Pharmazie
    Notizen: Summary The separation of substituted benzene derivaties on a reversed-phase C-18 column has been examined. The correlations between the logarithm of the capacity factor and several descriptors indicating the molecular size, shape and the physical properties of a solute were determined. The results indicated that hydrophobicity is the dominant factor to control the retention of substituted benzenes. Their retention in reversed-phase HPLC can be predicted with help of the equations derived by multicombination of the parameters.
    Materialart: Digitale Medien
    Standort Signatur Erwartet Verfügbarkeit
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  • 44
    ISSN: 1612-1112
    Schlagwort(e): Aldehydes and ketones ; 2,4-dinitrophenylhydrazine-coated silica gel ; Gas chromatography ; Column liquid chromatography ; Pollution
    Quelle: Springer Online Journal Archives 1860-2000
    Thema: Chemie und Pharmazie
    Notizen: Summary After a brief review of several methods described in the literature this paper discusses air-sampling on 2,4-dinitrophenylhydrazine-coated silica gel and identification requirements for aldehydes and ketones most commonly found in industrial pollution. Quantitative analysis of formaldehyde and acetaldehyde either by GC or by HPLC techniques is established using a dynamic system producing test atmospheres and compared with the usual colorimetric determinations.
    Materialart: Digitale Medien
    Standort Signatur Erwartet Verfügbarkeit
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