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  • Chemistry  (32)
  • 1980-1984  (19)
  • 1975-1979  (13)
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  • 1
    Electronic Resource
    Electronic Resource
    Darstellung und Kristallstruktur von KSbS2 (1975)
    Weinheim : Wiley-Blackwell
    Zeitschrift für anorganische Chemie 414 (1975), S. 211-219 
    Details
    ISSN: 0044-2313
    Keywords: Chemistry ; Inorganic Chemistry
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology
    Description / Table of Contents: Preparation and Crystal Structure of KSbS2Red KSbS2 was prepared in a aqueous solution of KHS and Sb2S3 under mild hydrothermal conditions. For crystallographic data see „Inhaltsübersicht“. There are SbS2--chains, built up by ψ-trigonal bipyramids, which are connected by sharing edges. The K+-Ions between these chains have a nearly octaedric coordination.
    Notes: Rotes KSbS2 wurde aus wässerigen Lösungen von KHS und Sb2S3 unter milden hydrothermalen Bedingungen dargestellt und strukturell untersucht. Die kristallographischen Daten sind: monoklin, Raumgruppe C2/c—C2h6 a = 8,75 ± 0,01 Å, b = 8,98 ± 0,01 Å, c = 6,84 ± 0,01 Å β = 121,6° ± 0,1 4 Formeleinheiten in der Elementarzelle. Nach der vollständigen röntgenographischen Strukturaufklärung liegen SbS2--Kettenanionen vor, die aus über Kanten verknüpften ψ-trigonalen Bipyramiden aufgebaut sind. Zwischen diesen Ketten sitzen die Kaliumionen mit einer nahezu oktaedrischen Koordination.
    Additional Material: 5 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/zaac.19754140304
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  • 2
    Electronic Resource
    Electronic Resource
    Darstellung und Kristallstruktur von (NH4)2Sb4S7 (1977)
    Weinheim : Wiley-Blackwell
    Zeitschrift für anorganische Chemie 437 (1977), S. 183-187 
    Details
    ISSN: 0044-2313
    Keywords: Chemistry ; Inorganic Chemistry
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology
    Description / Table of Contents: Preparation and Crystal Structure of (NH4)2Sb4S7(NH4)2Sb4S7 has been prepared and its structure determined. It crystallizes orthorhombic, space group Pbca, with \documentclass{article}\pagestyle{empty}\begin{document}$$ {\rm a = 1 133}{\rm .0(3) pm, b = 2625}{\rm .2(6) pm, c = 994}{\rm .0(3) pm}{\rm .} $$\end{document} Three distorted trigonal SbS3-pyramids are connected to a Sb3S3-ring in chair-conformation. These rings are bridged by further SbS3-pyramids to infinite chiralic chains.
    Notes: (NH4)2Sb4S7 wurde dargestellt und strukturell aufgeklärt. Es kristallisiert orthorhombisch, Raumgruppe Pbca, mit \documentclass{article}\pagestyle{empty}\begin{document}$$ {\rm a = 1 133,0(3) pm, b = 2625,2(6) pm, c = 994,0(3) pm}{\rm .} $$\end{document} Im Anionengitter sind jeweils 3 verzerrte trigonale SbS3-Pyramiden zu Sb3S3-Sechsringen in Sesselkonformation verknüpft. Diese Ringe sind über weitere SbS3-Pyramiden zu eindimensional unendlichen gewundenen Ketten verbunden.
    Additional Material: 3 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/zaac.19774370125
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  • 3
    Electronic Resource
    Electronic Resource
    Darstellung und Kristallstruktur von Cs2Sb4S7 (1978)
    Weinheim : Wiley-Blackwell
    Zeitschrift für anorganische Chemie 441 (1978), S. 98-102 
    Details
    ISSN: 0044-2313
    Keywords: Chemistry ; Inorganic Chemistry
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology
    Description / Table of Contents: Preparation and Crystal Structure of Cs2Sb4S7The first thioantimonite of Cesium has been synthesized and its crystal structure determined. The substance crystallizes monoclinic with spacegroup P21/c. The lattice constants are a = 1111.2(5) pm, b = 1227.1(5) pm, c = 1163.7(5) pm and ß = 97.60(5)°. There are four formula units in the unit cell. Sb-S chains are formed by trigonal SbS3 pyramids and ψ-trigonal SbS4 bipyramids.
    Notes: Als erstes Cäsiumthioantimonit wurde die Verbindung Cs2Sb4S7 aus wäßriger Sulfidlösung dargestellt und ihre Kristallstruktur aufgeklärt. Sie kristallisiert monoklin in der Raumgruppe P21/c mit den Gitterkonstanten: a = 1111,2(5) pm. b = 1227,1(5) pm, c = 1163,7(5) pm, ß = 97,60(5)°. Die Elementarzelle enthält 4 Formeleinheiten. Es liegen Sb-S-Kettenverbände vor, die aus trigonalen SbS3-Pyramiden und ψ-trigonalen SbS4-Bipyramiden gebildet werden.
    Additional Material: 2 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/zaac.19784410112
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  • 4
    Electronic Resource
    Electronic Resource
    Darstellung und Struktur von BaAl2Se4, BaGa2Se4, CaGa2Se4 und Caln2Te4 (1981)
    Weinheim : Wiley-Blackwell
    Zeitschrift für anorganische Chemie 479 (1981), S. 125-133 
    Details
    ISSN: 0044-2313
    Keywords: Chemistry ; Inorganic Chemistry
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology
    Description / Table of Contents: Preparation and Crystal Structure of BaAl2Se4, BaGa2Se4, CaGa2Se4, and CaIn2Te4The new compounds BaAl2Se4, BaGa2Se4, CaGa2Se4 and CaIn3Te4 crystallize with constants see “Inhaltsübersicht”. The structures are strongly related to the TlSe structure.
    Notes: Die Verbindungen BaAl2Se4, BaGa2Se4, CaGa2Se4 und CaIn2Te4 wurden erstmals dargestellt und strukturell aufgeklärt. Die kristallographischen Daten sind: BaAl2Se4: tetragonal, P4/nnc, Z = 4; a = 1135(2) pm, c = 619(1) pm, c/a = 0,545BaGa2Se4: orthorhombisch, Cccm, Z = 4; a = 648(1) pm, b = 1113(2) pm, c = 1124(2) pmCaGa2Se4: orthorhombisch, Fddd, Z = 32; a = 2106(2) pm, b = 2100(2) pm, c = 1266(2) pmCaIn2Te4: tetragonal, I4/mcm. Z = 2; a = 842(2) pm, c = 714(2) pm, c/a = 0,848. Die Strukturen aller dieser Verbindungen lassen sich als Varianten der TlSe-Struktur beschreiben.
    Additional Material: 5 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/zaac.19814790815
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  • 5
    Electronic Resource
    Electronic Resource
    Die Struktur des SrGa2Se4, eine neue Besetzungsvariante des TlSe-Typs (1983)
    Weinheim : Wiley-Blackwell
    Zeitschrift für anorganische Chemie 499 (1983), S. 145-152 
    Details
    ISSN: 0044-2313
    Keywords: Chemistry ; Inorganic Chemistry
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology
    Description / Table of Contents: Structure of SrGa2Se4, a New Variant of the TlSe TypeThe new compound SrGa2Se4 crystallizes in the orthorhombic system (space group Cccm) with constants see „Inhaltsübersicht“. The structure is a new variant of the TlSe-structure type.
    Notes: Die neue Verbindung SrGa2Se4 kristallisiert orthorhombisch (Raumgruppe Cccm) mit den Gitterkonstanten a = 1901,7 ± 0,6, b = 3233,9 ± 1,2, c = 3268,6 ± 1,2 pm. Die Struktur läßt sich als eine neue Besetzungsvariante des TlSe-Strukturtyps beschreiben.
    Additional Material: 4 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/zaac.19834990416
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  • 6
    Electronic Resource
    Electronic Resource
    Darstellung und Struktur der Verbindung Ca14AlSb11 (1984)
    Weinheim : Wiley-Blackwell
    Zeitschrift für anorganische Chemie 519 (1984), S. 183-188 
    Details
    ISSN: 0044-2313
    Keywords: Chemistry ; Inorganic Chemistry
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology
    Description / Table of Contents: Preparation and Structure of Ca14AlSb11The new compound Ca14AlSb11 crystallizes in the tetragonal system, space group I41/acd (No. 142) with lattice constants s. „Inhaltsübersicht“. In the structure there are Sb3- ions and complex tetrahedral AlSb49- and linear Sb37- anions. The compound can be interpreted as valence compound.
    Notes: Die neue Verbindung Ca14AlSb11 kristallisiert tetragonal in der Raumgruppe I41/acd (Nr. 142) mit den Gitterkonstanten a = 1667,6(5) pm, c = 2242,3(7) pm, c/a = 1,345.In der Struktur liegen neben Sb3--Ionen komplexe tetraedrische AlSb49-- und lineare Sb37--Anionen vor. Die Verbindung läßt sich dementsprechend als Valenzverbindung deuten.
    Additional Material: 2 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/zaac.19845191219
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  • 7
    Electronic Resource
    Electronic Resource
    Zur Strukturchemie der Alkalisalze der Tetrathiosäuren der Elemente der 5. Hauptgruppe (1976)
    Weinheim : Wiley-Blackwell
    Zeitschrift für anorganische Chemie 425 (1976), S. 67-80 
    Details
    ISSN: 0044-2313
    Keywords: Chemistry ; Inorganic Chemistry
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology
    Description / Table of Contents: Crystal Chemistry of the Alkali Salts of the Main Group V Element TetrathioacidsThe anhydrous tetrathioantimonates of K+, NH4+, and Na+ crystallize cubic in the (NH4)3SbS4-structure type. The analogous tetrathioarsenates and -phosphates form the (NH4)3AsS4-structure type. In the formation of these two different structures the density of the atomic packing is essential.
    Notes: Die wasserfreien Tetrathioantimonate von K+, NH4+ und Na+ kristallisieren kubisch im (NH4)3SbS4-Typ, während bei den bisher bekannten Alkalitetrathioarsenaten und -phosphaten der (NH4)3AsS4-Typ beobachtet wird. Die Ausbildung der beiden unterschiedlichen Strukturtypen wird auf Packungseffekte zurückgeführt.
    Additional Material: 6 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/zaac.19764250109
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  • 8
    Electronic Resource
    Electronic Resource
    Darstellung und Kristallstruktur von SrCu2Sb2 und SrZnBi2 (1976)
    Weinheim : Wiley-Blackwell
    Zeitschrift für anorganische Chemie 426 (1976), S. 205-214 
    Details
    ISSN: 0044-2313
    Keywords: Chemistry ; Inorganic Chemistry
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology
    Description / Table of Contents: Preparation and Crystal Structure of SrCu2Sb2 and SrZnBi2SrCu2Sb2 and SrZnBi2 have been prepared and analytically and structurally characterized. SrCu2Sb2 crystallizes tetragonal in the CaBe2Ge2 structure type. SrZnBi2 has its own structure type. In both structures the transition metal atoms form with the semimetal atoms tetragonal pyramids, which are connected by common edges of the basis to twodimensional sheets. These sheets are separated in the case of SrCu2Sb2 by single sheets of strontium atoms, in the case of SrZnBi2 by double sheets of strontium atoms in which fourfold nets of Bi atoms are located.
    Notes: SrCu2Sb2 und SrZnBi2 wurden dargestellt, analytisch und strukturell charakterisiert.SrCu2Sb2 kristallisiert tetragonal (a = 4,51 ± 0,01 Å, c = 10,91 ± 0,02 Å, Raumgruppe P4/nmm, z = 2) im CaBe2Ge2-Typ. SrZnBi2 kristallisiert in einem eigenen Strukturtyp (tetragonal, a = 4,64 ± 0,01 Å, c = 21,96 ± 0,03 Å, Raumgruppe I4/mmm, z = 4). In beiden Strukturen bilden die Übergangsmetalle mit den Halbmetallen zweidimensional unendliche Pyramidenschichten aus, die im Falle des SrCu2Sb2 durch Erdalkalieinfachschichten, im Falle des SrZnBi2 durch Erdalkalidoppelschichten mit eingelagerten Bi-Vierecknetzen getrennt sind.
    Additional Material: 12 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/zaac.19764260210
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  • 9
    Electronic Resource
    Electronic Resource
    Über Seleno- und Telluroarsenite, -antimonite und -bismutiteProfessor Walter Rüdorff zum 70. Geburtstage am 3. Oktober 1979 gewidmet (1979)
    Weinheim : Wiley-Blackwell
    Zeitschrift für anorganische Chemie 456 (1979), S. 87-94 
    Details
    ISSN: 0044-2313
    Keywords: Chemistry ; Inorganic Chemistry
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology
    Description / Table of Contents: On Seleno- and Telluroarsenites, -antimonites, and -bismutitesThe new compounds NaAsSe2, NaSbSe2, NaSbTe2, and NaBiTe2 have been prepared and their structures determined. NaSbSe2, NaSbTe2, and NaBiTe2 build up the NaCl structure with the following lattice constants: NaSbSe2: a = 596.6(2) pm, NaSbTe2: a = 631.7(2) pm, NaBiTe2: a = 636.6(3) pm. NaAsSe2 crystallizes orthorhombic with a = 583 ± 1pm, b = 2427 ± 5 pm, c = 1182 ± 2 pm, Pbca. In the structure there are distorted trigonal AsSe3 pyramids which are connected by corners to chains.
    Notes: Die neuen Verbindungen NaAsSe2, NaSbSe2, NaSbTe2 und NaBiTe2 wurden dargestellt und strukturell aufgeklärt. NaSbSe2, NaSbTe2 und NaBiTe2 kristallisieren in der NaCl-Struktur mit folgenden Gitterkonstanten: NaSbSe2: a = 596,6(2) pm, NaSbTe2: a = 631,7(2) pm, NaBiTe2: a = 636,6(3) pm. NaAsSe2 kristallisiert orthorhombisch mit a = 583 ± 1 pm, b = 2427 ± 5 pm, c = 1182 ± 2 pm, Pbca. In der Struktur liegen Ketten aus eckenverknüpften trigonalen AsSe3-Pyramiden vor.
    Additional Material: 3 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/zaac.19794560109
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  • 10
    Electronic Resource
    Electronic Resource
    Darstellung und Struktur von Li5Ga4 (1981)
    Weinheim : Wiley-Blackwell
    Zeitschrift für anorganische Chemie 474 (1981), S. 221-225 
    Details
    ISSN: 0044-2313
    Keywords: Chemistry ; Inorganic Chemistry
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology
    Description / Table of Contents: Preparation and Crystal Structure of Li5Ga4Li5Ga4 has been established as further, hitherto unknown phase in the LiGa system. The new compound crystallizes in the trigonal system (P3m1 - D3d3) with a = 437.5 ± 0.2 pm, c = 825.7 ± 0.2 pm, c/a = 1.885. The structure is strongly related to those of LiGa and Li3Ga2.
    Notes: Li5Ga4, eine bisher im Li/Ga-System noch nicht beschriebene Verbindung, kristallisiert trigonal (P3m1 - D3d3) mit a = 437,5 ± 0,2 pm und c = 825,7 ± 0,2 pm (c/a = 1,885). Die Struktur zeigt enge Bezüge zu denen der Nachbarphasen LiGa und Li3Ga2.
    Additional Material: 2 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/zaac.19814740323
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