ISSN:
1042-7163
Keywords:
Chemistry
Source:
Wiley InterScience Backfile Collection 1832-2000
Topics:
Chemistry and Pharmacology
Notes:
Synthesis of several 6-substituted-1,2,4,8,10,11-hexachloro-12H-dibenzo[d,g][1,3,2]dioxaphosphocin 6-oxides and their IR, 1H, 13C, and 31P NMR and mass spectral analyses are described. Observation of geminal coupling [2J(H,H) = 16.0 Hz] between bridged methylene protons (12-CH2) suggested their non-equivalence and is consistent with a boat-chair form which may be in conformational equilibrium with either a boat-boat or a distorted and extended boatlike conformation.
Additional Material:
1 Ill.
Type of Medium:
Electronic Resource
URL:
http://dx.doi.org/10.1002/hc.520050515
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