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  • Chemistry  (17)
  • Dynamic properties
  • 1990-1994  (17)
  • 1
    Electronic Resource
    Electronic Resource
    Effect of water absorption on the behavior of E-glass fiber/nylon-6 composites (1991)
    Brookfield, Conn. : Wiley-Blackwell
    Polymer Composites 12 (1991), S. 333-337 
    Details
    ISSN: 0272-8397
    Keywords: Chemistry ; Chemical Engineering
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics
    Notes: The effect of water absorption on the stress transferability across E-glass fiber/nylon 6 interface has been studied using the embedded single fiber composite technique. The behavior of silane coated fiber and untreated fiber composites after periods of water immersion were compared. The silane coating provided both higher interfacial shear stress transferability and protection from permanent water damage in the interphase region. It was found that water absorption in the nylon matrix reduced the shear stress transferability through plasticization of the matrix, weakening of the interface, and the development of tensile swelling stresses at the phase boundaries. In untreated materials the shear stress transferability was limited by decoupling of the matrix from the broken fiber ends by either interface slippage or local plane strain fracture in the interphase region near the fiber end. In the silane treated materials the shear stress transferability was limited by constrained yielding of the polysiloxane/nylon interphase at the fiber end, thus indicating plasticization of the matrix was the primary factor. After 20 days of water immersion, there was permanent deterioration of stress transferability in the untreated samples, but very little permanent damage in the treated samples.
    Additional Material: 3 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/pc.750120507
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  • 2
    Electronic Resource
    Electronic Resource
    In-situ composites: Evaluation of the adhesion between the thermoplastic matrix and the fibers of liquid crystalline polymer (1992)
    Brookfield, Conn. : Wiley-Blackwell
    Polymer Composites 13 (1992), S. 169-173 
    Details
    ISSN: 0272-8397
    Keywords: Chemistry ; Chemical Engineering
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics
    Notes: Mechanical properties of fiber reinforced composites depend on the formation of stable adhesive bonds between the constituents. In order to evaluate quantitatively the adhesion between liquid crystal polymer (LCP) fibers and a thermoplastic matrix of polycarbonate, the single fiber composite test (SFC), utilized for testing glass or carbon fiber composites, has been used. Neither chemical nor physical interaction has been found: the PC and LCP phases are completely incompatible. However, a mechanical friction between PC and LCP was observed during the drawing of the sample when the neck of the matrix started.
    Additional Material: 7 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/pc.750130304
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  • 3
    Electronic Resource
    Electronic Resource
    Cure kinetics of dicyanate matrix polymers (1992)
    Brookfield, Conn. : Wiley-Blackwell
    Polymer Composites 13 (1992), S. 191-196 
    Details
    ISSN: 0272-8397
    Keywords: Chemistry ; Chemical Engineering
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics
    Notes: The cure kinetics of two dicyanate resins were investigated by differential scanning calorimetry under isothermal and nonisothermal conditions. An autocatalytic kinetic model was proposed and a set of general kinetic parameters was calculated from the isothermal experiments. Good agreement between experimental data and the kinetic model has been obtained under different processing conditions, which demonstrated the validity and the usefulness of the analytical procedure and of the kinetic expression employed. Consequently, in its current form, the modeling methodology is capable of describing the degree of cure during a typical processing cycle and has the potential for comparing different resin formulations as well as the manifestations of cure in property development. Specifically, in this work the modeling methodology was tested using two distinct dicyanate resin systems while the development of the cure was also observed through dielectric analysis (DEA).
    Additional Material: 12 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/pc.750130307
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  • 4
    Electronic Resource
    Electronic Resource
    Wilhelmy plate studies of carbon fiber/viscous fluid systems (1993)
    Brookfield, Conn. : Wiley-Blackwell
    Polymer Composites 14 (1993), S. 224-228 
    Details
    ISSN: 0272-8397
    Keywords: Chemistry ; Chemical Engineering
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics
    Notes: The use of Wilhelmy plate techniques for studying the interactions of fibers with fluids of variable viscosity is discussed. The influence of hydrodynamic effects of force (F) VS. DEPTH (z) plots is interpreted on the basis of surface tension-independent added terms of the constitutive equation of the Wilhelmy experiment. Wetting experiments using pseudoplastic fluids (polyethyleneglycol/water solution) show that viscoelasticity is indeed important in the interpretation of Wilhelmy plate experiments. The comparison of wetting experiments performed on untreated and plasma-treated carbon fibers showed that at low stage speed and fluid viscosity, surface chemistry and morphology determines contact angles. At higher stage speeds and viscosities and advancing and receding angles are affected by surface chemistry-independent and hydrodynamics-dependent added contributions.
    Additional Material: 6 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/pc.750140307
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  • 5
    Electronic Resource
    Electronic Resource
    Toughening epoxy resins by liquid crystalline polymers (1992)
    New York, NY [u.a.] : Wiley-Blackwell
    Journal of Applied Polymer Science 44 (1992), S. 1465-1471 
    Details
    ISSN: 0021-8995
    Keywords: Chemistry ; Polymer and Materials Science
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology , Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics , Physics
    Notes: Toughening epoxy resins can be achieved by blending a low percentage of Liquid Crystalline Polymer with the thermoset. The processing technique consists of the spinning of blends of a thermoplastic (Ardel) with the LCP (PET/PHB60). The bundled filaments are subsequently dissolved in the uncured epoxy resin (Epon 825). After curing, the LCP phase separates from the matrix in the form of microfibers with a very high aspect ratio, which act as crack stoppers and improve fracture toughness of the material.
    Additional Material: 8 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/app.1992.070440816
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  • 6
    Electronic Resource
    Electronic Resource
    The effect of physical aging on long-term properties of poly-ether-ketone (PEEK) and PEEK-based composites (1990)
    New York, NY [u.a.] : Wiley-Blackwell
    Journal of Applied Polymer Science 39 (1990), S. 1163-1174 
    Details
    ISSN: 0021-8995
    Keywords: Chemistry ; Polymer and Materials Science
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology , Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics , Physics
    Notes: The viscoelastic properties of the amorphous and semicrystalline PEEK and of a PEEK-based composite (APC2) have been analyzed as a function of the aging time and related free volume relaxation, at temperatures close to the glass transition temperature. The effect of thermal treatments (physical aging) on the polymer amorphous phase of the three systems is presented. Creep tests approaching the “zero stress” were performed on samples subjected to different thermal histories. The presence of a second phase, namely crystallites and fibers, determines a loss of the mobility of the polymeric amorphous chains and consequently a decrease of the rate of free volume relaxation.
    Additional Material: 9 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/app.1990.070390511
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  • 7
    Electronic Resource
    Electronic Resource
    Blends of a polyetherimide and a liquid crystalline polymer: Fiber orientation and mechanical properties (1991)
    New York, NY [u.a.] : Wiley-Blackwell
    Journal of Applied Polymer Science 43 (1991), S. 839-844 
    Details
    ISSN: 0021-8995
    Keywords: Chemistry ; Polymer and Materials Science
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology , Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics , Physics
    Additional Material: 8 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/app.1991.070430501
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  • 8
    Electronic Resource
    Electronic Resource
    Physical characterization of incompatible blends of polymethylmethacrylate and polycaprolactone (1990)
    New York, NY [u.a.] : Wiley-Blackwell
    Journal of Applied Polymer Science 41 (1990), S. 2691-2704 
    Details
    ISSN: 0021-8995
    Keywords: Chemistry ; Polymer and Materials Science
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology , Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics , Physics
    Notes: Blends of polymethylmethacrylate (PMMA) and poly-ε-caprolactone (PCL) were prepared and characterized. The analysis of the glass transition temperature indicates no compatibility of the two polymers, which segregated into two distinct phases. The fracture strength of the blends can be explained on the basis of a constitutive model of spheres of PCL embedded in a PMMA matrix. The trend of water sorption confirms the hypothesis of phase segregation of PCL in the glassy matrix of PMMA.
    Additional Material: 7 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/app.1990.070411116
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  • 9
    Electronic Resource
    Electronic Resource
    Improvement of the processability of advanced polymers (1990)
    New York, NY [u.a.] : Wiley-Blackwell
    Journal of Applied Polymer Science 41 (1990), S. 2723-2737 
    Details
    ISSN: 0021-8995
    Keywords: Chemistry ; Polymer and Materials Science
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology , Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics , Physics
    Notes: The possibility of improving processability of engineering polymers was studied in this work. Low percentages of a thermotropic liquid crystalline polymer supplied by Bayer Co. were added to the polyetherimide Ultem. The thermal and morphological analysis revealed a two phase system. Rheological measurements in shear flow were carried out in the temperature range of the existence of the mesophase. A significant drop of ∼ 30% in the Ultem viscosity occurs even with 5% w/w TLCP. The influence of the addition of the thermotropic polymer on the mechanical properties of Ultem was also investigated. Moreover, the morphological analysis of the unfilled polymers and of the blends was performed and related to their rheological and mechanical behavior.
    Additional Material: 15 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/app.1990.070411119
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  • 10
    Electronic Resource
    Electronic Resource
    Poly(3-hydroxybutyrate)-co-(3-hydroxyvalerate)/Poly-L-lactide blends: Thermal and mechanical properties (1994)
    New York, NY [u.a.] : Wiley-Blackwell
    Journal of Applied Polymer Science 54 (1994), S. 1525-1535 
    Details
    ISSN: 0021-8995
    Keywords: Chemistry ; Polymer and Materials Science
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology , Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics , Physics
    Notes: Blends of poly(3-hydroxybutyrate)-poly(3-hydroxyvalerate) (PHBV) and poly(L-lactides) (PLLA) have been prepared by solvent casting. Compatibility, thermal behavior, morphology, and mechanical properties of systems with various compositions were studied using differential scanning calorimetry (DSC), dynamic mechanical measurement, tensile tests, scanning electron microscopy (SEM), and wide-angle X ray (WAXS). Glass transition temperature of solvent cast materials, detected by dynamic mechanical analysis (DMA), showed partial molecular interactions between PHBV and PLLA. Crystallinity of the PLLA phase slightly decreased with increasing amount of PHBV, confirming the partial dispersion of PLLA in the PHBV phase. Mechanical properties were analyzed with theoretical models able to predict the behavior of heterogeneous systems. Phase separation was confirmed by SEM observations. © 1994 John Wiley & Sons, Inc.
    Additional Material: 12 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/app.1994.070541017
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