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  • 1
    Electronic Resource
    Electronic Resource
    Total synthesis of the oligosaccharide fragment of calicheamicin .gamma.1I (1990)
    s.l. : American Chemical Society
    Journal of the American Chemical Society 112 (1990), S. 8193-8195 
    Details
    ISSN: 1520-5126
    Source: ACS Legacy Archives
    Topics: Chemistry and Pharmacology
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1021/ja00178a069
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  • 2
    Electronic Resource
    Electronic Resource
    Total synthesis of calicheamicin .gamma.1I. 1. Synthesis of the oligosaccharide fragment (1993)
    s.l. : American Chemical Society
    Journal of the American Chemical Society 115 (1993), S. 7593-7611 
    Details
    ISSN: 1520-5126
    Source: ACS Legacy Archives
    Topics: Chemistry and Pharmacology
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1021/ja00070a004
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  • 3
    Electronic Resource
    Electronic Resource
    Measurement of photosynthetic production of a marine phytoplankton population using a stable 13C isotope (1983)
    Springer
    Marine biology 73 (1983), S. 31-36 
    Details
    ISSN: 1432-1793
    Source: Springer Online Journal Archives 1860-2000
    Topics: Biology
    Notes: Abstract The use of stable isotope of carbon, 13C, for the determination of the photosynthetic rate of a marine phytoplankton population was examined. Particular concern was paid to the effects of non-phytoplanktonic organic carbon and the enrichment of inorganic carbon on the estimation of the photosynthetic rate. Photosynthetic rates determined by the 13C method showed a remarkable agreement with those determined by the 14C method. Insitu determinations of photosynthetic rate were made in three different water types: open ocean, coastal and neritic waters, which included oligo- and mesotrophic waters, by using the 13C method established.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1007/BF00396282
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  • 4
    Electronic Resource
    Electronic Resource
    Determination method for residual 1,3-dichloro-and 1,3,5-trichloro-2-(4-nitrophenoxy) benzene (nip and cnp) in fish and shellfish (1979)
    Springer
    Bulletin of environmental contamination and toxicology 23 (1979), S. 57-63 
    Details
    ISSN: 1432-0800
    Source: Springer Online Journal Archives 1860-2000
    Topics: Energy, Environment Protection, Nuclear Power Engineering , Medicine
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1007/BF01769916
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  • 5
    Electronic Resource
    Electronic Resource
    BamHI-SacI RFLP and Gm analysis of the immunoglobulin IGHG genes in the Northern Selkups (west Siberia): new haplotypes with deletion, duplication and triplication (1999)
    Springer
    Human genetics 〈Berlin〉 105 (1999), S. 530-541 
    Details
    ISSN: 1432-1203
    Source: Springer Online Journal Archives 1860-2000
    Topics: Biology , Medicine
    Notes: Abstract. Gm immunoglobulin allotypes have been studied in 1157 individuals of seven Northern Selkup populations, which account for 80% of the entire population of this west Siberian tribe. This study confirms that the northern Selkup populations are a Caucasoid-Mongoloid hybrid. Restriction fragment length polymorphism (RFLP) analysis of the IGHG genes using double BamHI-SacI digests, performed on 475 DNA samples, allowed us to describe nine new BamHI-SacI haplotypes (BS47 to BS55), eight of them being characterized by IGHG gene deletion or duplication: G1 (BS49) or G4 (BS55) deletion, G4 duplication (BS51), GP-G2-G4 multigene deletion (BS50), duplication (BS48, BS53 and BS54) or triplication (BS52). A new rare Gm haplotype 15,16*;1,17;23 has been found associated with BS52. The BS51 haplotype characterized by a duplicated G4 gene (additional 7.85 kb G4 band identifying a new G4*C5 allele) was always found associated with the Gm 5*;3;23 haplotype. A high RFLP diversity has been observed for the Northern-Mongoloid haplotype Gm 15,16*;1,17;.. which was found (1) with the BS27 haplotype characterized by a 3-exon hinge G3 gene, (2) with two different GP-G2-G4 multigene duplications, BS53 and BS54 haplotypes, which differ by the size of the duplicated G4 genes, and (3) with the BS55 haplotype characterized by a G4 deletion. In the Northern Selkups, haplotypes with duplicated genes were observed at a higher frequency (24%) than haplotypes with deleted genes (6%).
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1007/s004399900187
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  • 6
    Electronic Resource
    Electronic Resource
    Determination of the viscometric constants for chitosan and the application of universal calibration procedure in its gel permeation chromatography (1993)
    Springer
    Colloid & polymer science 271 (1993), S. 76-82 
    Details
    ISSN: 1435-1536
    Keywords: Chitosan ; molecular weight ; light scattering ; viscosity ; gel permeation chromatography
    Source: Springer Online Journal Archives 1860-2000
    Topics: Chemistry and Pharmacology , Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics
    Notes: Abstract The viscometric constantsa andK in the Mark-Houwink equation were determined in 0.5 M acetic acid-0.5 M.sodium acetate solution for chitosan fractionated by gel filtration. The weight-average molecular weight of each fraction was measured by the light-scattering method. The values obtained area=0.59 andK=0.119 cm3 g−1. The molecular weightsMw andMn for fractionated chitosan were measured by GPC. The value ofMw by GPC was much different from that by light scattering and, therefore, a universal calibration procedure was applied to the data by GPC. It was concluded that, also in the case of a cationic polysaccharide such as chitosan, the universal calibration procedure is effective for obtaining the reliable molecular weight by GPC.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1007/BF00652306
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  • 7
    Electronic Resource
    Electronic Resource
    Depolymerization of hyaluronate by the phototoxic drugs phenothiazines and sulfacetamide (2000)
    Springer
    Colloid & polymer science 278 (2000), S. 84-89 
    Details
    ISSN: 1435-1536
    Keywords: Key words Hyaluronate ; Depolymerization ; Phenothiazines ; Sulfacetamide ; UV irradiation
    Source: Springer Online Journal Archives 1860-2000
    Topics: Chemistry and Pharmacology , Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics
    Notes: Abstract Phenothiazines (promazine, promethazine, chlorpromazine) and sulfacetamide, known as phototoxic drugs, depolymerize aqueous sodium hyaluronate (HA) on exposure to light. The reduction in the HA molecular weight was followed by size-exclusion chromatography with low-angle laser light scattering. In the low-concentration region of the drugs below 0.05 mM, the rate constants of depolymerization increased. The molecular weight of HA was practically unchanged without UV irradiation in the presence of drugs or with UV irradiation in the absence of drugs, indicating the phenothiazines and sulfacetamide require photoenergy to yield any kind of damaging chemical species for HA depolymerization. An involvement of active oxygen radicals in the effects of promazine and promethazine was evidenced by inhibition under anaerobic conditions. Further, addition of mannitol controlled the reaction in the presence of oxygen, pointing to hydroxyl radicals as the damaging agent. Chlorpromazine and sulfacetamide preferably depolymerized HA under anaerobic conditions, suggesting the participation of hydrated electrons.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1007/s003960050014
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  • 8
    Electronic Resource
    Electronic Resource
    Effects of aging temperature on the microstructure and mechanical properties of 1.8Cu-7.3Ni-15.9Cr-1.2Mo-low C, N martensitic precipitation hardening stainless steel (2000)
    Springer
    Journal of materials science 35 (2000), S. 2245-2253 
    Details
    ISSN: 1573-4803
    Source: Springer Online Journal Archives 1860-2000
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics
    Notes: Abstract The effects of aging temperature on the microstructure and mechanical properties of a newly designed martensitic precipitation hardening stainless steel, which is 1.8Cu-15.9Cr-7.3Ni-1.2Mo-low C, N steel, for improving the toughness, ductility and corrosion resistance of stainless steel of 1000 MPa grade tensile strength were experimentally investigated. The specimen aged at 753 K for 14.4 ks has a typical lath martensitic structure with about 12% interlath austenite, while the specimens aged at 813 K and 853 K for 14.4 ks have the lamellar duplex microstructure of the reverted austenite and the aging hardened martensite. The formation process of reverted austenite is controlled by diffusion of Ni in martensite. The mean size of precipitates which are enriched with Cu increases with rising aging temperature, however, it is about 30 nm even after aging at 853 K for 14.4 ks. The specimens aged at 813 K and 853 K for 14.4 ks, in which the reversion of martensite to austenite is observed, have the excellent combinations of strength, ductility and toughness.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1023/A:1004778910345
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  • 9
    Electronic Resource
    Electronic Resource
    Quantum Tunneling of D(H) Atoms and 2 – in Solid Hydrogen (1998)
    Springer
    Journal of low temperature physics 111 (1998), S. 453-461 
    Details
    ISSN: 1573-7357
    Source: Springer Online Journal Archives 1860-2000
    Topics: Physics
    Notes: Abstract This paper contains three results. First, the rate constants for the tunneling reaction HD + D → H + D 2 in solid HD increase steeply with increasing temperature above 5 K, while they are almost independent of temperature below 5 K. A mechanism of a vacancy–assisted tunneling reaction is proposed to account for this temperature dependence. Second, a hydrogen atom and a hydrogen molecule form a van der Waals complex in the Ar matrix at 20 K, where the tunneling reaction HD + D →H + D 2 takes place in this complex. The analysis of well–resolved ESR spectra of the complex determined the distance between a hydrogen atom and a hydrogen molecule as 2.3 – 2.5 Å. Third, the decay rate constants of $${\text{H}}_{\text{2}}^ - $$ anions in solid parahydrogen decrease with decreasing temperature below 6.6 K, attain the minimum value at 5 K, and then increase with decreasing temperature in the range of 5 → 2.7 K. The abnormal temperature dependence of the decay rate constants below 5 K is ascribed to a phonon–scattering process of quantum diffusion.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1023/A:1022264509705
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  • 10
    Electronic Resource
    Electronic Resource
    Decay of 2 - Anions in Solid Parahydrogen via Two-Stage Quantum Tunneling Diffusion Processes (1999)
    Springer
    Journal of low temperature physics 114 (1999), S. 413-429 
    Details
    ISSN: 1573-7357
    Source: Springer Online Journal Archives 1860-2000
    Topics: Physics
    Notes: Abstract Decay mechanism of H 2 - anions in X(γ)-irradiated solid para-H2 (p-H 2 ) has been studied using high-resolution ESR spectroscopy in the temperature range between 1.3–6.6 K. The results are summarized as follows. First,the decay rate constant of the 2 - anions is not proportional to initial yields of reactive species such as cations and H atoms but proportional to the concentration of less-reactive species of HD molecules in p-H2 . This result shows that the decay of the 2 - anion is due to the reaction neither with cations nor H atoms but with HD molecules originally contained in the p-H2 sample at natural abundance. Second,the decay rate constant of the 2 - anions increases proportionally with the increase in temperature below 3 K and decreases with the increase in temperature between 3–5 K,although it increases exponentially with the increase in temperature above 5 K. This result indicates that the decay rate constant of the 2 - anions is controlled by the rate constant for the diffusion of the 2 - anions via one-phonon assisted quantum tunneling below 3 K,two-phonon scattered or assisted quantum tunneling between 3–5 K,and thermally-activated process above 5 K.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1023/A:1021850103903
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