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  • 11
    Electronic Resource
    Electronic Resource
    Pentabenzylcyclopentadienylkalium · 3 THF, eine Organokaliumverbindung mit „Klavierstuhl“-Geometrie (1989)
    Weinheim : Wiley-Blackwell
    Zeitschrift für die chemische Industrie 101 (1989), S. 793-794 
    Details
    ISSN: 0044-8249
    Keywords: Chemistry ; General Chemistry
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology
    Additional Material: 1 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/ange.19891010632
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  • 12
    Electronic Resource
    Electronic Resource
    Synthesis, characterization, and structures of 1-(9-Fluorenyl)-germatrane and 1-(Phenylacetylenyl)germatrane (1997)
    Weinheim : Wiley-Blackwell
    Zeitschrift für anorganische Chemie 623 (1997), S. 1144-1150 
    Details
    ISSN: 0044-2313
    Keywords: Trihalogenogermane ; Germatrane ; Transmetalation ; Crystal structure ; Chemistry ; Inorganic Chemistry
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology
    Description / Table of Contents: Darstellung, Charakterisierung und Strukturen von 1-(9-Fluorenyl)germatran and 1-(Phenylacetylenyl)germatranÜber die Synthesen der Titelverbindungen, nämlich N(CH2CH2O)3GeY (2 Y=Fluorenyl; 4 Y=PhC≡C) durch Reaktion von X3GeY (1 Y=Fluorenyl, X=Br; 5 Y=PhC≡C, X=Cl) mit N(CH2CH2OSnR3)3 (3 R=Et; 6 R=Bu) wird berichtet und die Darstellung der neuen Verbindung 1 wird beschrieben. Die Strukturen der Verbindungen wurden durch Elementaranalysen sowie mittels 1H and 13C NMR-Spektroskopie bestimmt, 2 und 4 massenspektrometrisch charakterisiert. 1, 2 und 4 wurden mit Röntgenbeugungsmethoden analysiert.
    Notes: Syntheses of the title compounds, viz. N(CH2CH2O)3GeY (2 Y=Fluorenyl; 4 Y=PhC≡C) by the reaction of X3GeY (1 Y=Fluorenyl, X=Br; 5 Y=PhC≡C, X=Cl) with N(CH2CH2OSnR3)3 (3 R=Et; 6 R=Bu) are reported including the preparation of the new compound 1. Identity and structures were established by elemental analyses, 1H and 13C NMR spectroscopy. 2 and 4 were characterized by mass spectrometry. Single crystal structures of 1, 2 and 4 were determined by X-ray diffraction methods.
    Additional Material: 3 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/zaac.19976230723
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  • 13
    Electronic Resource
    Electronic Resource
    Kernresonanzspektroskopische Untersuchungen an cis-(CH3)2Pt[P(OCH3)3]2 (1977)
    Chichester : Wiley-Blackwell
    Organic Magnetic Resonance 9 (1977), S. 325-327 
    Details
    ISSN: 0030-4921
    Keywords: Chemistry ; Analytical Chemistry and Spectroscopy
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology
    Description / Table of Contents: 100 MHz 1 H n.m.r. spectra of cis-(CH3)2Pt[P(OCH3)3]2 are analysed in full detail as superimposing [AR3X9]2 and [AR3X9]2M systems. The cis structure is derived from J(PP) and J(PtP).
    Notes: 100 MHz 1H NMR Spektren von cis- (CH3)2Pt[P(OCH3)3]2 werden als Superposition von [AR3X9]2-und [AR3X9]2M -Systemen analysiert. Die cis-Struktur wird abgeleitet von den Kopplungskonstanten J(PP) und J(PtP).
    Additional Material: 2 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/mrc.1270090608
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  • 14
    Electronic Resource
    Electronic Resource
    O=As(NMe2)3: Synthesis and crystal structure of the arsenic analogue of HMPTDedicated to Prof. Dr. K. Issleib on the occasion of his seventieth birthday. (1991)
    New York, NY [u.a.] : Wiley-Blackwell
    Heteroatom Chemistry 2 (1991), S. 629-631 
    Details
    ISSN: 1042-7163
    Keywords: Chemistry
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology
    Notes: O=As(NMe2)3 (HMAsT) is obtained in low yields by reacting O=AsCl3 with excess HNMe2 or by ozonolysis of As(NMe2)3; however, it is formed in yields 〉65% by using (Me3Si)2O2 and As(NMe2)3 in hydrocarbon solution. The structure of HMAsT was established by IR/Raman, NMR and mass spectroscopy, and single crystal X-ray structure analysis. The structure determination revealed (sp3C)-H…O-hydrogen bonding in the solid state. Acid-base reaction by methanolysis affords ionic [Me2NH2] [O2As(OMe)2] while iodide is oxidized to iodine.
    Additional Material: 1 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/hc.520020604
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  • 15
    Electronic Resource
    Electronic Resource
    Untersuchungen an Methylzinn-amiden (1965)
    Weinheim : Wiley-Blackwell
    Berichte der deutschen chemischen Gesellschaft 98 (1965), S. 520-525 
    Details
    ISSN: 0009-2940
    Keywords: Chemistry ; Inorganic Chemistry
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology
    Notes: Die einfachen PMR-Spektren der Methylzinn-dimethylamide (CH3)4-nSn-[N(CH3)2]n und einiger Substitutionsprodukte aus der Reaktion mit Hexamethyldisilazan werden mitgeteilt. Es wird dabei immer nur ein Silazanrest in das Zinnamid eingeführt. Frühere Ergebnisse und obiger Befund sprechen für die Annahme eines nicht unbeträchtlichen Doppelbindungsanteiles für die Zinn-Stickstoffbindung. Für diese Deutung spricht auch die Kopplung der magnetisch aktiven Zinnisotope 117,119Sn mit den Protonen der über den Stickstoff gebundenen Methylgruppen, die bei reinen Methylzinn-dimethylamiden nicht beobachtet wurde.
    Additional Material: 2 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/cber.19650980224
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  • 16
    Electronic Resource
    Electronic Resource
    Notiz zur Reaktivität der Zinn-Stickstoff-Bindung (1964)
    Weinheim : Wiley-Blackwell
    Berichte der deutschen chemischen Gesellschaft 97 (1964), S. 2087-2089 
    Details
    ISSN: 0009-2940
    Keywords: Chemistry ; Inorganic Chemistry
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology
    Additional Material: 2 Tab.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/cber.19640970744
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  • 17
    Electronic Resource
    Electronic Resource
    Dipolmomente einiger Organozinnchloride (1965)
    Weinheim : Wiley-Blackwell
    Berichte der deutschen chemischen Gesellschaft 98 (1965), S. 969-976 
    Details
    ISSN: 0009-2940
    Keywords: Chemistry ; Inorganic Chemistry
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology
    Notes: Die Dipolmomente einer Reihe von Organozinnchloriden R4-nSnCln(R = CH3, C2H5 C4H9, C6H5) deuten auf eine Zunahme der Polarität der Zinn-Chlor-Bindung mit steigender Zahl n hin. Die Phenyl-Zinn-Bindung erweist sich weniger polar als erwartet.
    Additional Material: 3 Tab.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/cber.19650980342
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  • 18
    Electronic Resource
    Electronic Resource
    Spektroskopische Untersuchungen an Organozinnverbindungen R4-4SnXn (1964)
    Weinheim : Wiley-Blackwell
    Berichte der deutschen chemischen Gesellschaft 97 (1964), S. 3444-3451 
    Details
    ISSN: 0009-2940
    Keywords: Chemistry ; Inorganic Chemistry
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology
    Notes: Die PMR-Spektren der Organozinn-diäthylamide R4-nSn(N(C6H5)2]n (R=C2H5, C4H9) und der daraus durch Alkoholyse dargestellten Alkoxide R4-nSn(OR)n (R=CH3, C2H5, C4H9, C6H5; R′=CH3, C2H5) werden mitgeteilt und diskutiert. In Übereinstimmung mit unseren früheren Untersuchungen sprechen die Befunde bei den Organozinn-diäthylamiden für einen covalenten Bindungstyp, während die Spektren der Alkoxide mehr auf einen ionogenen Bindungscharakter schließen lassen. Die 1R-Spektren einiger Organozinn-alkoxide werden erläutert, eine Pentakoordination des Zinns in dessen Alkoxy-Verbindungen wird diskutiert.
    Additional Material: 6 Tab.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/cber.19640971226
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  • 19
    Electronic Resource
    Electronic Resource
    Facile Preparation of Mono- and Bis(tin)-Substituted Niobocenes with Functionalized Stannyl Ligands: The Search for Non-Classical Interligand Interactions (1999)
    Weinheim : Wiley-Blackwell
    Berichte der deutschen chemischen Gesellschaft 1999 (1999), S. 825-831 
    Details
    ISSN: 1434-1948
    Keywords: Niobium ; Tin ; Hydrides ; Group 5 ; Group 14 ; Chemistry ; General Chemistry
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology
    Notes: The reaction of niobocene trihydride [Cp2NbH3] with one equivalent of an alkyl- or aryltin halide XnSnR4-n (n = 1, 2) leads to products of the displacement of hydride by tin, i.e. [Cp2NbH2(SnX3-nRn)] [R = Me, n = 3 (1); R = Me, × = Cl, n = 2 (3); R = Ph, n = 3 (4); R = Ph, × = Cl, n = 2 (5); R = Et, × = Br, n = 2 (6)]. Use of an excess of the tin reagent results in a halodealkylation exchange reaction at the tin atom bound to the metal center. Reaction of the mono(silyl) complexes [Cp2NbH2(SiXMe2)] (X = Cl, Ph) with organotin halides XnSnR4-n gives products of the displacement of silicon by tin, whereas the bis(silyl) complex [Cp2NbH(SiPhMe2)2] does not undergo this reaction. The bis(tin)-substituted niobocene [Cp2NbH(SnMe3)2] has been prepared by the reaction of [Cp2NbH2(SnMe3)] with the tin amide Me3SnNMe2 under thermal conditions, as well as by the literature method of thermolysis of [Cp2NbH(η2-C2H3Ph)] in the presence of Me3SnH. Reaction of [Cp2NbH(SnMe3)2] with two equivalents of Cl2SnMe2 affords the bis(tin)-substituted complex [Cp2NbH(SnClMe2)2] (9). The possible presence of non-classical hypervalent H···Sn-Cl interactions in this compound has been assessed by means of X-ray structure analysis. The structural data for 9 are in accord with an essentially classical description as a tin-substituted dihydride complex without significant Sn···H interactions.
    Additional Material: 1 Ill.
    Type of Medium: Electronic Resource
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  • 20
    Electronic Resource
    Electronic Resource
    Darstellung von Organozinn-cyaniden des Typs R3SnCN und R2Sn(CN)2 (1965)
    Weinheim : Wiley-Blackwell
    Berichte der deutschen chemischen Gesellschaft 98 (1965), S. 1201-1204 
    Details
    ISSN: 0009-2940
    Keywords: Chemistry ; Inorganic Chemistry
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology
    Notes: Bei der Umsetzung von Tri- und Diorganylzinn-diäthylamiden R3SnN(C2H5)2 bzw. R2Sn[N(C2H5)2]2 (R = Alkyl bzw. Aryl) mit wasserfreier Blausäure in inerten Lösungsmitteln erhält man in nahezu quantitativer Ausbeute die entsprechenden Organozinn-cyanide R3SnCN bzw. R2Sn(CN)2.
    Additional Material: 5 Tab.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/cber.19650980428
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