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  • 1
    facet.materialart.
    Unbekannt
    High-Resolution Imaging of Texture and Microstructure by the Moving Detector Method (2010)
    Details
    Publikationsdatum: 2021-03-29
    Beschreibung: In order to describe texture and microstructure of a polycrystalline material completely, crystal orientation g={?1F?2} must be known in all points x={x1?x2?x3} of the material. This can be achieved by locationresolved diffraction of high-energy, i.e. short-wave, X-rays from synchrotron sources. Highest resolution in the orientation- as well as the location-coordinates can be achieved by three variants of a detector sweeping technique in which an area detector is continuously moved during exposure. This technique results in two-dimensionally continuous images which are sections and projections of the six-dimensional orientation location space. Further evaluation of these images depends on whether individual grains are resolved in them or not. Because of the high penetration depth of high-energy synchrotron radiation in matter, this technique is also, and particularly, suitable for the investigation of the interior of big samples.
    Beschreibung: research
    Schlagwort(e): 548 ; VAE 120 ; VKA 200 ; VGA 410 ; Methodik {Strukturgeologie} ; Gefügekunde der Gesteine ; Röntgenanalyse {Mineralogie: Kristallographie}
    Sprache: Englisch
    Materialart: article , publishedVersion
    Format: 18 S.
    Format: application/pdf
    Standort Signatur Erwartet Verfügbarkeit
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    CITATION GEO-LEO
  • 2
    facet.materialart.
    Unbekannt
    High-Resolution Imaging of Texture and Microstructure by the Moving Detector Method (2018)
    Details
    Publikationsdatum: 2021-03-29
    Beschreibung: In order to describe texture and microstructure of a polycrystalline material completely, crystal orientation g={?1F?2} must be known in all points x={x1?x2?x3} of the material. This can be achieved by locationresolved diffraction of high-energy, i.e. short-wave, X-rays from synchrotron sources. Highest resolution in the orientation- as well as the location-coordinates can be achieved by three variants of a detector sweeping technique in which an area detector is continuously moved during exposure. This technique results in two-dimensionally continuous images which are sections and projections of the six-dimensional orientation location space. Further evaluation of these images depends on whether individual grains are resolved in them or not. Because of the high penetration depth of high-energy synchrotron radiation in matter, this technique is also, and particularly, suitable for the investigation of the interior of big samples.
    Schlagwort(e): 551 ; VAE 120 ; VKA 200 ; VGA 410 ; 38.03
    Sprache: Englisch
    Materialart: article , publishedVersion
    Format: application/pdf
    Standort Signatur Erwartet Verfügbarkeit
    BibTip Andere fanden auch interessant ...
    CITATION GEO-LEO
  • 3
    Digitale Medien
    Digitale Medien
    Cation selective tubular carrier-PVC-membranes containing polymeric plasticizer with low tendency of migration for Solid State Contact Electrodes (1994)
    New York, NY : Wiley-Blackwell
    Journal für Praktische Chemie/Chemiker-Zeitung 336 (1994), S. 575-580 
    Details
    ISSN: 0941-1216
    Schlagwort(e): Chemistry ; Organic Chemistry
    Quelle: Wiley InterScience Backfile Collection 1832-2000
    Thema: Chemie und Pharmazie
    Notizen: The lifetime of cation selective carrier-PVC-membranes partially depends on the components' remaining in the membrane. An exchange of monomeric by polymeric plasticizers with low tendency to migrate lengthens the function time drastically. Other than for Na+ - and NH4+-selective membranes, it is essential for K+ - and Ca2+-selective membranes and optional for H+-selective membranes to incorporate lipophilic anions in order to make the phase transfer catalysis more efficient. The resistence to saponification of phthalic acid polyester gives H+-selective membranes a high stability of measured values even in the alkaline range.For anion selective PVC-membranes, instead of cation selective plasticizers the plasticizing qualities of a liquid charged ligand should be used.The tubular carrier-PVC-membranes of our ion selective flow through measuring systems are diffusion welded to the ends of two PVC-tubes [1] so that they are absolutely tight with no risk of potential leakage. Migration of the membrane components plasticizer and ionophore across this border as well as their extraction [2, 3] into the measuring solution [4] will naturally reduce the membrane's functionning time [5].
    Zusätzliches Material: 3 Ill.
    Materialart: Digitale Medien
    URL: http://dx.doi.org/10.1002/prac.19943360703
    Standort Signatur Erwartet Verfügbarkeit
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    Artikel (Nationallizenzen)
    Volltext
  • 4
    Digitale Medien
    Digitale Medien
    Substituierte Alkinyle als axiale Liganden an häminähnlich gebundenem Eisen(III) - Einordnung in eine spektrochemische SerieHerrn Professor Dr. E. Hoyer zum 60. Geburtstag gewidmet (1991)
    New York, NY : Wiley-Blackwell
    Journal für Praktische Chemie/Chemiker-Zeitung 333 (1991), S. 423-430 
    Details
    ISSN: 0021-8383
    Schlagwort(e): Chemistry ; Organic Chemistry
    Quelle: Wiley InterScience Backfile Collection 1832-2000
    Thema: Chemie und Pharmazie
    Notizen: Substituted Alkinyles as Axial Ligands at Hemine Like Bound Iron(III) - Incorporation into a Spectrochemical Series.Substituted lithium alkynyles Li—C≡C—R (R = tBu, Ph, p-Cl—C6H4, Me3Si, iPr3Si, Ph3Si) react with the hemine like macrocyclic iron(III) complex 6,13-di(ethoxycarbonyl)-5, 14-dimethyl-1, 4, 8, 11-tetraazatetradeca-4,6,12,14-tetraenato[2-]iron(III)-iodide (formula 2;) in tetrahydrofuran to form anionic low-spin di-adducts [fe(C≡C—R)2]-. The incorporation of the alkynyles into a spectrochemical series of the axial ligands (studied by the sharp equatorial-ligand-to-metal CT absorption band) results in the wavelength-sequence (nm): OH- (≍ 510) « N3- (≍ 625) 〈 tBu—C≡C- (664) 〈 NH3 (666) 〈 Ph—C≡C- (692) 〈 Ph—NH2 (695) 〈 Me3Si—C≡C- (698) 〈 SCN- (713) 〈 Ph3Si—C ≡ C- (716) 〈 CN- (739) 〈 4-picoline (759) 〈 pyridine (765) 〈 nicotinamide (776) 〈 methylnicotinat (788) 〈 pyrazine (798) and points to a significant π-acceptor ability of the silyl substituents.
    Zusätzliches Material: 2 Tab.
    Materialart: Digitale Medien
    URL: http://dx.doi.org/10.1002/prac.19913330307
    Standort Signatur Erwartet Verfügbarkeit
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    Artikel (Nationallizenzen)
    Volltext
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