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  • 1
    Electronic Resource
    Electronic Resource
    Synthesis, characterization, peripheral studies, and structural analysis of E-4-(N-methylanilino)-3-pentene-2-one, C12H15NO (1998)
    Springer
    Journal of chemical crystallography 28 (1998), S. 899-903 
    Details
    ISSN: 1572-8854
    Keywords: Crystal structure ; ir/nmr ; β-amino-α ; β-unsaturaled ketone ; noncentrosemmtric ; enamino ketones
    Source: Springer Online Journal Archives 1860-2000
    Topics: Geosciences , Physics
    Notes: Abstract Crystallographic structural refinement of E-4-(N-methylanilino)-3-pentene-2-one (I) has been carried out by means of three-dimensional single-crystal X-ray diffractometry. The title compound crystallizes in space group C2 (No. 5,Z = 4). The lattice constants are a = 21.543(4), b = 6.433(1), c = 8.019(2) Å, and β = 97.82(3)°. Characterizations include physical property determinations and spectrometric identifications employing IR, 1H and 13C NMR, and X-ray powder analyses. The molecules in the crystal lattice are held together by van der Waals forces. Selected bond distances and angles are presented and discussed as well as synthesis and peripheral studies.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1023/A:1022802619976
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    Paper (German National Licenses)
    Fulltext
  • 2
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    QMI: Rising to the Space Station Design Challenge (2002)
    In:  Other Sources
    Details
    Publication Date: 2019-07-18
    Description: The Quench Module Insert (QMI) materials processing furnace is being designed to operate for 8000 hours over four years on the International Space Station (ISS) as part of the first Materials Science Research Rack (MSRR-1) of the Materials Science Research Facility (MSRF). The Bridgman-type furnace is being built for the directional solidification processing of metals and alloys in the microgravity environment of space. Most notably it will be used for processing aluminum and related alloys. Designing for the space station environment presents intriguing design challenges in the form of a ten-year life requirement coupled with both limited opportunities for maintenance and resource constraints in the form of limited power and space. The long life requirement has driven the design of several features in the furnace, including the design of the heater core, the selection and placement of the thermocouples, overall performance monitoring, and the design of the chill block. The power and space limitations have been addressed through a compact furnace design using efficient vacuum insulation. Details on these design features, as well as development test performance results to date, are presented.
    Keywords: Spacecraft Design, Testing and Performance
    Type: International Space Station Utilization Conference/World Space Congress; Oct 19, 2002; Houston, TX; United States
    Format: text
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    NASA TECHNICAL REPORTS
  • 3
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    Heater Development, Fabrication, and Testing: Analysis of Fabricated Heaters (2008)
    In:  CASI
    Details
    Publication Date: 2019-07-12
    Description: Thermal simulators (highly designed heater elements) developed at the Early Flight Fission Test Facility (EFF-TF) are used to simulate the heat from nuclear fission in a variety of reactor concepts. When inserted into the reactor geometry, the purpose of the thermal simulators is to deliver thermal power to the test article in the same fashion as if nuclear fuel were present. Considerable effort has been expended to mimic heat from fission as closely as possible. To accurately represent the fuel, the simulators should be capable of matching the overall properties of the nuclear fuel rather than simply matching the fuel temperatures. This includes matching thermal stresses in the pin, pin conductivities, total core power, and core power profile (axial and radial). This Technical Memorandum discusses the historical development of the thermal simulators used in nonnuclear testing at the EFF-TF and provides a basis for the development of the current series of thermal simulators. The status of current heater fabrication and testing is assessed, providing data and analyses for both successes and failures experienced in the heater development and testing program.
    Keywords: Spacecraft Design, Testing and Performance
    Type: NASA/TM-2008-215466 , M-1235
    Format: application/pdf
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  • 4
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    Thermal Control System for a Small, Extended Duration Lunar Surface Science Platform (2010)
    In:  CASI
    Details
    Publication Date: 2019-07-13
    Description: The presentation slides include: Introduction: lunar mission definition, Problem: requirements/methodology, Concept: thermal switching options, Analysis: system evaluation, Plans: dual-radiator LHP (loop heat pipe) test bed, and Conclusions: from this study.
    Keywords: Spacecraft Design, Testing and Performance
    Type: M10-0336 , Spacecraft Thermal COntrol Workshop; Mar 09, 2010 - Mar 11, 2010; El Segundo, CA; United States
    Format: application/pdf
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