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  • Physics  (602)
  • SPACE RADIATION  (527)
  • 1980-1984  (502)
  • 1970-1974  (627)
  • 1
    Electronic Resource
    Electronic Resource
    Aromatic polyamides. II. Thermal degradation of some aromatic polyamides and their model diamides (1981)
    New York : Wiley-Blackwell
    Journal of Polymer Science: Polymer Chemistry Edition 19 (1981), S. 2817-2834 
    Details
    ISSN: 0360-6376
    Keywords: Physics ; Polymer and Materials Science
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology
    Notes: Thermal degradation behavior of poly(1,3-phenylene isophthalamide) and poly(chloro-2,4-phenylene isophthalamide) was investigated with the aid of some appropriate model compounds. The pyrolysis products of these materials were identified by gas chromatography (GC), gas chromatography/Fourier transform infrared spectroscopy (GC/FT-IR), and gas chromatography/mass spectrometry (GC/MS). The residual chars were characterized by IR spectroscopy. Thermogravimetric analysis (TGA) was applied to study the effect of end-group concentration on the degradation characteristics of the two polyamides. Kinetic parameters that describe the thermal degradation of the polyamides were also evaluated by TGA. The results of this investigation suggest that the thermal decomposition of these aromatic polyamides involves homolytic as well as hydrolytic cleavages of the amide units.
    Additional Material: 13 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/pol.1981.170191115
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    Paper (German National Licenses)
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  • 2
    Electronic Resource
    Electronic Resource
    ESCA investigation of the electronic structure of polyhexafluorobut-2-yneThis is considered as Part X of Reactions Involving Fluoride Ion and Part VI of Applications of ESCA to Structure and Bonding in Polymers. A preliminary account of this work has been presented at the Faraday Discussion Meeting No. 54 on the photoelectron spectroscopy of molecules, Sussex University, 1972. (1974)
    New York : Wiley-Blackwell
    Journal of Polymer Science: Polymer Chemistry Edition 12 (1974), S. 1647-1652 
    Details
    ISSN: 0360-6376
    Keywords: Physics ; Polymer and Materials Science
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology
    Notes: Polyperfluorobut-2-yne is prepared by a fluoride ion-induced polymerization of hexafluorobut-2-yne. The mass spectrum indicates a regular fragmentation pattern but the ESCA spectrum establishes the structure as a polyene, rather than a crosslinked system, and the occurrence of a shake-up peak assists in this assignment.
    Additional Material: 3 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/pol.1974.170120805
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  • 3
    Electronic Resource
    Electronic Resource
    Spectroscopic studies of solutions, suspensions, and precipitates of poly(1,6-di-p-toluene sulfonyloxy-2,4-hexadiyne) (1981)
    New York : Wiley-Blackwell
    Journal of Polymer Science: Polymer Physics Edition 19 (1981), S. 321-334 
    Details
    ISSN: 0098-1273
    Keywords: Physics ; Polymer and Materials Science
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology , Physics
    Notes: Optical-absorption, fluorescence, and Raman spectra for solutions, suspensions, and precipitates of poly(1,6-di-p-toluene sulfonoxy-2,4-hexadiyne) in and from nitrobenzene, acetone, and chloroform are presented. These are interpreted in terms of the occurrence of two forms of the polymer chain; a quasicrystalline form with properties close to those of single crystal polymer and a chain-extended form occurring in solution and colloidal particles, with an absorption energy of about 2.5 eV (20,000 cm-1). No evidence is found for the presence of very short polymer chains in partially polymerized monomer at low conversion. The relationship of these results to those for deformed single crystals is briefly discussed.
    Additional Material: 9 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/pol.1981.180190212
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  • 4
    Electronic Resource
    Electronic Resource
    Copolymerization of styrene and diethyl fumarate with ZnBr2. IV. Comparison between photoinitiation and electroinitiation (1972)
    New York : Wiley-Blackwell
    Journal of Polymer Science Part A-1: Polymer Chemistry 10 (1972), S. 3253-3265 
    Details
    ISSN: 0449-296X
    Keywords: Physics ; Polymer and Materials Science
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology
    Notes: A comparative analysis of photoinitiation and electroinitiation can help elucidate initiation processes in donor-acceptor charge-transfer copolymerization. The technique has been applied to the zinc bromide-catalyzed copolymerization of styrene and diethyl fumarate in methanol. The photocopolymer product was analyzed by GPC, NMR, and elemental analysis. The results showed that 1:1 copolymers were formed initially, but changes occurred in both the kinetics and products after the early stages of the reaction. Significant correlations found between the two initiation methods included the initial kinetic order with respect to the initiating process and the effect on product yield of equivalent increases in total initiation energy. The limiting value of zinc bromide for both initiation methods was found to be the same. The data obtained support the contention that the copolymerization proceeds through a donor-acceptor process and that photoactivation of the preformed complex, inducing electron transfer, is a likely initiation process.
    Additional Material: 9 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/pol.1972.170101112
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  • 5
    Electronic Resource
    Electronic Resource
    Copolymerization of styrene and diethyl fumarate with zinc bromide. III. Electroinitiation at low current densities (1972)
    New York : Wiley-Blackwell
    Journal of Polymer Science Part A-1: Polymer Chemistry 10 (1972), S. 3267-3277 
    Details
    ISSN: 0449-296X
    Keywords: Physics ; Polymer and Materials Science
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology
    Notes: The electroinitiated preparation of equimolar copolymers of styrene and diethyl fumarate is described. The reaction medium consisted of these monomers dissolved in a methanol-zinc bromide solution. Rates of polymerization increased with increasing applied current and the copolymer yield increased linearly with the total number of Faradays transferred. The copolymer composition is 1:1 and is essentially invariant with the degree of conversion (〈15%), electroinitiation rate, and monomer feed ratios. A reaction mechanism involving donor-acceptor complexes and electroinitiated excitation of these complexes at the electrode is postulated.
    Additional Material: 5 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/pol.1972.170101113
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  • 6
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    Pioneer 10 observations of the solar wind interaction with Jupiter (1974)
    In:  Other Sources
    Details
    Publication Date: 2011-08-16
    Description: Detailed analysis of the Pioneer 10 plasma analyzer experiment flight data during the Jupiter flyby in late November and early December 1973 has been performed. The observations show that the interaction of Jupiter's magnetic field with the solar wind is similar in many ways to that at earth, but the scale size is over 100 times larger. Jupiter is found to have a detached standing bow shock wave of high Alfven Mach number. Like the earth, Jupiter has a prominent magnetopause that deflects the magnetosheath plasma and excludes its direct entry into the Jovian magnetosphere. Unlike that of the earth, the sunward hemisphere of Jupiter's outer magnetosphere is found to be highly inflated with thermal plasma and a high-beta region that is highly responsive to changes in solar wind dynamic pressure.
    Keywords: SPACE RADIATION
    Type: Journal of Geophysical Research; 79; Sept. 1
    Format: text
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  • 7
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    Arcsecond Positions for Milliarcsecond VLBI Nuclei of Extragalactic Radio Sources, Part 2: 207 Sources (1984)
    In:  CASI
    Details
    Publication Date: 2014-09-11
    Description: Very long base interferometry measurements of time delay and fringe frequency at 2.29 GHz on baselines of 10,000 km between Deep Space Network stations were used to determine the positions of the milliarcsecond nuclei in 207 extragalactic radio sources. Estimated accuracies generally range from approximately 0.1 to approximately 1.0, in both right ascension and declination, with all sources having uncertainties 4" in both coordinates. The observed sources are part of an all-sky VLBI catalog of milliarcsecond radio sources. Arcsecond positions are now determined for 752 of these sources. Arcsecond positions serve as a useful starting point in the construction of high-precision VLBI reference frames and are also important for unambiguous determination of optical counterparts to compact radio sources.
    Keywords: SPACE RADIATION
    Type: The Telecommun. and Data Acquisition Rept.; p 1-11
    Format: text
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  • 8
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    Pioneer 10 observations of the solar wind interation with Jupiter (1974)
    In:  CASI
    Details
    Publication Date: 2019-06-27
    Description: Pioneer 10 Plasma Analyzer experiment flight data during the Jupiter flyby are presented. The observations show that the interaction of Jupiter's magnetic field with the solar wind is similar in many ways to that at earth, but the scale size is over 100 times larger. Jupiter is found to have a detached standing bow shock wave of high Alfven Mach number. Jupiter has a prominent magnetopause which deflects the magnetosheath plasma and excludes its direct entry into the Jovian magnetosphere. The sunward hemisphere of Jupiter's outer magnetosphere is found to be highly inflated with thermal plasma and a high beta region which is highly responsive to changes in solar wind dynamic pressure. Observational arguments are presented which tend to discount a thin disklike magnetosphere but, rather, favor a Jovian magnetosphere, albeit probabily considerably flattened as compared to the earth's magnetosphere, yet still with reasonable thickness. Results concerning the shock jump conditions, the magnetosheath flow field and inferred internal magnetospheric plasma are presented.
    Keywords: SPACE RADIATION
    Type: NASA-TM-X-62357
    Format: application/pdf
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  • 9
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    Composition of interplanetary particles at energies from 0.1 to 150 MeV/nucleon, part B (1972)
    In:  CASI
    Details
    Publication Date: 2005-11-30
    Description: During the Apollo 16 mission, a solar flare produced an enormous amount of low-energy nuclei, many orders of magnitude greater than the level inferred from studies of tracks in the window of the Apollo 12 spacecraft during a time when the sun was quiet. The differential energy spectrum of nuclei with Z less than or equal to 6 falls by seven orders of magnitude over the interval from 0.1 to 20 MeV/nucleon, then remains almost flat up to approximately 100 MeV/nucleon. The two parts correspond to contributions from the sun and from galactic cosmic rays. Any maximum in the spectrum occurs below the lowest energy studied.
    Keywords: SPACE RADIATION
    Type: NASA. Lyndon B. Johnson Space Center Apollo 16 Prelim. Sci. Rept.; 8 p
    Format: text
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  • 10
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    Searches for gamma ray emission from radio pulsars (1983)
    In:  Other Sources
    Details
    Publication Date: 2011-08-18
    Description: Searches were made for pulsed high energy (E greater than 35 MeV) gamma radiation from 43 pulsars using the SAS-2 data base and radio parameters. No positive results were found, and the upper limits are consistent with the concept that gamma ray production efficiency increases with increasing apparent age. Two limits suggest that efficiency cannot be a simple function of apparent age beyond 1,000,000 years. Previously announced in STAR as N83-24463
    Keywords: SPACE RADIATION
    Type: Astronomy and Astrophysics (ISSN 0004-6361); 127; 1, Oc
    Format: text
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