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  • ENERGY PRODUCTION AND CONVERSION  (133)
  • Analytical Chemistry and Spectroscopy  (98)
  • SOLAR PHYSICS  (65)
  • 1980-1984  (296)
  • 1981  (296)
Collection
Keywords
Publisher
Years
  • 1980-1984  (296)
Year
  • 1
    Electronic Resource
    Electronic Resource
    NQR investigations of 35Cl in crystalline 2,5-dichloro-4-nitroaniline (1981)
    Chichester : Wiley-Blackwell
    Organic Magnetic Resonance 16 (1981), S. 123-125 
    Details
    ISSN: 0030-4921
    Keywords: Chemistry ; Analytical Chemistry and Spectroscopy
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology
    Notes: Two NQR lines were observed for 35Cl in 2,5-dichloro-4-nitroaniline at room temperature, using a self-quenched super-regenerative spectrometer. Analysis of the Zeeman effect on the two lines using a cylindrical single crystal reveals that the crystal belongs to the monoclinic system. The principal field gradient Z axes enclose an angle of 35° and 28° in the cases of the low and high frequency resonance lines, respectively. The b axis is parallel to 81°, 280°. The unit cell contains either two or a multiple of two molecules. The molecules in the crystal can be arranged into two sets, with the molecular planes in each set being parallel among each other. The angle subtended between the two planes is 159° and each of the planes is inclined to the b axis at an angle of 79.5°. There is an in-plane bending of the two C—Cl bonds by 5.5°. The ionic, single bond and double bond characters of the C—Cl bonds for both chlorines are almost equal, and are in the ratio 24:73:3.
    Additional Material: 3 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/mrc.1270160212
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    Paper (German National Licenses)
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  • 2
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    Analysis of DSN software anomalies (1981)
    In:  CASI
    Details
    Publication Date: 2019-06-28
    Description: A categorized data base of software errors which were discovered during the various stages of development and operational use of the Deep Space Network DSN/Mark 3 System was developed. A study team identified several existing error classification schemes (taxonomies), prepared a detailed annotated bibliography of the error taxonomy literature, and produced a new classification scheme which was tuned to the DSN anomaly reporting system and encapsulated the work of others. Based upon the DSN/RCI error taxonomy, error data on approximately 1000 reported DSN/Mark 3 anomalies were analyzed, interpreted and classified. Next, error data are summarized and histograms were produced highlighting key tendencies.
    Keywords: ENERGY PRODUCTION AND CONVERSION
    Type: NASA-CR-164369 , JPL-9950-536 , RCI-TR-005 , LO-726925
    Format: application/pdf
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    NASA TECHNICAL REPORTS
  • 3
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    Assessment of disk MHD generators for a base load powerplant (1981)
    In:  CASI
    Details
    Publication Date: 2019-07-13
    Description: Results from a study of the disk MHD generator are presented. Both open and closed cycle disk systems were investigated. Costing of the open cycle disk components (nozzle, channel, diffuser, radiant boiler, magnet and power management) was done. However, no detailed costing was done for the closed cycle systems. Preliminary plant design for the open cycle systems was also completed. Based on the system study results, an economic assessment of the open cycle systems is presented. Costs of the open cycle disk conponents are less than comparable linear generator components. Also, costs of electricity for the open cycle disk systems are competitive with comparable linear systems. Advantages of the disk design simplicity are considered. Improvements in the channel availability or a reduction in the channel lifetime requirement are possible as a result of the disk design.
    Keywords: ENERGY PRODUCTION AND CONVERSION
    Type: NASA-TM-82609 , DOE/NASA/10769-17 , E-849 , Symp. on Engr. Aspects of Magnetohydrodyn.; Jun 15, 1981 - Jun 17, 1981; Tullahoma, TN; United States
    Format: application/pdf
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    NASA TECHNICAL REPORTS
  • 4
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    Applicability of advanced automotive heat engines to solar thermal power (1981)
    In:  CASI
    Details
    Publication Date: 2019-07-13
    Description: The requirements of a solar thermal power system are reviewed and compared with the predicted characteristics of automobile engines under development. A good match is found in terms of power level and efficiency when the automobile engines, designed for maximum powers of 65-100 kW (87 to 133 hp) are operated to the nominal 20-40 kW electric output requirement of the solar thermal application. At these reduced power levels it appears that the automotive gas turbine and Stirling engines have the potential to deliver the 40+ percent efficiency goal of the solar thermal program.
    Keywords: ENERGY PRODUCTION AND CONVERSION
    Type: NASA-TM-81658 , E-675 , DOE/NASA/1060-4 , SAE Intern. Eng. Congr. and Exposition,; Feb 23, 1981 - Feb 27, 1981; Detroit, MI; United States
    Format: application/pdf
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    NASA TECHNICAL REPORTS
  • 5
    Electronic Resource
    Electronic Resource
    1H and 13C NMR study of 8-hydroxyquinoline and some of its 5-substituted analogues (1981)
    Chichester : Wiley-Blackwell
    Organic Magnetic Resonance 15 (1981), S. 280-284 
    Details
    ISSN: 0030-4921
    Keywords: Chemistry ; Analytical Chemistry and Spectroscopy
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology
    Notes: 1H and 13C NMR spectra of 8-hydroxyquinoline (oxine) and its 5-Me, 5-F, 5-Cl, 5-Br and 5-NO2 derivatives have been studied in DMSO-d6 solution. The 1H and 13C chemical shifts and proton-proton, proton-fluorine, carbon-proton and carbon-fluorine coupling constants have been determined. The 1H and 13C chemical shifts have been correlated with the charge densities on the hydrogen and carbon atoms calculated by the CNDO/2 method. The correlation of the 1H and 13C chemical shifts with the total charge densities on the carbon atoms is approximately linear (rH2 = 0.85, rC2 = 0.84). The proton in peri position to the nitro group in 5-NO2-oxine is an exception.
    Additional Material: 2 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/mrc.1270150314
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  • 6
    Electronic Resource
    Electronic Resource
    Carbon-13 NMR studies of benzoquinones (1981)
    Chichester : Wiley-Blackwell
    Organic Magnetic Resonance 15 (1981), S. 311-316 
    Details
    ISSN: 0030-4921
    Keywords: Chemistry ; Analytical Chemistry and Spectroscopy
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology
    Notes: The assignment of all ring carbons of p-benzoquinones derived from perezone and from thymoquinone was completed using gated decoupled spectra. The long range proton-carbon couplings are discussed in terms of the degree of substitution of the quinone ring. The tautomeric interconversion of the two energetically equivalent forms of 2,5-dihydroxy-1,4-benzoquinones has been studied in various solvents and at several temperatures.
    Additional Material: 2 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/mrc.1270150321
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  • 7
    Electronic Resource
    Electronic Resource
    Examination of the aspirin acetylation site of human serum albumin by 13C NMR spectroscopy (1981)
    Chichester : Wiley-Blackwell
    Organic Magnetic Resonance 15 (1981), S. 158-161 
    Details
    ISSN: 0030-4921
    Keywords: Chemistry ; Analytical Chemistry and Spectroscopy
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology
    Notes: Human serum albumin has been specifically acetylated using aspirin in which the methyl carbon of the acetyl group was enriched to 90% 13C. A single resonance at 23.13 ppm downfield from tetramethylsilane was observed in 13C differences spectra obtained at both 25.2 and 45.3 MHz. Chemical shift studies of several model compounds suggest that this is the resonance position to be expected for an acetamide group exposed to solvent. The line width observed for the enriched methyl resonance is consistent with free rotation of the methyl group.
    Additional Material: 1 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/mrc.1270150210
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  • 8
    Electronic Resource
    Electronic Resource
    Carbon-13 NMR characterization of the bispyridinium oximes, toxogonin, HS-3, HS-6 and HI-6 (1981)
    Chichester : Wiley-Blackwell
    Organic Magnetic Resonance 16 (1981), S. 7-10 
    Details
    ISSN: 0030-4921
    Keywords: Chemistry ; Analytical Chemistry and Spectroscopy
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology
    Notes: The structure of the bispyridinium oximes, toxogonin, HS-3, HS-6 and HI-6, used as antidotes in organophosphorus poisoning, is confirmed by 13C NMR spectroscopy. The 13C NMR spectra of the corresponding monopyridinium precursors substantiate the signal assignment in the bispyridinium oxime spectra. In all oximes studied the hydroxyiminomethyl group (—CH=N—OH) exists in the syn configuration. The 13C signal differences also readily allow analysis of binary mixtures of the oximes and provide an easy method for monitoring their stability.
    Additional Material: 1 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/mrc.1270160103
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  • 9
    Electronic Resource
    Electronic Resource
    A chemical ionization gas chromatographic mass spectrometric assay for octopamine and tyramine in rat brain (1981)
    Chichester : Wiley-Blackwell
    Biological Mass Spectrometry 8 (1981), S. 170-173 
    Details
    ISSN: 1052-9306
    Keywords: Chemistry ; Analytical Chemistry and Spectroscopy
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology
    Notes: A method has been developed for the quantitation of the putative phenolamine neurotransmitter octopamine, and its precursor tyramine, in brain tissue. The procedure employs methane chemical ionization of the pentafluoropropionate derivatives of octopamine and tyramine together with the use of deuterated internal standards and selected ion monitoring. Deuterated analogues of octopamine and tyramine are added to brain homogenates in aqueous perchloric acid and ion exchange is used to isolate the brain amines. The method is capable of measuring 20 pg of octopamine and tyramine. The measured concentration (ng g-1 wet tissue) of octopamine and tyramine in rat brain was as follows: whole brain (less cerebellum) (0.6 and 2.2); hypothalamus (3.2 and tyramine value not statistically significant); striatum (0.5 and 11.8) and cortex (0.6 and 1.0). Administration of pargyline resulted in an increase (around ten-fold) in octopamine and tyramine concentration in all the above brain regions. In contrast α-methyltyrosine produced only a small increase (50%) in the concentration of tyramine in the striatum.
    Additional Material: 1 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/bms.1200080408
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  • 10
    Electronic Resource
    Electronic Resource
    Obtaining quantitative data for PNAs with capillary column gas chromatography using split and splitless injectionWork supported by the U. S. Department of Energy Under Contract DE-AC06-76RLO 1830. (1981)
    Weinheim : Wiley-Blackwell
    Journal of High Resolution Chromatography 4 (1981), S. 638-641 
    Details
    ISSN: 0935-6304
    Keywords: Gas chromatography ; Capillary, fused silica ; Split injection ; Splitless injection ; Polynuclear aromatic hydrocarbons, quantitation ; Chemistry ; Analytical Chemistry and Spectroscopy
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology
    Additional Material: 1 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/jhrc.1240041206
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