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  • 1
    Electronic Resource
    Electronic Resource
    Effect of thermal treatment on the electrothermographic and electrical properties of poly(acrylonitrile butadiene styrene) (1985)
    Weinheim : Wiley-Blackwell
    Angewandte Makromolekulare Chemie 130 (1985), S. 91-97 
    Details
    ISSN: 0003-3146
    Keywords: Chemistry ; Polymer and Materials Science
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology , Physics
    Description / Table of Contents: Es wurden Untersuchungen zum elektrothermographischen und zum Leitfähigkeitsverhalten von Poly(Acrylnitril-Butadien-Styrol) (ABS) nach unterschiedlichen thermischen Vorbehandlungen durchgeführt. Die spezifischen Widerstände von bei 50°C gelagerten ABS-Platten erwiesen sich als klein (∼ 1015 Ω · cm). Auch die Ladungsaufnahme und die Ladungsspeicherung waren schlecht. Der Grund dafür ist die Adsorption von Wassermolekülen. Werden die Platten bei 100°C oder mehr für 5 h thermisch beansprucht, zeigen sie erhöhte spezifische Widerstände (∼ 1017 Ω· cm bei 50°C) und haben deshalb eine bessere Ladungsaufnahme und -speicherung. Sowohl Umwelt- und Lagerungsbedingungen als auch eine thermische Behandlung während der Herstellung der Platten haben unterhalb 110°C keinen Einfluß auf die Temperaturabhängigkeit der spezifische Widerstände.
    Notes: Studies on the electrothermographic and conductivity behaviour of poly(acrylonitrile butadiene styrene) (ABS) films of different thermal pretreatments were carried out. The resistivity in ABS layers stored at 50°C was found to be low (∼ 1015 Ω · cm). The charge acceptance and its retention also is poor. The reason for that is the adsorption of water molecules. The layers, when thermally treated at 100°C or more for 5 h, show an enhanced resistivity (∼ 1017 Ω · cm at 50°C) and hence an improvement in charge acceptance as well as in charge retention. Environmental and storage conditions as well as thermal treatment during layer preparations have no effect on the temperature dependence of the resistivity beyond 110°C.
    Additional Material: 3 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/apmc.1985.051300107
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  • 2
    Electronic Resource
    Electronic Resource
    Effect of forming conditions and sensitization on temperature dependence of d. c. conductivity of cellulose acetate (1986)
    Weinheim : Wiley-Blackwell
    Acta Polymerica 37 (1986), S. 634-637 
    Details
    ISSN: 0323-7648
    Keywords: Chemistry ; Polymer and Materials Science
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology , Physics
    Description / Table of Contents: Die Temperaturabhängigkeit der Gleichstromleitfähigkeit von unterschiedlich thermisch vorbehandelten Celluloseacetatfilmen wurde untersucht. Die Ergebnisse werden mit elektrothermographischen Parametern, wie der Ladungsaufnahme und dem Ladungsrückhaltevermögen, korreliert. Weiterhin wurde der Einfluß einer Sensibilisierung des Polymers mit Leucomalachitgrün auf die Leitfähigkeit ermittelt.
    Notes: Studies on the temperature dependence of d.c. conductivity of cellulose acetate films with different thermal treatment were carried out. The results were correlated with electrothermographic parameters like charge acceptance and retentivity. Further the effect of sensitization with leucomalachite green on the conductivity of the polymer was investigated.
    Additional Material: 5 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/actp.1986.010371008
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  • 3
    Electronic Resource
    Electronic Resource
    Temperature-dependent charging currents in poly(methyl methacrylate) and leucomalachite green mixed system (1987)
    Weinheim : Wiley-Blackwell
    Acta Polymerica 38 (1987), S. 199-200 
    Details
    ISSN: 0323-7648
    Keywords: Chemistry ; Polymer and Materials Science
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology , Physics
    Additional Material: 3 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/actp.1987.010380310
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  • 4
    Electronic Resource
    Electronic Resource
    Effect of thickness on surface potential characteristics of corona charged poly(acrylonitrile-butadiene-styrene) layers (1989)
    Weinheim : Wiley-Blackwell
    Acta Polymerica 40 (1989), S. 552-553 
    Details
    ISSN: 0323-7648
    Keywords: Chemistry ; Polymer and Materials Science
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology , Physics
    Additional Material: 3 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/actp.1989.010400815
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  • 5
    Electronic Resource
    Electronic Resource
    On the thickness and spatial distribution of a fluoropolymer film deposited by solution dipping (1980)
    New York, NY [u.a.] : Wiley-Blackwell
    Journal of Applied Polymer Science 25 (1980), S. 211-222 
    Details
    ISSN: 0021-8995
    Keywords: Chemistry ; Polymer and Materials Science
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology , Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics , Physics
    Notes: Poly-1H,1H-pentadecafuorooctyl methacrylate is a barrier compound used to prevent silicone oil from creeping to relay contacts. It is essentially a methyl methacrylate polymer with a fluorocarbon side chain substituted for one of the methyl hydrogens. It is applied by dipping the part into a solution, with Freon TF as the solvent and the fluorocarbon polymer as the solute. This work considers the spatial distribution of the resulting film of barrier compound when it is deposited in this manner. The specific variables considered are concentration and withdrawal velocity. The samples were withdrawn from the solution with velocity perpendicular to the surface, and we show that the macrosopic uniformity and thickness of the film is dependent on this velocity. There exists a critical velocity (dependent on concentration) above which the film is nonuniform and below which the film is macroscopically uniform. Below the critical velocity, the thickness varies with velocity with approximately a v2/3 dependence. The critical velocity is about 13 mm/sec for a concentration of 0.2%. For macroscopically uniform films, a microscopic nonunitormity exists with a coverage of about 1/4 for an average film thickness of 90 Å.
    Additional Material: 6 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/app.1980.070250207
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  • 6
    Electronic Resource
    Electronic Resource
    The effect of stretching conditions on properties of amorphous polyethylene terephthalate film (1987)
    New York, NY [u.a.] : Wiley-Blackwell
    Journal of Applied Polymer Science 34 (1987), S. 2231-2247 
    Details
    ISSN: 0021-8995
    Keywords: Chemistry ; Polymer and Materials Science
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology , Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics , Physics
    Notes: The effect of stretching condition on stress-induced crystallization of amorphous polyethylene terephthalate (PET) film has been studied. Cast PET film was stretched at 85°C with stretching rates ranging from 100% per minute to 600% per minute for various stretching ratios. The stretched film samples were annealed at 140°C both under tension as well as under relaxed conditions. Tensile properties were determined using Instron Tensile Tester and results were compared. Tenacity, yield stress, and initial modulus were found to increase while elongation at break decreased with the increase in stretching rate. The degree of crystallinity was measured by x-ray diffraction as well as density methods. Birefringence and crystalline orientation factor values were determined experimentally and using these, amorphous orientation factor values were calculated. Birefringence, crystalline orientation and amorphous orientation values were found to increase with the increase in stretching rate. These studies showed that at low stretching rates a significant amount of relaxation takes place, resulting in lower orientation and strength. On the other hand, at higher stretching rates relaxation is minimized thus providing high orientation and strength. Upon annealing the crystallinity values increased as expected, however the trend of orientation and mechanical properties with respect to stretching rate was similar to those of unannealed films.
    Additional Material: 17 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/app.1987.070340615
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  • 7
    Electronic Resource
    Electronic Resource
    Correction factors for sizing weakly anisotropic transparent fibers using light scattering (1984)
    New York : Wiley-Blackwell
    Journal of Polymer Science: Polymer Physics Edition 22 (1984), S. 647-653 
    Details
    ISSN: 0098-1273
    Keywords: Physics ; Polymer and Materials Science
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology , Physics
    Notes: Correction factors defined as the ratio of the true size parameter and the size parameter deduced from Fraunhofer diffraction theory are presented for weakly anisotropic transparent fibers. These correction factors enable the Fraunhofer diffraction approximation to be used for sizing weakly anisotropic fibers from light-scattering measurements. Fibers in the diameter range 4-50 μm and refractive index range 1.45-1.56 are considered. It is shown that for fibers having birefringence -0.005 ≤ Δm ≤ 0.01, the diameters may be obtained to within 9% accuracy if the fiber diameter lies between 4 and 50 μm.
    Additional Material: 4 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/pol.1984.180220408
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  • 8
    Electronic Resource
    Electronic Resource
    Studies of conformational isomerism in α-melanocyte stimulating hormone by design of cyclic analogues (1998)
    New York : Wiley-Blackwell
    Biopolymers 46 (1998), S. 155-167 
    Details
    ISSN: 0006-3525
    Keywords: α-MSH ; [D-Phe7]α-MSH ; isomerism ; cyclic analogues ; Chemistry ; Polymer and Materials Science
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology
    Notes: Results of energy calculations for α-MSH (α-melanocyte stimulating hormone, Ac-Ser1-Tyr2-Ser3-Met4-Glu5-His6-Phe7-Arg8-Trp9-Gly10-Lys11-Pro12-Val13-NH2) and [D-Phe7]α-MSH were used for design of cyclic peptides with the general aim to stabilize different conformational isomers of the parent compound. The minimal structural modifications of the conformationally flexible Gly10 residue, as substitutions for L-Ala, D-Ala, or Aib (replacing of hydrogen atoms by methyl groups), were applied to obtain octa- and heptapeptide analogues of α-MSH(4-11) and α-MSH(5-11), which were cyclized by lactam bridges between the side chains in positions 5 and 11. Some of these analogues, namely those with substitutions of the Gly10 residue with L-Ala or Aib, showed biological activity potencies on frog skin comparable to the potency of the parent tridecapeptide hormone. Additional energy calculations for designed cyclic analogues were used for further refinement of the model for the biologically active conformations of the His-Phe-Arg-Trp “message” sequence within the sequences of α-MSH and [D-Phe7]α-MSH. In such conformations the aromatic moieties of the side chains of the His6, L/D-Phe7, and Trp9 residues form a continuous hydrophobic “surface,” presumably interacting with a complementary receptor site. This feature is characteristic for low-energy conformers of active cyclic analogues, but it is absent in the case of inactive analogues. This particular spatial arrangement of functional groups involved in the message sequence is very close for α-MSH and [D-Phe7]α-MSH, as well as for biologically active cyclic analogues despite differences of dihedral angle values for corresponding low-energy conformations. © 1998 John Wiley & Sons, Inc. Biopoly 46: 155-167, 1998
    Additional Material: 4 Ill.
    Type of Medium: Electronic Resource
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  • 9
    Electronic Resource
    Electronic Resource
    Raman spectral study of solid and dissolved poly(vinyl alcohol) and ethylene-vinyl alcohol copolymer (1994)
    Bognor Regis [u.a.] : Wiley-Blackwell
    Journal of Polymer Science Part B: Polymer Physics 32 (1994), S. 1163-1174 
    Details
    ISSN: 0887-6266
    Keywords: poly(vinyl alcohol) ; raman spectroscopy ; polymer ; aqueous solution ; Chemistry ; Polymer and Materials Science
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology , Physics
    Notes: We have measured the Raman spectra of ethylene-vinyl alcohol copolymer (EVOH) and poly(vinyl alcohol) (PVOH). Spectra of 88% hydrolyzed PVOH were examined from the partially crystalline solid, from PVOH dissolved in both H2O and D2O, and from films precipitated from these solutions. The spectrum in H2O differs from that of the starting material by disappearance of sharp bands having Raman shift values of 1146 and 1093 cm-1, strengthening of a band near 915 cm-1, decrease in frequency of bands at 480, 1356, and 1441 cm-1, and increase in frequency of bands at 369, 413, 1023, 1371, and 2910 cm-1. The spectrum of the film shows partial reversal of these trends. With D2O as the solvent, the band shifts are slightly different from those listed above and new bands appear. These changes are indicative of loss of crystallinity, change in stereochemistry, and partial deuteration of hydroxyl during dissolution of this PVOH sample at room temperature. © 1994 John Wiley & Sons, Inc.
    Additional Material: 5 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/polb.1994.090320704
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  • 10
    Electronic Resource
    Electronic Resource
    Examination of elemental nonuniformities in laser surface melted ternary copper alloys (1980)
    Chichester [u.a.] : Wiley-Blackwell
    Surface and Interface Analysis 2 (1980), S. 179-182 
    Details
    ISSN: 0142-2421
    Keywords: Chemistry ; Polymer and Materials Science
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Physics
    Notes: The enhanced corrosion resistance of laser melted surfaces is often rationalized from the viewpoint of the homogenizing nature of the rapid quench from the liquid. We utilize Auger spectroscopy to examine elemental nonuniformities in laser surface melted ternary copper alloys (CDA-614 and CDA-725). In both systems we find depletion of the highest vapor pressure element from the central area of laser melt stripes, that region which reaches the highest temperature and remains molten for the greatest period of time. Although this near surface depletion is a small effect relative to the homogenization taking place over the orders of 10 and 102 µm, it may be a significant effect which should be taken into account when explaining changes in corrosion and oxidation behavior.
    Additional Material: 3 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/sia.740020505
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