ISSN:
1612-1112
Keywords:
Column liquid chromatography
;
Pre-column derivatisation
;
Morpholine and degradation products
;
Boiler feed water
Source:
Springer Online Journal Archives 1860-2000
Topics:
Chemistry and Pharmacology
Notes:
Summary Morpholine and its amine-type thermal degradation products present in boiler feed water and steam condensate were derivatised with N-succinimidyl-p-nitrophenylacetate. These pre-column derivatives were determined by high-performance liquid chromatography with UV detection at 280 nm. The analytical column was Supelco-sil-ODS with an isocratic mobile phase. Morpholine and its breakdown products were monitored in the range 0.01–10 μg ml−1 with a relative standard deviation of 0.4–3.0%. Chromatographic analysis of boiler feed water and steam condensate samples collected from a boiler servicing a petroleum refinery is described.
Type of Medium:
Electronic Resource
URL:
http://dx.doi.org/10.1007/BF02269698
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