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  • Chemical Engineering  (8)
  • Analytical Chemistry and Spectroscopy  (5)
  • BIOTECHNOLOGY  (4)
  • 1
    Electronic Resource
    Electronic Resource
    Laser desorption/fourier transform mass spectra of glycoalkaloids and steroid glycosides (1986)
    Chichester : Wiley-Blackwell
    Biological Mass Spectrometry 13 (1986), S. 199-204 
    Details
    ISSN: 1052-9306
    Keywords: Chemistry ; Analytical Chemistry and Spectroscopy
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology
    Notes: Positive- and negative-ion mass spectra of five glycoconjugates were obtained using laser desorption/Fourier transform mass spectrometry. These were the glycoalkaloids α-solanine and α-tomatine and the steroid glycosides gitoxin, lanatoside A and digitonin. Doping with KCl yielded both potassium- and chloride-attachment ions. Few fragment ions were observed for these species, with the exception of digitonin, although the negative-ion spectra showed relatively more fragmentation than the positive-ion spectra. All major fragments appeared to arise from losses of sugar groups due to cleavages at the glycosidic linkages. This contrasted sharply with the behavior of the malto-oligosaccharides studied in this laboratory.
    Additional Material: 6 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/bms.1200130409
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  • 2
    Electronic Resource
    Electronic Resource
    Laser desorption fourier transform mass spectra of malto-oligosaccharides (1985)
    Chichester : Wiley-Blackwell
    Biological Mass Spectrometry 12 (1985), S. 424-428 
    Details
    ISSN: 1052-9306
    Keywords: Chemistry ; Analytical Chemistry and Spectroscopy
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology
    Notes: Laser desorption mass spectra of malto-oligomers, including starch, have been obtained using Fourier transform mass spectrometry. Fragmentations of these oligomers have been examined after doping with metal salts to obtain cation-attachment ions. Doping starch with NaCl, KBr and Ag2O results in analogous cation-attachment oligosaccharide fragment ions for all three metal ions. A distinct and unusual fragmentation pattern is observed for the larger oligomers.
    Additional Material: 3 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/bms.1200120812
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  • 3
    Electronic Resource
    Electronic Resource
    Measurement of (C13)arginine incorporation into apolipoprotein B-100 in very low density lipoproteins and low density lipoproteins in normal subjects using (13C)sodium bicarbonate infusion and isotope ratio mass spectrometry (1990)
    Chichester : Wiley-Blackwell
    Biological Mass Spectrometry 19 (1990), S. 459-464 
    Details
    ISSN: 1052-9306
    Keywords: Chemistry ; Analytical Chemistry and Spectroscopy
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology
    Notes: We describe a new stable isotope technique for the in vivo study of hepatic plasma protein synthesis in humans. The method involves the infusion of (13C)sodium bicarbonate for 1 h and the measurement of the isotopic enrichment of (13C)arginine in newly synthesized apolipoprotein B of very low density lipoproteins (VLDL-apoB) and low density lipoproteins (LDL-apoB) in blood samples taken over a 5-6 h period from the commencement of the infusion. Isotope ratio mass spectrometry was utilized to measure 13CO2 enrichment following hydrolysis of these proteins and conversion of the guanidinium carbon of arginine in the hydrolysate to carbon dioxide by sequential incubation with arginase and urease. The method is capable of measuring isotopic enrichment as low as 0.001 at. % excess (APE) with a precision of 1.2%. In both subjects studied, the (13C)arginine of VLDL-apoB reached enrichments of 0.2 APE and that of the arginine of LDL-apoB, 0.03 APE. Incorporation of labeled arginine into LDL-apoB was demonstrable at 60-90 min. The new technique is safe and is applicable to the study of the hepatic biosynthesis of a wide range of plasma proteins.
    Additional Material: 5 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/bms.1200190803
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  • 4
    Electronic Resource
    Electronic Resource
    Novel reinforced reaction injection molding (RRIM) processing: Computer-controlled multiple-stream RRIM production of interpenetrating polymer networks and polyurethanes (1987)
    Stamford, Conn. [u.a.] : Wiley-Blackwell
    Polymer Engineering and Science 27 (1987), S. 1209-1215 
    Details
    ISSN: 0032-3888
    Keywords: Chemistry ; Chemical Engineering
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology , Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics , Physics
    Notes: A four-stream computer-controlled reinforced reaction injection molding (RRIM) machine has been developed that attains high accuracy in dispense ratios throughout the injection period. This machine has been used for novel processing of polyurethanes, offering a route to varying product properties either throughout a shot or on a shotto-shot basis. It also has been used for what appears to be the first production on commercial scale RRIM equipment of a polyurethane-acrylic interpenetrating polymer network (IPN) in commercial cycle times of around 2 min.
    Additional Material: 5 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/pen.760271602
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  • 5
    Electronic Resource
    Electronic Resource
    Die drawing: Solid phase drawing of polymers through a converging die (1981)
    Stamford, Conn. [u.a.] : Wiley-Blackwell
    Polymer Engineering and Science 21 (1981), S. 612-618 
    Details
    ISSN: 0032-3888
    Keywords: Chemistry ; Chemical Engineering
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology , Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics , Physics
    Notes: Die drawing, a new process for the production of oriented thermoplastic rods with an ultrahigh modulus of elasticity, involves drawing an isotropic workpiece through a converging die at temperatures below the polymer melting point. Die drawing of polypropylene is described, but the process is applicable to any polymer which can be drawn by conventional means. The considerable advantages of die drawing compared with conventional tensile drawing and hydrostatic or ram extrusion are discussed.
    Additional Material: 12 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/pen.760211007
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  • 6
    Electronic Resource
    Electronic Resource
    Vapor-Liquid equilibrium relations predicted by thermodynamic examination of activity coefficients (1955)
    Hoboken, NJ : Wiley-Blackwell
    AIChE Journal 1 (1955), S. 241-246 
    Details
    ISSN: 0001-1541
    Keywords: Chemistry ; Chemical Engineering
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology , Process Engineering, Biotechnology, Nutrition Technology
    Additional Material: 5 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/aic.690010218
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  • 7
    Electronic Resource
    Electronic Resource
    Studies of thermal conductivity of liquids. Part I (1955)
    Hoboken, NJ : Wiley-Blackwell
    AIChE Journal 1 (1955), S. 275-288 
    Details
    ISSN: 0001-1541
    Keywords: Chemistry ; Chemical Engineering
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology , Process Engineering, Biotechnology, Nutrition Technology
    Notes: Values of thermal conductivity and temperature coefficients for fifty-three pure organic liquids, obtained with newly designed, extensively tested apparatus, are presented. For thirty-one of these liquids values of thermal conductivity or temperature coefficients have not been previously reported. The statisically determined maximum error in the presented values of thermal conductivity of liquids is ±1.50%.A method of correlating the thermal conductivity of liquids based on a modified statement of the theory of corresponding states is presented. Group contributions to the thermal conductivity were calculated. The thermal conductivity of liquids was predicted by this method and the average deviation of the calculated from the observed values for forty-seven liquids is ±1.50%. The proposed method of correlation permits the calculation of the thermal conductivity of a series of liquids at any temperature from a single known value.
    Additional Material: 1 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/aic.690010302
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  • 8
    Electronic Resource
    Electronic Resource
    Studies of thermal conductivity of liquids: Part III (1957)
    Hoboken, NJ : Wiley-Blackwell
    AIChE Journal 3 (1957), S. 121-126 
    Details
    ISSN: 0001-1541
    Keywords: Chemistry ; Chemical Engineering
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology , Process Engineering, Biotechnology, Nutrition Technology
    Notes: Values of thermal conductivity and temperature coefficients for thirty-five pure organic liquids, in addition to those previously reported, obtained with a previously described apparatus (Part I), are presented. Values of thermal conductivity or temperature coefficients for twenty-eight of these liquids have not been reported before. The experimentally determined maximum error is ±1.0%.The two methods for predicting the thermal conductivity of liquids previously proposed (Parts I and II) are extended to cover the types of compounds studied in this investigation, in particular ring compounds.The temperature coefficient of thermal conductivity was observed to decrease rapidly, approaching zero as the freezing point is approached. The existence of a transition temperature or region within the liquid state is shown and identified with the onset of molecular rotation.
    Additional Material: 3 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/aic.690030120
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  • 9
    Electronic Resource
    Electronic Resource
    Prediction of specific heat of organic liquids (1956)
    Hoboken, NJ : Wiley-Blackwell
    AIChE Journal 2 (1956), S. 88-93 
    Details
    ISSN: 0001-1541
    Keywords: Chemistry ; Chemical Engineering
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology , Process Engineering, Biotechnology, Nutrition Technology
    Notes: A theoretical equation is presented for predicting the specific heat at constant volume and constant pressure of organic liquids as a function of temperature from data on the velocity of sound, infrared and Raman spectra. By use of this equation, the average deviation of the calculated from the experimental values of specific heat for 100 organic liquids at 68°F. is ±1.5%.An alternate correlation for hydrocarbon liquids based on a modified statement of the theory of corresponding states is also presented. Based on it, the average deviation of the calculated from the experimental values for 100 points representing the entire temperature range is ±0.9%.
    Additional Material: 6 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/aic.690020119
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  • 10
    Electronic Resource
    Electronic Resource
    Activity coefficients at infinite dilution (1955)
    Hoboken, NJ : Wiley-Blackwell
    AIChE Journal 1 (1955), S. 496-500 
    Details
    ISSN: 0001-1541
    Keywords: Chemistry ; Chemical Engineering
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology , Process Engineering, Biotechnology, Nutrition Technology
    Notes: Equations are derived for obtaining activity coefficients at infinite dilution in binary systems by use of one of the following: (1) an isobaric temperature - liquid composition diagram, (2) an isobaric temperature - vapor composition diagram, (3) an isothermal pressure - liquid composition diagram, or (4) an isothermal pressure - vapor composition diagram. The derived equations are thermodynamically exact, and application involves no doubtful extrapolation of experimental data, as has heretofore been the case.Each equation involves the slope of one of the diagrams at the point corresponding to the pure component. Attention is called to the fact that data on the compositions of both the vapor and liquid phases in equilibrium are not required. Use of the equations is illustrated.
    Additional Material: 3 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/aic.690010419
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