ISSN:
1089-7623
Source:
AIP Digital Archive
Topics:
Physics
,
Electrical Engineering, Measurement and Control Technology
Notes:
In this paper, the performance of a novel high-pressure diamond-anvil powder x-ray diffractometer in Guinier geometry is reported. The diffractometer is a combination of a curved quartz-crystal monochromator, a Mao–Bell-type diamond-anvil cell, a flat position sensitive detector, and a Huber goniometer with compound stages to realize this geometry. The incident x-ray beam is from a rotating anode x-ray generator. It is shown that the above experimental arrangement results in an enhanced S/N ratio, improvement in resolution, and reduction of the data-acquisition time. Test results on UAl2 are presented to demonstrate the advantages of the setup in the study of phase transitions at high pressure. © 1995 American Institute of Physics.
Type of Medium:
Electronic Resource
URL:
http://dx.doi.org/10.1063/1.1145595
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