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  • 1
    Publikationsdatum: 2016-03-18
    Beschreibung: In this study, we have used in-situ micro-Laue diffraction combined with micropillar compression of focused ion beam milled Al 13 Co 4 complex metallic alloy to investigate the evolution of deformation in Al 13 Co 4 . Streaking of the Laue spots shows that the onset of plastic flow occurs at stresses as low as 0.8 GPa, although macroscopic yield only becomes apparent at 2 GPa. The measured misorientations, obtained from peak splitting, enable the geometrically necessary dislocation density to be estimated as 1.1 × 10 13  m −2 .
    Print ISSN: 0003-6951
    Digitale ISSN: 1077-3118
    Thema: Physik
    Standort Signatur Erwartet Verfügbarkeit
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  • 2
    Publikationsdatum: 2016-01-13
    Beschreibung: CrAlN/Si 3 N 4 nanocomposite coatings with different Si contents were deposited to understand how Si influences the microstructure and mechanical behaviour of the coatings, in particular, the fracture toughness. The coating composition, chemical bonding, microstructure, and mechanical properties were studied by energy dispersive spectroscopy, x-ray photoelectron spectroscopy, x-ray diffraction, and nanoindentation, respectively. Using a micro double cantilever beam sample, it was found that the fracture toughness of CrAlN/Si 3 N 4 coatings was higher than that of both the CrN and CrAlN coatings and increased with increasing Si content. Cross-sectional transmission electron microscopy suggested that this was caused by the suppression of cracking at columnar boundaries.
    Print ISSN: 0021-8979
    Digitale ISSN: 1089-7550
    Thema: Physik
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  • 3
    Digitale Medien
    Digitale Medien
    [S.l.] : American Institute of Physics (AIP)
    Journal of Applied Physics 76 (1994), S. 6371-6373 
    ISSN: 1089-7550
    Quelle: AIP Digital Archive
    Thema: Physik
    Notizen: The addition of Tb to melt spun iron-boron or iron-zirconium compounds raises the magneto- striction to practically useful levels (≥450 ppm) at room temperature. The present work examines the corresponding compositional and temperature dependencies of the magnetization in Tbx (Fe0.82B0.18)1−x for 0≤x≤0.5 and Tb y (Fe0.90Zr0.10)1−y for 0≤y≤0.1. Increasing the Tb content in Fe-B compounds decreases the room-temperature magnetization towards a compensation point and lowers the Curie temperature Tc. In Fe-Zr compounds, Tb increases the room-temperature magnetization and raises Tc. Magnetic phase diagrams are presented for each group of compounds and exchange frustration effects identified by comparing the observed temperature dependencies of the reduced magnetization with predictions from the Handrich mean field model. Only 3 at. % Tb in Fe-Zr is sufficient to annul exchange fluctuations, but in Fe-B compounds exchange frustration persists throughout the compositional range.
    Materialart: Digitale Medien
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  • 4
    Digitale Medien
    Digitale Medien
    [S.l.] : American Institute of Physics (AIP)
    Journal of Applied Physics 79 (1996), S. 6643-6645 
    ISSN: 1089-7550
    Quelle: AIP Digital Archive
    Thema: Physik
    Notizen: The effects of externally uniform applied orthogonal and parallel in-plane magnetic fields on the stripe-chopping characteristics and negative vertical Bloch line replication probability have been studied experimentally and by numerical simulation on a 5 μm bubble film. The orthogonal and parallel in-plane fields on the stripe domain were varied from −50 to 50 Oe and −9 to 9 Oe, respectively, to represent actual working device parameters. The numerical simulation results agree with the experimental data, confirming the suppression of horizontal Bloch line nucleation by the external-uniform in-plane fields and the in-plane field components of the chopping conductor. © 1996 American Institute of Physics.
    Materialart: Digitale Medien
    Standort Signatur Erwartet Verfügbarkeit
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  • 5
    Digitale Medien
    Digitale Medien
    [S.l.] : American Institute of Physics (AIP)
    Journal of Applied Physics 65 (1989), S. 2856-2858 
    ISSN: 1089-7550
    Quelle: AIP Digital Archive
    Thema: Physik
    Notizen: High critical-current densities, Jc, have been observed in single crystals and thin films of YBa2Cu3Ox. Jc in bulk materials is diappointingly low reaching a maximum in untextured material of about 103 A cm−2. The importance of raising Jc in bulk materials is paramount and most applications of bulk materials require high Jc in high magnetic fields. The work of Jin et al. in raising Jc to 17 000 A cm−2 in zero field represents a most important step in the development of bulk materials and gives real hope to bulk applications. In the communication we first describe the properties of untextured wire, and then we describe our process for melt texturing and the difficulties encountered.
    Materialart: Digitale Medien
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  • 6
    Digitale Medien
    Digitale Medien
    [S.l.] : American Institute of Physics (AIP)
    Review of Scientific Instruments 68 (1997), S. 4107-4119 
    ISSN: 1089-7623
    Quelle: AIP Digital Archive
    Thema: Physik , Elektrotechnik, Elektronik, Nachrichtentechnik
    Notizen: Fluorescence lifetime-resolved imaging (FLI) is a relatively new technique of fluorescence imaging whereby the spatial distribution of fluorescence decay times can be determined directly at every pixel of an image simultaneously. The fluorescence decay times of many chromophores can act as sensitive gauges of their molecular environments. By employing measurement techniques that are quantitatively related to the radiative dynamics of the dye molecules (in the nanosecond time range), additional physical parameters are available for discerning different fluorophores with disparate lifetimes, or for characterizing a single fluorophore in different surroundings. Many physical processes such as molecular aggregation, binding of dyes to macromolecular species, inclusion of chromophores in specific cellular organwelles, fluorescence resonance energy transfer, and dynamic quenching determine the excited-state lifetime of a fluorophore. The FLI technique provides a way to measure these processes directly at 103–106 pixels in an image. In addition, if image domains differ with respect to the mean fluorescence lifetime, FLI can be used to improve the contrast of a fluorescence image. By measuring the fluorescence lifetime one can determine whether fluorescence intensity differences from different locations in an image can be attributed to differences in dye concentration or whether physical spectroscopic effects such as local differences in the rate of dynamic quenching are responsible. All the above applications provide new possibilities for biology and medical diagnostics. However the speed of data acquisition and analysis in current FLI instrumentation is limited in general to several minutes; for real-time applications (in order to follow rapid changes of microscopic samples or make in vivo endoscopic medical diagnosis) the present instruments are too slow. We present here a FLI apparatus that is capable of acquiring, processing, and displaying fluorescence lifetime-resolved images in quasi-real time. We also present rapid algorithms for analyzing the data in real time. © 1997 American Institute of Physics.
    Materialart: Digitale Medien
    Standort Signatur Erwartet Verfügbarkeit
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  • 7
    Digitale Medien
    Digitale Medien
    [S.l.] : American Institute of Physics (AIP)
    Review of Scientific Instruments 67 (1996), S. 3073-3081 
    ISSN: 1089-7623
    Quelle: AIP Digital Archive
    Thema: Physik , Elektrotechnik, Elektronik, Nachrichtentechnik
    Notizen: An atomic beam polarized ion source, used heavily since 1989 for producing polarized H± and D± beams for experiments between 25 keV and 20 MeV, has been modified to accept a Lamb shift, spin-filter polarimeter. In this source, polarized ground-state H or D atoms enter an electron cyclotron resonance ionizer where they are stripped to produce an outgoing positive polarized ion beam. When negative ions are desired, cesium vapor is introduced into a downstream charge-exchange canal. The polarimeter, based on an atomic physics concept first developed to produce nuclear-spin-polarized beams at Los Alamos, is designed to monitor the polarization of 2S1/2 metastable H or D atoms emerging from the cesium canal. Metastable 2S1/2 atoms created by electron pickup in a collision with cesium are "filtered'' by the polarimeter according to magnetic substate, as the magnetic field imposed on the polarimeter cavity is tuned between 53 and 61 mT. Photons produced by subsequent quenching of these filtered atoms to their ground state are monitored downstream by a phototube to reveal the magnetic substate population of the incident positive beam. To install the polarimeter cavity and phototube assembly, the existing polarized ion source was lengthened by 30 cm. Installation is complete, and comparisons with calibrated nuclear polarimeters have shown agreement to better than 0.023. Principles of operation, a description of the hardware, measurements for cross calibration, and impressions gained from its use are all presented. © 1996 American Institute of Physics.
    Materialart: Digitale Medien
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  • 8
    Digitale Medien
    Digitale Medien
    [S.l.] : American Institute of Physics (AIP)
    Review of Scientific Instruments 67 (1996), S. 813-817 
    ISSN: 1089-7623
    Quelle: AIP Digital Archive
    Thema: Physik , Elektrotechnik, Elektronik, Nachrichtentechnik
    Notizen: A mini-gel tube electrophoresis apparatus that is easily constructed and simple to operate has been developed. The system can be accommodated in standard commercially available high pressure tubing, and has been tested at up to 200 MPa. The narrow diameter of the glass tubes allows rapid and efficient dissipation of heat. Adequate buffer capacity is maintained in the low volume anode reservoir by increasing the concentration of the buffer. Analytical separations can be achieved in short times with high resolution. After the electrophoresis has been carried out at elevated pressure, the gel can easily be extruded from the tube and loaded onto a standard slab gel for a second-dimensional run at atmospheric pressure. We illustrate the application of this apparatus with the high pressure gel electrophoresis separation and subsequent identification of the constituent subunits of E. coli RNA polymerase. © 1996 American Institute of Physics.
    Materialart: Digitale Medien
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  • 9
    Digitale Medien
    Digitale Medien
    [S.l.] : American Institute of Physics (AIP)
    Journal of Applied Physics 87 (2000), S. 1096-1102 
    ISSN: 1089-7550
    Quelle: AIP Digital Archive
    Thema: Physik
    Notizen: High resolution images of cross-tie domain wall structures have been obtained by magnetic force microscopy (MFM) for a 37.5 nm Co91Nb6Zr3 film using a NiFe thin film coated tip. Between successive cross ties, the main or spinal wall was found to be consistently subdivided unequally into pairs of oppositely oriented Néel wall sections separated by circular Bloch lines. Main and wing walls intersect at cross Bloch lines. A reversed-contrast MFM image of the same uneven cross-tie wall structure was obtained after reversing the tip magnetization. MFM images reflect only the field from the divergence of the underlying magnetization M and contain no direct information on curl M. Accordingly they are best interpreted by comparison with the magnetization pattern of a similar cross-tie structure obtained by micromagnetic computation. This enables the cross and circular Bloch line singularities to be distinguished in the MFM images of the cross-tie structure. By combining repeated observations made with opposite tip magnetizations, disturbance of the main and wing wall structures by the tip was extracted from the MFM signal which was then compared with the signal computed for a two-dimensional model wall. The main wall was found to be an asymmetric Néel wall with a weak S shaped magnetic structure. The wing walls were found to be Néel walls of acute angle, decreasing with distance from the spine. © 2000 American Institute of Physics.
    Materialart: Digitale Medien
    Standort Signatur Erwartet Verfügbarkeit
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  • 10
    Digitale Medien
    Digitale Medien
    [S.l.] : American Institute of Physics (AIP)
    Journal of Applied Physics 60 (1986), S. 3567-3575 
    ISSN: 1089-7550
    Quelle: AIP Digital Archive
    Thema: Physik
    Notizen: High-dose silicon implants have been used to preamorphize the surface of single-crystal silicon prior to the implantation of low-energy BF2. The preamorphization results in shallow junction formation with minimal channeling of the boron, but high concentrations of electrically active defects are formed, leading to excessive reverse bias leakage currents. Measurements of leakage current and deep-level defects indicated that two distinct types of electrically active defects were important: those associated with what are probably complexes or clusters of point defects located near the far end of the range of the implanted silicon, and those associated with extended defects (loops) at the edge of the regrown amorphous region. The former defects were deep-level donors present in high concentrations (〉1017 cm−3) after regrowth of the amorphous layer at 600 or 700 °C and resulted in leakage currents 〉10−4 A/cm2. These centers could be annealed out at 800 °C reducing the leakage current to values between 5×10−8 and 2×10−5 A/cm2 depending upon the relative locations of the extended defects and the metallurgical junction. Measurements and modeling have shown that the location of the band of extended defects is critical in controlling the leakage current and that it will need to be a few hundred angstroms shallower than the junction itself for the associated generation current to be fully suppressed.
    Materialart: Digitale Medien
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