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  • 1
    Digitale Medien
    Digitale Medien
    Springer
    Journal of molecular histology 25 (1993), S. 830-833 
    ISSN: 1573-6865
    Quelle: Springer Online Journal Archives 1860-2000
    Thema: Biologie , Medizin
    Notizen: Summary An immunofluorescent staining method for detecting platelet-activating factor (PAF) is described. This method employs a polyclonal anti-PAF rabbit antibody. When rat brain, heart, lung, liver or kidney tissue was stained using this method, the heart, lung and kidney exhibited PAF-specific staining. Analysis of the amount of PAF in different organs, either by immunofluorescence or by bioassay, showed that kidney tissue contains the greatest amount of PAF.
    Materialart: Digitale Medien
    Standort Signatur Erwartet Verfügbarkeit
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  • 2
    Digitale Medien
    Digitale Medien
    Springer
    Journal of molecular histology 25 (1993), S. 830-833 
    ISSN: 1573-6865
    Quelle: Springer Online Journal Archives 1860-2000
    Thema: Biologie , Medizin
    Notizen: Summary An immunofluorescent staining method for detecting platelet-activating factor (PAF) is described. This method employs a polyclonal anti-PAF rabbit antibody. When rat brain, heart, lung, liver or kidney tissue was stained using this method, the heart, lung and kidney exhibited PAF-specific staining. Analysis of the amount of PAF in different organs, either by immunofluorescence or by bioassay, showed that kidney tissue contains the greatest amount of PAF.
    Materialart: Digitale Medien
    Standort Signatur Erwartet Verfügbarkeit
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  • 3
    Digitale Medien
    Digitale Medien
    New York, NY [u.a.] : Wiley-Blackwell
    Journal of Applied Polymer Science 25 (1980), S. 1861-1866 
    ISSN: 0021-8995
    Schlagwort(e): Chemistry ; Polymer and Materials Science
    Quelle: Wiley InterScience Backfile Collection 1832-2000
    Thema: Chemie und Pharmazie , Maschinenbau , Physik
    Notizen: The tensile strength and ultimate strain of polypropylene fibers were measured by the creep fracture method at various temperatures. The tensile strength against time-to-break curves at various temperatures, which were plotted on log-log scales, were superposed by shifting the curves along the logarithmic time-to-break axis, and the composite curve of the tensile strength as a function of a reduced time to break was obtained. On the other hand, to construct the composite curve of ultimate strain from the ultimate strain against time-to-break curves at various temperatures, shifting the curves along the logarithmic ultimate strain axis was required in combination with shifting along the logarithmic time-to-break axis. The temperature dependence of the shift factor aT followed an equation of the Williams-Landel-Ferry (WLF) form. The volume fraction of free volume at the glass transition temperature and the coefficient of thermal volume expansion, which were calculated from the WLF coefficients determined for the polypropylene fibers, are almost the same as those known as “universal values” for amorphous polymers.
    Zusätzliches Material: 6 Ill.
    Materialart: Digitale Medien
    Standort Signatur Erwartet Verfügbarkeit
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  • 4
    Digitale Medien
    Digitale Medien
    New York, NY [u.a.] : Wiley-Blackwell
    Journal of Applied Polymer Science 37 (1989), S. 2683-2697 
    ISSN: 0021-8995
    Schlagwort(e): Chemistry ; Polymer and Materials Science
    Quelle: Wiley InterScience Backfile Collection 1832-2000
    Thema: Chemie und Pharmazie , Maschinenbau , Physik
    Notizen: Two kinds of polypropylene with different molecular weight (MI = 15 and 30) were melt-spun at the spinning temperatures of 210-290°C and take-up velocities of 0.15-3 km/min. In the cases of the spinning temperatures of 270 and 290°C for MI15 and 250 and 290°C for MI30, the density showed a minimum with increasing take-up velocity at around 0.5-1 km/min. This result suggests that crystallization behavior is influenced by two competitive effects, i.e., cooling rate and crystallization rate both of which are enhanced by the increase in take-up velocity. Crystal structures of slightly oriented monoclinic, slightly oriented pseudohexagonal, highly oriented pseudohexagonal, and highly oriented monoclinic were successively observed with increasing take-up velocity. The change of crystallization temperature may result in the different kinds of crystal modifications. Numerical calculations on nonisothermal orientation-induced crystallization in the melt spinning process and experimental results showed qualitative agreement in the change of crystallinity with take-up velocity, spinning temperature, and molecular weight.
    Zusätzliches Material: 7 Ill.
    Materialart: Digitale Medien
    Standort Signatur Erwartet Verfügbarkeit
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  • 5
    Digitale Medien
    Digitale Medien
    New York, NY [u.a.] : Wiley-Blackwell
    Journal of Applied Polymer Science 59 (1996), S. 51-56 
    ISSN: 0021-8995
    Schlagwort(e): Chemistry ; Polymer and Materials Science
    Quelle: Wiley InterScience Backfile Collection 1832-2000
    Thema: Chemie und Pharmazie , Maschinenbau , Physik
    Notizen: The degrees of swelling of noncrystalline regions of domestic and tussah silk fibers were investigated by measuring the small-angle X-ray scattering intensity of the fibers in wet conditions and analyzing the scattering intensity based on a two-phase model, i.e., crystalline regions and water-swollen noncrystalline regions. The influence of the degree of swelling of noncrystalline regions on the graft treatment of these fibers with methacrylamide was investigated. The changes in the structure caused by the graft treatment were also analyzed using the wide-angle X-ray diffraction measurements. As compared with the tussah silk fibers, the domestic silk fibers showed a larger degree of swelling of the noncrystalline regions, and gained a larger amount of resin by the graft treatment. The crystallites with smaller sizes in the tussah silk fibers were destroyed preferentially by the graft treatment. For the domestic silk fibers, the crystallites were destroyed more seriously and rather homogeneously independent of the crystallite sizes. © 1996 John Wiley & Sons, Inc.
    Zusätzliches Material: 5 Ill.
    Materialart: Digitale Medien
    Standort Signatur Erwartet Verfügbarkeit
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  • 6
    ISSN: 0021-8995
    Schlagwort(e): Chemistry ; Polymer and Materials Science
    Quelle: Wiley InterScience Backfile Collection 1832-2000
    Thema: Chemie und Pharmazie , Maschinenbau , Physik
    Notizen: High-speed bicomponent spinning of poly(ethylene terephthalate)(PET)(core) and poly-propylene (PP) (sheath) was carried out and the structure development in the individual components, PET and PP, was investigated. The orientation and crystallinity development in the PET component was enhanced as compared to that of the single-component spinning while the PP component remained in a low orientation state and had a pseudohexagonal crystal structure even at high take-up speeds. To clarify the mutual interaction between the two components in bicomponent spinning, a semiquantitative numerical simulation was performed. The simulation results obtained using the Newtonian fluid model showed that the solidification stress in the PET component was enhanced while that of the PP component was decreased in comparison with the corresponding single-component spinning. This is due to the difference in the temperature dependence of their elongational viscosity. Simulation with an upper-convected Maxwell model as the constitutive equation suggested that significant stress relaxation of the PP component can occur in the spinline if the PET component solidifies earlier than does PP. Based on the structural characterization results, and the simulation results, it was concluded that the difference in the activation energy of the elongational viscosity and solidification temperature between the two polymers are the main factors influencing the mutual interaction in the bicomponent spinning process. © 1996 John Wiley & Sons, Inc.
    Zusätzliches Material: 15 Ill.
    Materialart: Digitale Medien
    Standort Signatur Erwartet Verfügbarkeit
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  • 7
    Digitale Medien
    Digitale Medien
    New York, NY [u.a.] : Wiley-Blackwell
    Journal of Applied Polymer Science 61 (1996), S. 1359-1364 
    ISSN: 0021-8995
    Schlagwort(e): Chemistry ; Polymer and Materials Science
    Quelle: Wiley InterScience Backfile Collection 1832-2000
    Thema: Chemie und Pharmazie , Maschinenbau , Physik
    Notizen: Silk fibers were treated with methacrylamide (MAA), and changes in the mechanical properties of the silk fibers were investigated. The breaking load of the silk fibers was almost unchanged, whereas rigidity was markedly increased by the methylmethacrylate (MAA) treatment. Elongation at break of the silk fibers decreased significantly when the fibers were treated with MAA up to polymer add-on (ca. 300%). The cross-sectional area of the MAA-treated silk fiber was given by the addition of the cross-sectional area of the original silk fiber and that of the MAA polymer. The Young's modulus of MAA-treated silk fibers increased linearly with increasing volume fractions of fiber in MAA-grafted silk fibers. The Young's modulus of the MAA polymer in the MAA-treated silk fibers was estimated by extrapolating the relation between Young's moduli and volume fractions of fiber to the zero volume fraction of fiber. The Young's modulus of the MAA polymer in the MAA-treated silk fibers was larger than the sonic modulus measured for an MAA polymer plate. © 1996 John Wiley & Sons, Inc.
    Zusätzliches Material: 9 Ill.
    Materialart: Digitale Medien
    Standort Signatur Erwartet Verfügbarkeit
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  • 8
    Digitale Medien
    Digitale Medien
    New York, NY [u.a.] : Wiley-Blackwell
    Journal of Applied Polymer Science 26 (1981), S. 3565-3573 
    ISSN: 0021-8995
    Schlagwort(e): Chemistry ; Polymer and Materials Science
    Quelle: Wiley InterScience Backfile Collection 1832-2000
    Thema: Chemie und Pharmazie , Maschinenbau , Physik
    Notizen: The ultimate properties of polypropylene fibers, prepared by drawing the same undrawn fibers to different draw ratios, were determined by the creep fracture method at temperatures from 40 to 120°C. The composite curves of the engineering stress at break, the true stress at break, the ultimate extension ratio were constructed as a function of reduced time to break by assuming time-temperature superposition. The temperature dependence of the shift factor aT used in the superposition could be represented by a single equation of the Williams, Landel, and Ferry form. The composite curves of the true stress at break for the samples with different draw ratios were almost the same independently of draw ratio. The composite curves of the ultimate extension ratio for these samples could be reduced to a single curve by assuming that the ultimate extension ratio evaluated with respect to the unit length of the undrawn fibers were constant independently of draw ratio if the time to break and temperature conditions of the measurement were fixed constant. A possible fracture mechanism is discussed on the basis of the fracture mechanisms proposed by Samuels and Peterlin.
    Zusätzliches Material: 7 Ill.
    Materialart: Digitale Medien
    Standort Signatur Erwartet Verfügbarkeit
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  • 9
    Digitale Medien
    Digitale Medien
    New York, NY [u.a.] : Wiley-Blackwell
    Journal of Applied Polymer Science 29 (1984), S. 1319-1326 
    ISSN: 0021-8995
    Schlagwort(e): Chemistry ; Polymer and Materials Science
    Quelle: Wiley InterScience Backfile Collection 1832-2000
    Thema: Chemie und Pharmazie , Maschinenbau , Physik
    Notizen: The length changes of acrylic fibers during isothermal treatment at temperatures from 208°C to 270°C were measured under constant tensile stresses. In order to elucidate the relation between the length and structural changes during heat treatment, the measurements of density, the elemental composition, and the aromatization index determined from X-ray diffraction were made for the fibers heat-treated at 252°C for various periods of time. It is shown that a contraction in length which accompanied a volume contraction occurred during extended heat treatment, even when the fibers were subjected to high tensile stresses. The volume contraction is attributed to the fact that planar cyclized polymer segments, formed by additional polymerization of the nitrile side groups, are built up and construct a stacking which is denser than the original fiber structure. The orientation of the stacking of the cyclized segments was measured for the fibers heat-treated in the fixed state giving a high orientation, which is comparable to that of the fibers heat-treated under a high tensile stress giving an extension to the fibers in the initial periods of heat treatment. These results were explained by considering the interaction of external constraint and volume contraction which occurs during heat treatment.
    Zusätzliches Material: 7 Ill.
    Materialart: Digitale Medien
    Standort Signatur Erwartet Verfügbarkeit
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  • 10
    Digitale Medien
    Digitale Medien
    New York : Wiley-Blackwell
    Journal of Polymer Science: Polymer Physics Edition 21 (1983), S. 275-284 
    ISSN: 0098-1273
    Schlagwort(e): Physics ; Polymer and Materials Science
    Quelle: Wiley InterScience Backfile Collection 1832-2000
    Thema: Chemie und Pharmazie , Physik
    Notizen: X-ray diffraction studies of fibers of the polyester/ether poly(ethylene-1,2-diphenoxyethane-p,p′ -dicarboxylate) (PEET) produced by high-speed melt spinning show the existence of two polymorphic forms, designated α and β, in the solid state. The α form is obtained by annealing filaments melt spun at takeup speeds below 3000 m/min and is also found in samples crystallized from the melt and from dilute solutions. The α form has a monoclinic unit cell with dimensions a = 7.83, b = 10.33, c = 18.68 Å, and β = 83.1°. The equilibrium melting temperature and heat of fusion of the α form are 288.3°C and 19.1 cal/g, respectively. The β form predominates in highly oriented filaments obtained at takeup velocities above 6000 m/min. The unit cell is orthorhombic with dimensions a = 7.28, b = 5.65, and c = 18.64 Å. The β form does not transform to the α form on annealing.
    Zusätzliches Material: 6 Ill.
    Materialart: Digitale Medien
    Standort Signatur Erwartet Verfügbarkeit
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