ISSN:
1572-8854
Source:
Springer Online Journal Archives 1860-2000
Topics:
Geosciences
,
Physics
Notes:
Abstract Crystals of the synthesized title compound (C22H15I3N2) are monoclinic. Space group P21/a,a=15.072(2),b=10.936(1),c=15.363(2) Å,β=108.49(1)°. The structure was solved by direct methods and refined by block-matrix least-squares procedure to giveR=0.059 and Rw=0.043 for 3658 reflections above 2σ(I). The central hexaatomic ring is in a very flattened envelope conformation being the methylene group very little deviated from the plane defined by the other five atoms. The phenyl group is rotated 63.40° from that plane.
Type of Medium:
Electronic Resource
URL:
http://dx.doi.org/10.1007/BF01161061
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