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  • 1
    Electronic Resource
    Electronic Resource
    Crystallization behavior of high-density polyethylene/linear low-density polyethylene blend (1992)
    New York, NY [u.a.] : Wiley-Blackwell
    Journal of Applied Polymer Science 44 (1992), S. 719-726 
    Details
    ISSN: 0021-8995
    Keywords: Chemistry ; Polymer and Materials Science
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology , Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics , Physics
    Notes: Binary blend of high-density polyethylene (HDPE) and linear low-density polyethylene (LLDPE), prepared by melt mixing in an extruder, in the entire range of blending ratio, is studied for crystallization behavior by differential scanning calorimetry (DSC) and X-ray diffraction measurements. Cocrystallization was evident in the entire range of blend composition, from the single-peak character in both DSC crystallization exotherms and meltingendotherms and the X-ray diffraction peaks. A detailed analysis of DSC crystallization exotherms revealed a systematic effect of the addition of LLDPE on nucleation rate and the subsequently developed crystalline morphology, which could be distinguished in the three regions of blending ratio, viz, the “HDPE-rich blend,” “LLDPE-rich blend,” and the “middle range from 30-70% LLDPE content.” Variations in crystallinity, crystallite size, and d spacing are discussed in terms of differences in molecular structure of the components.
    Additional Material: 6 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/app.1992.070440418
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  • 2
    Electronic Resource
    Electronic Resource
    Mechanical properties and morphology of high-density polyethylene/linear low-density polyethylene blend (1992)
    New York, NY [u.a.] : Wiley-Blackwell
    Journal of Applied Polymer Science 46 (1992), S. 99-108 
    Details
    ISSN: 0021-8995
    Keywords: Chemistry ; Polymer and Materials Science
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology , Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics , Physics
    Notes: The binary blend of high-density polyethylene (HDPE) and linear low-density polyethylene (LLDPE) in the range of composition from 100% HDPE to 100% LLDPE has been investigated for tensile and flexural properties and the morphology in the deformed state on tensile fracture. Tensile properties (initial modulus, yield stress, and elongation-at-yield, ultimate tensile strength and elongation-at-break, and work of yield and work of rupture) and flexural properties (flexural modulus and flexural yield stress) are studied as a function of blend composition. Behavior, in terms of these properties, is distinguishable in three zones of blend composition, viz. (i) HDPE-rich blend, (ii) LLDPE-rich blend, and (iii) the middle zone. In zones (i) and (ii), the variations of these properties are more or less linear, whereas in the middle region [i.e., zone (iii)], there is a reversal of trends in variation or sometimes a behavior opposite to the expected one. The results are explained on the basis of the effects of cocrystallization and the presence of octene-containing segments in the amorphous phase. Scanning electron micrographs of the tensile fracture surfaces are presented to illustrate the occurrence of transverse bands interconnecting the fibrils.
    Additional Material: 7 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/app.1992.070460110
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  • 3
    Electronic Resource
    Electronic Resource
    Flexural and impact properties of high-density polyethylene/linear low-density polythylene blend (1993)
    New York, NY [u.a.] : Wiley-Blackwell
    Journal of Applied Polymer Science 49 (1993), S. 477-485 
    Details
    ISSN: 0021-8995
    Keywords: Chemistry ; Polymer and Materials Science
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology , Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics , Physics
    Notes: In this article, a study of flexural and impact properties of binary blends of high-density polyethylene (HDPE) and linear low-density polyethylene (LLDPE), over a full range of blending ratios, is presented. The property distinctions in the three ranges of composition (viz., HDPE-rich blend, LLDPE-rich blend, and the middle region) are remarkable and consistent with the different effects of cocrystallization in the respective concentration ranges. Furthermore, the analysis of flexural yield properties data, in terms of the Ree-Eyring equation, and the correlation of results with variation of x-ray crystallinity are presented, which suggests the existence of two types (i.e., mobile and immobile) of segments in the amorphous phase of the blend. The relative variation of these two types of amorphous phase in the three different composition ranges of the blend are discussed. The impact strength variation of this blend is also found to correlate with the variation of the fraction of amorphous phase in the blend. © 1993 John Wiley & Sons, Inc.
    Additional Material: 7 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/app.1993.070490312
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  • 4
    Electronic Resource
    Electronic Resource
    Effect of cocrystallization on kinetic parameters of high-density polyethylene/linear low-density polyethylene blend (1996)
    New York, NY [u.a.] : Wiley-Blackwell
    Journal of Applied Polymer Science 61 (1996), S. 951-957 
    Details
    ISSN: 0021-8995
    Keywords: Chemistry ; Polymer and Materials Science
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology , Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics , Physics
    Notes: The isothermal crystallization kinetics of a binary melt blend of high-density polyethylene (HDPE)/linear low-density polyethylene (LLDPE) is presented. An effort was made to understand the phenomenon of cocrystallization between these two constituting components of the blend with the help of kinetic parameters. The analysis based on the Avrami exponent entails that both HDPE and LLDPE undergo individual seeding of nuclei and they merge with each other in the growth process to form cocrystallites. The incorporation of the LLDPE segment in the HDPE crystallites progressively dilutes the properties of HDPE in the blend. The half-time of crystallization (t1/2) shows variation in three distinct stages: The t1/2 increases slowly in the region of 0-30% LLDPE content (HDPE-rich blend), remains constant in the 30-70% LLDPE-containing region (middle region of blend composition), and increases sharply thereafter. These variations of t1/2 quite appreciably explain the change in % crystallinity, the Avrami exponent, and crystallite-size distribution. These observations were further supported by the small-angle light-scattering experiment. © 1996 John Wiley & Sons, Inc.
    Additional Material: 5 Ill.
    Type of Medium: Electronic Resource
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  • 5
    Electronic Resource
    Electronic Resource
    Crystallization kinetics of high-density polyethylene/linear low-density polyethylene blend (1994)
    New York, NY [u.a.] : Wiley-Blackwell
    Journal of Applied Polymer Science 51 (1994), S. 231-239 
    Details
    ISSN: 0021-8995
    Keywords: Chemistry ; Polymer and Materials Science
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology , Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics , Physics
    Notes: This article presents crystallization kinetics studies on a cocrystallizing polymer highdensity polyethylene (HDPE)/linear lowd-ensity polyethylene (LLDPE) blend. The nonisothermal crystallization exotherms obtained by differential scanning calorimetry (DSC) were analyzed to investigate the effect of cocrystallization on kinetics parameters, namely the Avrami exponent and activation energy. The regular change of Avrami exponent with blend composition from a value of about 3 corresponding to HDPE to a value of 2 corresponding to LLDPE is observed. A sheaf-like crystalline growth with variation of nucleation depending on blend composition is concluded from these results of DSC exotherm analysis in conjunction with the small-angle light scattering observations. The observed variation of activation energy of crystallization with blend composition suggests the role of interaction of side chains and comonomer units present in the LLDPE. © 1994 John Wiley & Sons, Inc.
    Additional Material: 6 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/app.1994.070510204
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  • 6
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    COBALT STATUS IN QUEBEC SOILS (1967)
    Canadian Science Publishing
    Details
    Publication Date: 1967-06-01
    Description: Studies on thirty mineral soil series and five organic soils from the broad cultivated areas of Quebec indicated that total cobalt, extracted with 70% perchloric acid digestion, ranged from 1.1 to 21.6 ppm and 2.5% acetic acid-extractable cobalt from 0.3 to 0.83 ppm. Extractable cobalt in the surface soils was significantly correlated with total cobalt, which in turn was highly dependent on the clay content of the soil. The soil pH or the organic matter content did not seem to have any influence on the cobalt content in the cultivated soils. Light-textured and podzolized soils are likely to be low m cobalt, while soils with richer clay content are higher. Organic soils, in general, were found to be lower in cobalt content than mineral soils. Nineteen out of the thirty mineral soils studied and all the organic soils contained less than 0.25 ppm of extractable cobalt and may be considered as critical or deficient because forage grown on such soils is likely to cause cobalt deficiency in livestock.
    Print ISSN: 0008-4271
    Electronic ISSN: 1918-1841
    Topics: Geosciences , Agriculture, Forestry, Horticulture, Fishery, Domestic Science, Nutrition
    Published by Canadian Science Publishing
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