ALBERT

All Library Books, journals and Electronic Records Telegrafenberg

X
feed icon rss

Your email was sent successfully. Check your inbox.

An error occurred while sending the email. Please try again.

Proceed reservation?

Export
  • 1
    Electronic Resource
    Electronic Resource
    Determination of bromine and iodine in biological and environmental materials using epithermal neutron activation analysis (1997)
    Springer
    Fresenius' journal of analytical chemistry 357 (1997), S. 1106-1110 
    Details
    ISSN: 1432-1130
    Source: Springer Online Journal Archives 1860-2000
    Topics: Chemistry and Pharmacology
    Notes: Abstract Epithermal neutron activation analysis (ENAA) was applied to the determination of the contents of bromine and iodine in 40 biological and environmental standard reference materials and Chinese diets. Boron nitride (BN) for solid samples and BN+Cd for liquid samples were adopted as shield material. Irradiation was carried out in inner and outer irradiation sites in a Miniature Source Reactor (MNSR) for solid and liquid samples, respectively. The 443 keV photopeak of 128I and the 616 keV photopeak of 80Br were used. The precision of measurement (relative standard deviation) is 2∼6% for contents of iodine of more than 100 ng/g and 8∼12% in the 20∼100 ng/g range in solid samples, and 12∼18% at less than 100 ng/ml in liquid samples. For bromine, the precision of measurement is 2–8% for solid samples and lower than 13% for liquid samples. The detection limits under experimental conditions varied between 10∼30 ng/g, 55∼95 ng/g and 25∼68 ng/g for iodine and 50∼150 ng/g, 200∼450 ng/g and 100∼300 ng/g for bromine in ENAA with BN shield in inner irradiation sites, with Cd shield and BN+Cd shield in outer irradiation sites, respectively.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1007/s002160050314
    Location Call Number Expected Availability
    BibTip Others were also interested in ...
    Paper (German National Licenses)
    Fulltext
  • 2
    Electronic Resource
    Electronic Resource
    Development of a Monoclonal Antibody-based ELISA for Detection of Sulfamethazine and N4−acetyl Sulfamethazine in Chicken Breast Muscle Tissue (2005)
    Oxford, UK : Blackwell Publishing Ltd
    Journal of food science 70 (2005), S. 0 
    Details
    ISSN: 1750-3841
    Source: Blackwell Publishing Journal Backfiles 1879-2005
    Topics: Agriculture, Forestry, Horticulture, Fishery, Domestic Science, Nutrition , Process Engineering, Biotechnology, Nutrition Technology
    Notes: : An anti-sulfamethazine monoclonal antibody was developed in a BALB/c mouse immunized with sulfamethazine (SM2) -human serum albumin (HSA). Using this monoclonal antibody, an indirect competitive enzyme-linked immunosorbent assay (cELISA) was developed to detect SM2 and its metabolites in chicken breast muscle tissue. The 50% inhibition value (IC50) was 9.3 ng/mL. When SM2 was spiked at levels of 20 to 200 ng/g, recoveries ranged from 81.3% to 104.2% with coefficients of variation (CVs) of 4.3% to 19.3%. The metabolite N4−acetyl SM2 was also evaluated by the same assay. When it was fortified atlevels of 20 to 200 ng/g, recoveries ranged from 80.4% to 100.8% with CVs of 3.0% to 14.2%. The results were confirmed with analysis by high-performance liquid chromatography (HPLC). In an actual residue study, the results obtained by cELISA did not correlate well with those obtained by HPLC (P 〈 0.05). This might be due to the coextraction of cross-reactive SM2-related residues that were not quantified by the HPLC method. The study indicated that the presence of residues should be anticipated when considering the maximum residue limit of SM2 residue.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1111/j.1365-2621.2005.tb09012.x
    Location Call Number Expected Availability
    BibTip Others were also interested in ...
    Paper (German National Licenses)
    Fulltext
  • 3
    Electronic Resource
    Electronic Resource
    Determination of 24 elements in four algae reference materials by neutron activation analysis and inductively coupled plasma mass spectrometry (1998)
    Springer
    Fresenius' journal of analytical chemistry 360 (1998), S. 423-426 
    Details
    ISSN: 1432-1130
    Source: Springer Online Journal Archives 1860-2000
    Topics: Chemistry and Pharmacology
    Notes: Abstract Four algae reference materials, IAEA-391, 392, 393 and IAEA-140, prepared by the International Atomic Energy Agency for intercomparison under different preparation conditions were analyzed for 24 elements. Conventional neutron activation analysis (NAA) was used to determine Al, Ca, Cl, Co, Cr, Cu, Fe, K, Mg, Mn, Mo, Na, Sb, V and Zn and epithermal NAA using BN and Cd as shielding material for I, Br, As, Ni, Mo and Cd. Inductively coupled plasma mass spectrometry (ICP-MS) as a complementary and comparative method was applied to determine Pb, Sn, Ni, Sr, Rb, As, Co, Cr, Cu, Mn, V, Mo and Zn. Two analytical quality control standard reference materials IAEA-V-10 (hay powder) and IAEA-331 (spinach) were analyzed simultaneously with real samples. The results agree quite well with each other and with the certified values.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1007/s002160050727
    Location Call Number Expected Availability
    BibTip Others were also interested in ...
    Paper (German National Licenses)
    Fulltext
  • 4
    Electronic Resource
    Electronic Resource
    Subcellular distribution of Al, Cu, Mg, Mn and other elements in the human liver (1999)
    Springer
    Fresenius' journal of analytical chemistry 363 (1999), S. 512-516 
    Details
    ISSN: 1432-1130
    Source: Springer Online Journal Archives 1860-2000
    Topics: Chemistry and Pharmacology
    Notes: Abstract The elemental concentrations and chemical species of Al, Br, Cl, Cu, K, Mg, Mn, Na and I in human liver and its subcellular fractions were studied by several biochemical techniques combined with neutron activation analysis. The highest concentrations of Al, Mg, and I were found in the nuclei, whereas those of Br, Cu, Cl, K, Mn and Na in the cytosol. About 20% of Br, half of Al and most of Cu (78.8%), Mg (65.9%) and Mn (80.6%) remained in the cellulose bags after dialysis of liver homogenate, which were suggested to be bound to macromolecules. K (100%) and more than 95% of Cl and Na were found to be in the dialyzates. Similar results were found in the fractions of nuclei, mitochondria, lysosome and microsome, respectively, after the same treatment. Further study was carried out to elucidate the elemental distribution in the cytosol by ethanol precipitation and by ammonium sulfate fractionation. The results suggested that several kinds of Cu-, Mn- and Mg-bound proteins existed in the cytosol of human liver cells.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1007/s002160051235
    Location Call Number Expected Availability
    BibTip Others were also interested in ...
    Paper (German National Licenses)
    Fulltext
  • 5
    Electronic Resource
    Electronic Resource
    Molecular activation analysis for chemical species studies (1999)
    Springer
    Fresenius' journal of analytical chemistry 363 (1999), S. 477-480 
    Details
    ISSN: 1432-1130
    Source: Springer Online Journal Archives 1860-2000
    Topics: Chemistry and Pharmacology
    Notes: Abstract Molecular activation analysis (MAA) refers to an activation analysis method that is able to provide information on the chemical species of elements in systems of interest, though its exact definition has yet to be assigned. Its development is strongly stimulated by the urgent need to know the chemical species of elements, because knowledge of bulk contents or concentrations is often insufficient to judge biological, environmental or geochemical effects of elements. The features, methodology and limitations of MAA are outlined, as well as the up-to-date MAA progress in our laboratory.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1007/s002160051227
    Location Call Number Expected Availability
    BibTip Others were also interested in ...
    Paper (German National Licenses)
    Fulltext
  • 6
    Electronic Resource
    Electronic Resource
    A study of relationship of element contents in human hair with some respiratory system diseases (1994)
    Springer
    Journal of radioanalytical and nuclear chemistry 185 (1994), S. 109-118 
    Details
    ISSN: 1588-2780
    Source: Springer Online Journal Archives 1860-2000
    Topics: Chemistry and Pharmacology , Energy, Environment Protection, Nuclear Power Engineering
    Notes: Abstract 19 elements, such as Ca, Mg, Fe, Se, Cu, Zn, etc., in hair of 65 patients with chronic bronchitis, pulmonary emphysema and cor-pulmonale diseases and 65 healthy people have been investigated by instrumental neutron activation analysis. The results show that the contents of Ca and Mg are lower and Fe, As and Co are higher in the hair of patients than in healthy persons. The contents of Ca and Mg are lower and Fe is higher in the hair of patients during attack periods of chronic bronchitis than in relaxed periods. The differences are significant (P〈0.05–0.01). The content of Ca is closely related to that of Mg in hair (P〈0.01). The contents of inorganic elements in the Chinese medicine cough and asthma capsule used to treat chronic bronchitis have been determined. The results show that the contents of elements Ca, Mg, Sr, etc., are higher in this medicine than the average amounts of these elements in 120 other Chinese medicines.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1007/BF02042957
    Location Call Number Expected Availability
    BibTip Others were also interested in ...
    Paper (German National Licenses)
    Fulltext
  • 7
    Electronic Resource
    Electronic Resource
    Chemical Species of Iodine in Some Seaweeds II. Iodine-Bound Biological Macromolecules (2000)
    Springer
    Journal of radioanalytical and nuclear chemistry 245 (2000), S. 461-467 
    Details
    ISSN: 1588-2780
    Source: Springer Online Journal Archives 1860-2000
    Topics: Chemistry and Pharmacology , Energy, Environment Protection, Nuclear Power Engineering
    Notes: Abstract The distribution of iodine in various biological macromolecules in Sargassum kjellmanianum was studied using neutron activation analysis combined with chemical and biochemical separation techniques. The results indicate that iodine is mainly bound with protein, part of iodine with pigment and polyphenol, and little with polysaccharides, such as algin, fucoidan and cellulose. This result is significant for the mechanism of enriching iodine of algae and utilization of alga iodine.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1023/A:1006728420096
    Location Call Number Expected Availability
    BibTip Others were also interested in ...
    Paper (German National Licenses)
    Fulltext
  • 8
    Electronic Resource
    Electronic Resource
    Epithermal neutron activation analysis and its application in the Miniature Neutron Source Reactor (1996)
    Springer
    Journal of radioanalytical and nuclear chemistry 210 (1996), S. 137-148 
    Details
    ISSN: 1588-2780
    Source: Springer Online Journal Archives 1860-2000
    Topics: Chemistry and Pharmacology , Energy, Environment Protection, Nuclear Power Engineering
    Notes: Abstract The cadmium and boron ratios from 44 elements, totally 66 nuclides, were determined in the inner and outer irradiation sites of the Miniature Neutron Source Reactor (MNSR). China Institute of Atomic Energy. A permanent Cd-shielded epithermal neutron irradiation site has been designed and installed in the outer of the beryllium reflector of this reactor. Elements e.g., I, Br, Sr, Si, Th and U in biological samples, such as foodstuff, water and blood, geological and environmental samples, such as soil, rock, sediment and vegetable leaves were analyzed by BN-shielded epithermal neutron activation analysis (ENAA), and Au, As, Sb, Th and U by Cd-shielded ENAA. The results show that the detection limits of these elements by ENAA are better by a factor of 1.5–7 than those with conventional NAA.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1007/BF02055413
    Location Call Number Expected Availability
    BibTip Others were also interested in ...
    Paper (German National Licenses)
    Fulltext
  • 9
    Electronic Resource
    Electronic Resource
    A study of six elements daily dietary intake of Chinese people (1997)
    Springer
    Journal of radioanalytical and nuclear chemistry 222 (1997), S. 165-170 
    Details
    ISSN: 1588-2780
    Source: Springer Online Journal Archives 1860-2000
    Topics: Chemistry and Pharmacology , Energy, Environment Protection, Nuclear Power Engineering
    Notes: Abstract Neutron activation analysis (NAA) was used to determine the concentrations of 6 elements Cr, Co, Rb, Cl, Br and I in 12 kinds of Chinese diets. The daily dietary intakes of these elements in 4 areas groups of China were investigated and the analytical results were compared with other countries and WHO recommended dietary intakes.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1007/BF02034264
    Location Call Number Expected Availability
    BibTip Others were also interested in ...
    Paper (German National Licenses)
    Fulltext
  • 10
    Electronic Resource
    Electronic Resource
    Accuracy, precision and sensitivity in cyclic INAA with short-lived radionuclides (1997)
    Springer
    Journal of radioanalytical and nuclear chemistry 223 (1997), S. 67-72 
    Details
    ISSN: 1588-2780
    Source: Springer Online Journal Archives 1860-2000
    Topics: Chemistry and Pharmacology , Energy, Environment Protection, Nuclear Power Engineering
    Notes: Abstract Repeated irradiation enhances the precision and sensitivity of INAA based on short-live radionuclides, but entail systematic losses due to dead time. The relative standard deviation in the net peak area decreases with the square root of the number of cycles while the systematic bias increases with it. The limits of decision, detection and determination decrease in a somewhat more complicated way with the number of cycles. The derived formulation is applied to the determination of selenium in hair by the 161.9 keV photopeak of77mSe,T 1/2=17.8 s.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1007/BF02223365
    Location Call Number Expected Availability
    BibTip Others were also interested in ...
    Paper (German National Licenses)
    Fulltext
Close ⊗
This website uses cookies and the analysis tool Matomo. More information can be found here...