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  • 1
    Electronic Resource
    Electronic Resource
    [S.l.] : American Institute of Physics (AIP)
    Journal of Applied Physics 87 (2000), S. 439-442 
    ISSN: 1089-7550
    Source: AIP Digital Archive
    Topics: Physics
    Notes: Atom probe field ion microscopy was employed to investigate the distribution of Al in a nanocrystalline Fe88Zr7B3Al2 soft magnet with optimal magnetic performance. The atom probe concentration depth profiles show that the Al atoms preferentially partition into the residual amorphous phase, and the partitioning factor of Al is approximately five times larger in the amorphous phase than in the bcc Fe phase. Based on the experimental results, the beneficial effect of the addition of Al on the soft magnetic properties is attributed to the change of the inherent magnetostriction constant of the residual amorphous phase induced by Al partitioning. © 2000 American Institute of Physics.
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  • 2
    Electronic Resource
    Electronic Resource
    [S.l.] : American Institute of Physics (AIP)
    Journal of Applied Physics 88 (2000), S. 6928-6930 
    ISSN: 1089-7550
    Source: AIP Digital Archive
    Topics: Physics
    Notes: Atom probe field ion microscopy was employed to investigate the distribution of the alloying elements in a nanocrystalline Fe76.5Nd8Co8B6Nb1.5 (at. %) alloy consisting of soft magnetic α-Fe and hard magnetic Nd2Fe14B. It was found that Co atoms prefer to partition into Nd2Fe14B phase. The partitioning factor of Co in the hard magnetic phase is approximately 2 with respect to the soft magnetic phase, α-Fe. Atom probe concentration and integrated depth profiles showed that the Nb atoms segregate at the interfaces between the soft and the hard magnetic phases. Based on the atom probe results, the beneficial effects of Nb and Co on the microstructure and the hard magnetic properties of the nanocomposite are discussed. © 2000 American Institute of Physics.
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  • 3
    Electronic Resource
    Electronic Resource
    Woodbury, NY : American Institute of Physics (AIP)
    Applied Physics Letters 79 (2001), S. 42-44 
    ISSN: 1077-3118
    Source: AIP Digital Archive
    Topics: Physics
    Notes: By differential scanning calorimetric measurement, the kinetics of the phase transformation present in Zr65Al7.5Ni10Cu12.5Ag5 bulk metallic glass during continuous heating was investigated. It was found that the effective activation energy from a supercooled liquid to an icosahedral quasicrystalline phase is much lower than that from the supercooled liquid to eutectic crystalline phases. In addition, the activation energy from the icosahedral phase to the crystalline phases is almost the same as that from the supercooled liquid to the crystalline phases. Both of them support that the local atomic structure is similar for the supercooled liquid and the icosahedral phase in the bulk metallic glass. © 2001 American Institute of Physics.
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  • 4
    Electronic Resource
    Electronic Resource
    Woodbury, NY : American Institute of Physics (AIP)
    Applied Physics Letters 76 (2000), S. 967-969 
    ISSN: 1077-3118
    Source: AIP Digital Archive
    Topics: Physics
    Notes: An icosahedral (I) quasicrystalline phase with a grain size below 40 nm was formed as a metastable phase in crystallization of the bulk glassy Zr65Al7.5Cu17.5−xNi10Mx (M=Ag, Pd, Au, or Pt; x=5 and 10 at %) alloys. The volume fraction (Vf) of the I phase is about 85% for the 5% M alloy and nearly 100% for the 10% M alloy. The I phase changes to Zr2Cu+Zr2Ni+Zr2Al3 in a fully annealed state. Compressive fracture strength (σc,f) and fracture elongation (εc,f) of the 10% Pd cylinder with a diameter of 2 mm are respectively 1640 MPa and 2.2% for the glassy phase and increase to 1830 MPa and 3.1% for the I phase. The increase in σc,f is due to the suppression effect of the I particles against the shear deformation of the intergranular glassy phase, and the increase in εc,f results from the localization effect of deformation into the glassy layer. The precipitation of the I phase implies that the glassy alloys include randomly oriented I configurations. The present work shows promise for the new class of high-strength nanoquasicrystalline materials. © 2000 American Institute of Physics.
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  • 5
    Electronic Resource
    Electronic Resource
    Woodbury, NY : American Institute of Physics (AIP)
    Applied Physics Letters 75 (1999), S. 1697-1699 
    ISSN: 1077-3118
    Source: AIP Digital Archive
    Topics: Physics
    Notes: A quasicrystalline phase was discovered in a Zr65Al7.5Ni10Cu12.5Ag5 bulk metallic glass annealed in the supercooled liquid range. Through systematical transmission electron microscopy rotation analyses, the selected area electron diffraction patterns are obtained corresponding to fivefold, threefold, and twofold rotational symmetry, demonstrating that the precipitated phase is an icosahedral quasicrystalline phase with good rotational symmetry. It is concluded that the addition of Ag in the Zr-based metallic glass promotes the formation of the quasicrystalline phase. The present experimental result implies that there is a natural relationship between the Zr-based bulk metallic glasses and icosahedral quasicrystalline. © 1999 American Institute of Physics.
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  • 6
    Electronic Resource
    Electronic Resource
    Woodbury, NY : American Institute of Physics (AIP)
    Applied Physics Letters 74 (1999), S. 812-814 
    ISSN: 1077-3118
    Source: AIP Digital Archive
    Topics: Physics
    Notes: We report atom probe results on impurity oxygen dissolution in a Zr65Cu15Al10Pd10 metallic glass and its redistribution during nanocrystallization. Approximately 0.1 at. % impurity oxygen is detected from the as-melt-spun Zr65Cu15Al10Pd10 metallic glass. Oxygen redistribution occurs during annealing. In some crystallites, oxygen up to 4 at. % is detected, and virtually no oxygen is dissolved in the remaining amorphous phase. This result directly demonstrates that impurity oxygen promotes the crystallization by forming metastable phases containing high content oxygen and thereby influences the kinetics of crystallization. © 1999 American Institute of Physics.
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  • 7
    Electronic Resource
    Electronic Resource
    Woodbury, NY : American Institute of Physics (AIP)
    Applied Physics Letters 74 (1999), S. 2131-2133 
    ISSN: 1077-3118
    Source: AIP Digital Archive
    Topics: Physics
    Notes: Fracture surfaces of a nanocrystallized Zr65Cu15Al10Pd10 metallic glass were observed on an atomic scale with field ion microscopy. Based on geometrical and phase characteristics of the fracture morphologies, it can be determined that a crack propagates along the interfaces between nanocrystals and the amorphous matrix in the alloy with optimized microstructures. Combining with macromechanical properties, it is proposed that the strengthening effect of nanocrystals in the Zr-based metallic glass arises from a strong interaction between nanocrystals and local shear bands during deformation processes of the glassy matrix. © 1999 American Institute of Physics.
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  • 8
    Electronic Resource
    Electronic Resource
    Woodbury, NY : American Institute of Physics (AIP)
    Applied Physics Letters 77 (2000), S. 4298-4300 
    ISSN: 1077-3118
    Source: AIP Digital Archive
    Topics: Physics
    Notes: A method is proposed to measure the plastic deformation of thin metallic films on Si substrates induced by thermal cycling. The cross-sectional profiles of pattern-grown square Al films with a thickness of ∼250 nm and a size of ∼6 μm×6 μm were measured before and after thermal cycling by employing an atomic force microscope. With the assistance of statistical analysis, the change in the size and shape of the thin films were determined. Based on theoretical considerations, the thermal cycling deformation of thin films is attributed to creep and plasticity effects, accommodated by diffusion-controlled interfacial sliding. © 2000 American Institute of Physics.
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  • 9
    Electronic Resource
    Electronic Resource
    Oxford, UK : Blackwell Science Inc
    Journal of the American Ceramic Society 88 (2005), S. 0 
    ISSN: 1551-2916
    Source: Blackwell Publishing Journal Backfiles 1879-2005
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics , Physics
    Notes: Two commercial hot-pressed boron carbide ceramics were investigated by transmission electron microscopy. Atomic-scale observations suggest that the grain boundaries of the two materials are free of grain-boundary films. Two triple-junction phases were found and characterized to be rhombohedral Fe2B103 and orthorhombic Ti3B4. In addition, intra-granular precipitates, AlN, Mo2(C, B) and graphite, were identified and found to have coherent relationships with the boron carbide matrix. Micron-scale inclusions were also observed and most of them were determined to be graphite. The formation mechanisms of the secondary phases and their possible influence on mechanical properties are also discussed.
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  • 10
    ISSN: 0014-5793
    Keywords: 5 S rRNA ; Molecular evolution ; Secondary structure
    Source: Elsevier Journal Backfiles on ScienceDirect 1907 - 2002
    Topics: Biology , Chemistry and Pharmacology , Physics
    Type of Medium: Electronic Resource
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