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Synthesis of 14,20-Bis-epi-1α,25-dihydroxy-19-norvitamin D3 and Analogues (1999)

Van Gool, Michiel ; Zhao, Xu-yang ; Sabbe, Katrien ; [et al.]

Weinheim : Wiley-Blackwell

Liebigs Annalen 1999 (1999), S. 2241-2248

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ISSN: 1434-193X

Keywords: 14,20-Bis-epi Inhoffen-Lythgoe diol ; Hajos-Wiechert ketone, enantiomeric purity ; Acyclic diastereoselective alkylation ; Alkylations ; Hydroborations ; Epimerisation ; Chemistry ; General Chemistry

Source: Wiley InterScience Backfile Collection 1832-2000

Topics: Chemistry and Pharmacology

Notes: 14,20-Bis-epi-1α,25-dihydroxy-19-norvitamin D3 and side chain analogues thereof have been synthesised via the 14,20-bis-epi-Inhoffen-Lythgoe diol 9. The synthesis of this precursor was performed via degradation of vitamin D2 and by total synthesis starting from Hajos-Wiechert ketone 24.

Type of Medium: Electronic Resource

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