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  • 1
    Electronic Resource
    Electronic Resource
    Transmission near-field scanning microscope for infrared chemical imaging (1999)
    [S.l.] : American Institute of Physics (AIP)
    Journal of Applied Physics 86 (1999), S. 2795-2799 
    Details
    ISSN: 1089-7550
    Source: AIP Digital Archive
    Topics: Physics
    Notes: We report transmission infrared near-field scanning microscopy (IR-NSOM) imaging of chemically amplified photoresist polymers patterned by ultraviolet exposure. Chemical specificity was attained using infrared wavelengths tuned to the 3 μm OH stretch absorption band of the polymer, a band sensitive to the chemical changes characteristic of the lithographic photochemical process of this material. Contrast mechanisms are discussed together with the IR-NSOM specifics, such as the fabrication of an infrared near-field probe with high throughput, which lead to an attainable resolution of λ/10 and a transmission sensitivity of 1%. © 1999 American Institute of Physics.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1063/1.371127
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  • 2
    Electronic Resource
    Electronic Resource
    Fourier-transform microwave spectrum, structure, harmonic force field, and hyperfine constants of sulfur chloride fluoride, ClSF (1997)
    College Park, Md. : American Institute of Physics (AIP)
    The Journal of Chemical Physics 106 (1997), S. 10037-10047 
    Details
    ISSN: 1089-7690
    Source: AIP Digital Archive
    Topics: Physics , Chemistry and Pharmacology
    Notes: The rotational spectrum of sulfur choride fluoride, ClSF, has been observed for the first time in the frequency range 8–26 GHz by means of a pulsed molecular jet Fourier-transform microwave spectrometer. The unstable sample molecule has been prepared using a pulsed electrical discharge in jets containing a mixture of SF6 and SCl2 in Ne. Besides the parent species 35Cl32S19F, the isotopomers 37Cl32S19F and 35Cl34S19F could be observed in natural abundance. Rotational constants and quartic centrifugal distortion constants as well as nuclear quadrupole coupling constants due to 35Cl and 37Cl and spin–rotation constants due to 35Cl, 37Cl, and 19F are given. The data were used for the determination of r0, rΔP, rs structural parameters. Additionally, the new data were used for the refinement of the molecular harmonic force field. Results from those harmonic force field calculations were applied in the evaluation of the ground-state average structure, rz, and the estimation of the equilibrium structure, re. The rs structure is r(SF)=160.653(162) pm, r(SCl)=199.437(65) pm, and (angle)(ClSF)=100.732(81)°. The diagonal elements of the 35Cl/37Cl quadrupole coupling tensors have been obtained, and are interpreted in terms of the bonding at 35Cl/37Cl. Negative 19F spin–rotation constants suggest a close analogy of the electronic structures of ClSF and SF2. © 1997 American Institute of Physics.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1063/1.474061
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  • 3
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    High-resolution late Holocene sedimentary cores record the long history of the city of Cádiz (south-western Spain) (2020)
    Copernicus
    Details
    Publication Date: 2020-05-27
    Description: Today, coastal cities worldwide are facing major changes resulting from climate change and anthropogenic forcing, which requires adaptation and mitigation strategies to be established. In this context, sedimentological archives in many Mediterranean cities record a multi-millennial history of environmental dynamics and human adaptation, revealing a long-lasting resilience. Founded by the Phoenicians around 3000 years ago, Cádiz (south-western Spain) is a key example of a coastal resilient city. This urban centre is considered to be one of the first cities of western Europe and has experienced major natural hazards during its long history, such as coastal erosion, storms, and also tsunamis (like the one in 1755 CE following the destructive Lisbon earthquake). In the framework of an international, joint archaeological and geoarchaeological project, three cores have been drilled in a marine palaeochannel that ran through the ancient city of Cádiz. These cores reveal a ≥50 m thick Holocene sedimentary sequence. Importantly, most of the deposits date from the 1st millennium BCE to the 1st millennium CE. This exceptional sedimentary archive will allow our scientific team to achieve its research goals, which are (1) to reconstruct the palaeogeographical evolution of this specific coastal area; (2) to trace the intensity of activities of the city of Cádiz based on archaeological data, as well as geochemical and palaeoecological indicators; and (3) to identify and date high-energy event deposits such as storms and tsunamis.
    Print ISSN: 1816-8957
    Electronic ISSN: 1816-3459
    Topics: Geosciences
    Published by Copernicus on behalf of International Continental Scientific Drilling Program.
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  • 4
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    Revisiting Late Pleistocene glacier dynamics north-west of the Feldberg, southern Black Forest, Germany (2020)
    Copernicus
    Details
    Publication Date: 2020-06-26
    Description: The southern Black Forest was temporarily covered by a ∼1000 km2 large ice cap during the Late Pleistocene. However, during the last glaciation maximum in the Alps the atmospheric circulation over Europe was presumably characterised by the advection of humid air masses from the Mediterranean Sea. As a consequence, the ice cap of the Black Forest was likely in a leeward position due to its location north of the Alps. This raises the question of whether it reached its last maximum extent simultaneously with the glaciers in the Alps. As modern dating techniques have hitherto not been applied to the southern Black Forest, the timing of the last local glaciation maximum remains poorly constrained. As a first step towards an independent regional glacier chronology, we present a critical re-examination of glacial landforms in the area north-west of the highest summit of the Black Forest (Feldberg, 1493 m a.s.l.). It relies on both the analysis of remote sensing data and field mapping. The review of previous studies highlights important disagreements regarding the location of ice-marginal positions and their correlation. In addition, our findings challenge earlier studies on the glaciation of the Black Forest: some previously described ice-marginal positions could not be confirmed, whereas some of the newly identified moraines are described for the first time. This highlights the need for detailed geomorphological investigations prior to the application of geochronological methods. A multi-ridged series of terminal moraines in one of the studied valleys, Sankt Wilhelmer Tal, is proposed as the main target for future dating. Due to discrepancies with earlier studies, future efforts should reinvestigate other key areas related to the last glaciation of the southern Black Forest.
    Print ISSN: 0424-7116
    Electronic ISSN: 2199-9090
    Topics: Geosciences , History
    Published by Copernicus on behalf of Deutsche Quartärvereinigung.
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  • 5
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    Sources and pathways of biocides and their transformation products in urban storm water infrastructure of a 2 ha urban district (2021)
    Copernicus
    Details
    Publication Date: 2021-08-20
    Description: Biocides used in film protection products leaching from facades are known to be a potential threat to the environment. This study identifies individual sources and entry pathways in a small-scale urban area. We investigate emissions of commonly used biocides (terbutryn, diuron, and octylisothiazolinone – OIT) and some of their transformation products (TPs; diuron-desmethyl, terbumeton, terbuthylazine-2-hydroxy, and terbutryn-desethyl) from a 2 ha residential area 13 years after construction has ended. Sampling utilizes existing urban water infrastructure representative for decentralized storm water management in central and northern Europe and applies a two-step approach to (a) determine the occurrence of biocides above water quality limits (i.e., predicted no-effect concentration, PNEC) and (b) identify source areas and characterize entry pathways into surface and groundwater. Monitoring focuses on the analysis of selected biocides and TPs by liquid chromatography–mass spectrometry/mass spectrometry (LC-MS/MS) in water samples taken from facades, rainwater pipes, drainage, and storm water infiltration systems. In standing water in a swale, we found high concentrations of diuron (174 ng L−1) and terbutryn (40 ng L−1) above PNEC for surface water. We confirmed expected sources, i.e., facades. Sampling of rain downpipes from flat roofs identified additional sources of all biocides and two TPs of terbutryn and one TP of diuron. Diuron and terbutryn were found in three drainage pipes representing different entry pathways of biocides. In one drainage pipe collecting road runoff, only diuron-desmethyl and terbutryn-desethyl were detected. In two other drainage pipes collecting infiltrated water through soil, terbuthylazine-2-hydroxy was additionally detected. One of the pipes collecting infiltrated water through soil concentration showed the highest concentrations of terbutryn and two of its TPs (terbutryn-desethyl and terbuthylazine-2-hydroxy). This suggests a high leaching potential of terbutryn. The applied two-step approach determined sources and pathways of biocide and their TPs. This study contributes to expanding knowledge on their entry and distribution and, thus, eventually towards reducing emissions.
    Print ISSN: 1027-5606
    Electronic ISSN: 1607-7938
    Topics: Geography , Geosciences
    Published by Copernicus on behalf of European Geosciences Union.
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  • 6
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    Circumpolar polynya regions and ice production in the Arctic: results from MODIS thermal infrared imagery from 2002/2003 to 2014/2015 with a regional focus on the Laptev Sea (2016)
    Copernicus
    Details
    Publication Date: 2016-12-15
    Description: High-resolution MODIS thermal infrared satellite data are used to infer spatial and temporal characteristics of 17 prominent coastal polynya regions over the entire Arctic basin. Thin-ice thickness (TIT) distributions (≤ 20 cm) are calculated from MODIS ice-surface temperatures, combined with ECMWF ERA-Interim atmospheric reanalysis data in an energy balance model for 13 winter seasons (2002/2003 to 2014/2015; November to March). From all available MODIS swath data, daily thin-ice thickness composites are computed in order to derive quantities such as polynya area and total thermodynamic (i.e., potential) ice production. A gap-filling approach is applied to account for cloud and data gaps in the MODIS composites. All polynya regions combined cover an average thin-ice area of 226.6 ± 36.1 × 103 km2 in winter. This allows for an average total winter-accumulated ice production of about 1811 ± 293 km3, whereby the Kara Sea region, the North Water polynya (both 15 %), polynyas on the western side of Novaya Zemlya (20 %), as well as scattered smaller polynyas in the Canadian Arctic Archipelago (all combined 12 %) are the main contributors. Other well-known sites of polynya formation (Laptev Sea, Chukchi Sea) show smaller contributions and range between 2 and 5 %. We notice distinct differences to earlier studies on pan-Arctic polynya characteristics, originating in some part from the use of high-resolution MODIS data, as the capability to resolve small-scale (〉 2 km) polynyas and also large leads are increased. Despite the short record of 13 winter seasons, positive trends in ice production are detected for several regions of the eastern Arctic (most significantly in the Laptev Sea region with an increase of 6.8 km3 yr−1) and the North Water polynya, while other polynyas in the western Arctic show a more pronounced variability with varying trends. We emphasize the role of the Laptev Sea polynyas as being a major influence on Transpolar Drift characteristics through a distinct relation between increasing ice production and ice area export. Overall, our study presents a spatially highly accurate characterization of circumpolar polynya dynamics and ice production, which should be valuable for future modeling efforts of atmosphere–ice–ocean interactions in the Arctic.
    Print ISSN: 1994-0416
    Electronic ISSN: 1994-0424
    Topics: Geography , Geosciences
    Published by Copernicus on behalf of European Geosciences Union.
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  • 7
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    Thin-ice dynamics and ice production in the Storfjorden polynya for winter seasons 2002/2003–2013/2014 using MODIS thermal infrared imagery (2015)
    Copernicus
    Details
    Publication Date: 2015-05-21
    Description: Spatial and temporal characteristics of the Storfjorden polynya, which forms regularly in the proximity of the islands Spitsbergen, Barentsøya and Edgeøya in the Svalbard archipelago under the influence of strong northeasterly winds, have been investigated for the period of 2002/2003 to 2013/2014 using thermal infrared satellite imagery. Thin-ice thicknesses were calculated from MODIS ice-surface temperatures combined with ECMWF ERA-Interim atmospheric reanalysis data in an energy-balance model. Associated quantities like polynya area and total ice production were derived and compared to previous remote sensing and modeling studies. A basic coverage-correction scheme was applied to account for cloud gaps in the daily composites. On average, both polynya area and ice production are thereby increased by about 30%. The sea ice in the Storfjorden area experiences a late fall freeze-up in several years over the 12-winter period, which becomes most apparent through an increasing frequency of large thin-ice areas until the end of December. In the course of an average winter season, ice thicknesses below 10 cm are dominating within the Storfjorden basin. During the regarded period, the mean polynya area is 4555.7 ± 1542.9 km2. Maximum daily ice production rates can reach as high as 26 cm d−1, while the average ice production is estimated at 28.3 ± 8.5 km3 per winter and therefore lower than in previous studies. Despite this comparatively short record of 12 winter seasons, a significant positive trend of 20.2 km3 per decade could be detected, which originates primarily from a delayed freeze-up in November and December in recent winter seasons. This contrasts earlier reports of a slightly negative trend in accumulated ice production prior to 2002. Although featuring more pronounced interannual variations between 2004/2005 and 2011/2012, our estimates underline the importance of this relatively small coastal polynya system considering its contribution to the cold halocline layer through salt release during ice-formation processes. In addition, calculated quasi-daily thin-ice thickness charts represent a valuable data set for atmosphere and ocean modeling applications.
    Print ISSN: 1994-0416
    Electronic ISSN: 1994-0424
    Topics: Geography , Geosciences
    Published by Copernicus on behalf of European Geosciences Union.
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  • 8
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    Quantification of ice production in Laptev Sea polynyas and its sensitivity to thin-ice parameterizations in a regional climate model (2016)
    Copernicus
    Details
    Publication Date: 2016-12-09
    Description: The quantification of sea-ice production in the Laptev Sea polynyas is important for the Arctic sea-ice budget and the heat loss to the atmosphere. We estimated the ice production for the winter season 2007/2008 (November–April) based on simulations with the regional climate model COSMO-CLM at a horizontal resolution of 5 km and compared it to remote sensing estimates. A reference and five sensitivity simulations were performed with different assumptions on grid-scale and subgrid-scale ice thickness considered within polynyas, using a tile approach for fractional sea ice. In addition, the impact of heat loss on the atmospheric boundary layer was investigated. About 29.1 km3 of total winter ice production was estimated for the reference simulation, which varies by up to +124 % depending on the thin-ice assumptions. For the most realistic assumptions based on remote sensing of ice thickness the ice production increases by +39 %. The use of the tile approach enlarges the area and enhances the magnitude of the heat loss from polynyas up to +110 % if subgrid-scale open water is assumed and by +20 % for realistic assumptions. This enhanced heat loss causes in turn higher ice production rates and stronger impact on the atmospheric boundary layer structure over the polynyas. The study shows that ice production is highly sensitive to the thin-ice parameterizations for fractional sea-ice cover. In summary, realistic ice production estimates could be retrieved from our simulations. Neglecting subgrid-scale energy fluxes might considerably underestimate the ice production in coastal polynyas, such as in the Laptev Sea, with possible consequences on the Arctic sea-ice budget.
    Print ISSN: 1994-0416
    Electronic ISSN: 1994-0424
    Topics: Geography , Geosciences
    Published by Copernicus on behalf of European Geosciences Union.
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  • 9
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    Thin-ice dynamics and ice production in the Storfjorden polynya for winter-seasons 2002/2003–2013/2014 using MODIS thermal infrared imagery (2014)
    Copernicus
    Details
    Publication Date: 2014-11-13
    Description: Spatial and temporal characteristics of the Storfjorden polynya, which forms regularly in the proximity of the islands Spitsbergen, Barentsøya and Edgeøya in the Svalbard archipelago under the influence of strong north-easterly winds, have been investigated for the period 2002/2003 to 2013/2014 using thermal infrared satellite imagery. Thin-ice thicknesses were calculated from MODIS ice-surface temperatures, combined with ECMWF ERA-Interim atmospheric reanalysis data in an energy-balance model. Based on calculated thin-ice thicknesses, associated quantities like polynya area and total ice production were derived and compared to previous remote sensing and modeling studies. A basic coverage-correction scheme was applied to account for cloud-gaps in the daily composites. The sea ice in the Storfjorden area experiences a late fall freeze-up in several years over the 12 winter-period, with an increasing frequency of large polynya events until the end of December. During the regarded period, the mean polynya area is 4555.7 ± 1542.9 km2. The average ice production in the fjord is estimated with 28.3 ± 8.5 km3 per winter and therefore lower than in previous studies. Despite this comparatively short record of 12 winter-seasons, a significant positive trend of 20.2 km3 per decade could be detected, which contrasts earlier reports of a slightly negative trend in accumulated ice production prior to 2002. Derived estimates underline the importance of this relatively small coastal polynya system considering its contribution to the cold halocline layer through salt release during ice formation processes.
    Print ISSN: 1994-0432
    Electronic ISSN: 1994-0440
    Topics: Geography , Geosciences
    Published by Copernicus on behalf of European Geosciences Union.
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  • 10
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    Late Glacial and Holocene aeolian sands and soil formation from the Pomeranian outwash plain (Mecklenburg, NE-Germany) (2010)
    Copernicus
    Details
    Publication Date: 2010-07-10
    Description: Anhand von zwei Dünenprofilen wird die Art, Dauer und Intensität von spätglazialen und holozänen Flugsand- und Bodenbildungen innerhalb des Pommerschen Sandergebietes dargestellt. Hierfür wurde ein interdisziplinärer Ansatz aus Sedimentologie, Pedologie, Palynologie und Geochronologie verwendet. Während des Spätglazials kommen auf den Sanderhochflächen flache Flugsanddecken zur Ablagerung, unterbrochen durch die Bildung des Finowbodens. Durch die Ausbreitung einer geschlossenen Vegetationsdecke im Frühholozän, erfolgt eine Stabilisierung der Reliefoberfläche mit anschließender Bodenbildung. Nach intensiven mittelalterlichen Rodungen werden die Oberflächen erneut destabilisiert. Es kommt zur partiellen Aufarbeitung der Flugsande resultierend in Dünenbildungen und einem kuppigen Relief. Eine der untersuchten Dünen wurde dabei komplett im späten Subatlantikum gebildet. Diese Studie unterstreicht die zeitlich-räumliche Variabilität äolischer Aktivität, wobei Umlagerungen entsprechender Korngrößen während verschiedener Phasen nach der Deglaziation ermöglicht wurden.
    Print ISSN: 0424-7116
    Electronic ISSN: 2199-9090
    Topics: Geosciences , History
    Published by Copernicus on behalf of Deutsche Quartärvereinigung.
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