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  • 1
    Electronic Resource
    Electronic Resource
    Mechanical degradation of mica during processing with polypropylene (1984)
    Brookfield, Conn. : Wiley-Blackwell
    Polymer Composites 5 (1984), S. 264-276 
    Details
    ISSN: 0272-8397
    Keywords: Chemistry ; Chemical Engineering
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics
    Notes: Mechanical degradation of reinforcing fillers during processing is a problem that has been seldom studied due to a lack of particle size determination techniques. Using phlogopite mica as an example, a method allowing a rapid and accurate characterization of flake size and aspect ratio will be described. The influence of several parameters on the mechanical degradation of mica flakes in a mica/polypropylene system has been studied using a laboratory roller blade mixer. The degradation was found to occur in two stages. The first stage takes place immediately after the addition of mica, where the average flake size decreases very rapidly by as much as 20 percent. In the second stage, the particle size remains essentially constant with the time of mixing at low concentrations (2 percent wt); at higher concentrations (40 percent wt) there is a slow reduction in the flake size. The influence of other parameters such as system viscosity, mode of mica addition, silane treatment, and the initial particle size is also discussed.
    Additional Material: 21 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/pc.750050406
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  • 2
    Electronic Resource
    Electronic Resource
    Factors affecting the surface texture in extruded mica-polypropylene composites (1984)
    Brookfield, Conn. : Wiley-Blackwell
    Polymer Composites 5 (1984), S. 299-306 
    Details
    ISSN: 0272-8397
    Keywords: Chemistry ; Chemical Engineering
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics
    Notes: A Taylor-Hobson Talysurf instrument was used to quantify the surface roughness of phlogopite mica-polypropylene extrudates. The rate of feeding and the speed of rotation of the screw were found to have a significant effect on the surface texture. Under the appropriate conditions of extrusion the roughness of 40 percent (by weight) mica-filled polypropylene extrudates could be reduced by a factor of three. This effect was found to be independent of the extrusion rate.
    Additional Material: 13 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/pc.750050409
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  • 3
    Electronic Resource
    Electronic Resource
    Rotary injection reaction injection molding (RI-RIM). Part II: Interfacial segregation of release systems (1990)
    Stamford, Conn. [u.a.] : Wiley-Blackwell
    Polymer Engineering and Science 30 (1990), S. 175-186 
    Details
    ISSN: 0032-3888
    Keywords: Chemistry ; Chemical Engineering
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology , Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics , Physics
    Notes: This paper describes the shear imposed interfacial segregation of release systems for the facilitated attenuation of polyurethane (PU) adhesion to metal coun-terfaces using a RI-RIM system. It is shown that the migration rate of the dispersed release additives due to a shear imposed stress in the resin fluid is much greater than that arising from Fickian diffusion, thereby removing a vital constraint from conventional practice. The novel rotary injection RIM system is presented to simulate the on-line injection and shear induced interfacial segregation in model PU/abherent systems. A wide range of recipes comprising single (liquids or solids) and multicomponent (liquid-liquid and solid-liquid) release materials were injected into the polymerizing resin mixture to provide cohesively weak and friable “particle” boundary layer assemblies at the PU/metal interface. An instrumented Blister Test was employed to evaluate the quality of the molded interfaces in terms of adhesion and the concentration distribution of the injected species in the final cured moldings was determined through high pressure liquid chromatography (HPLC). A comparison of the results on the shear modified and the compounded interfaces confirm an accentuated lateral migration of the additives to the interface resulting in an appreciable diminution in the adhesion of the system. Finally, transport models are suggested to account for the observed augmented transport.
    Additional Material: 12 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/pen.760300307
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  • 4
    Electronic Resource
    Electronic Resource
    A personal computer software program for coathanger die simulation (1994)
    Stamford, Conn. [u.a.] : Wiley-Blackwell
    Polymer Engineering and Science 34 (1994), S. 657-664 
    Details
    ISSN: 0032-3888
    Keywords: Chemistry ; Chemical Engineering
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology , Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics , Physics
    Notes: A good extrusion die must distribute the polymer melt in the flow channel such that the material exits from the die with a uniform velocity and temperature. Coathanger dies are commonly used for the extrusion of plastic sheets and films. The die is usually provided with a straining bar allowing a regulation of the flowrate in the case of a poor design. But this, in turn, can affect temperature uniformity. Therefore, the design of coathanger die is a complex task which is mainly accomplished by trial and error in industry. Analyses of the flow in coathanger dies have been reported in the literature. Analytical and numerical approaches are used to solve this problem. The first one involves many simplifying assumptions: the most important ones being the unidirectional and isothermal flow of the polymer. Most numerical methods deal with a 2-D geometry, but only a few of them have considered the non-isothermal flow. A new model has been developed using a modified FAN method (Flow Analysis Network introduced by Tadmor) for the calculation of the 2-D flow, coupled with a finite-difference scheme for the calculation of temperature. The overall model can run on a PC with only a few minutes of calculation. Good agreement was obtained between experimental data and simulations.
    Additional Material: 16 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/pen.760340807
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  • 5
    Electronic Resource
    Electronic Resource
    Mechanical properties in multidimensional composites (1991)
    Stamford, Conn. [u.a.] : Wiley-Blackwell
    Polymer Engineering and Science 31 (1991), S. 40-46 
    Details
    ISSN: 0032-3888
    Keywords: Chemistry ; Chemical Engineering
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology , Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics , Physics
    Notes: The mechanical properties of three dimensional stitched composites were compared against those of the traditional two dimensional laminates. An attempt was made to correlate the change in properties to the change in the third directional fiber density. Tests conducted were the impact, three-point bending, damage tolerance, end notched flexure, and bending fatigue test. The results of these tests show that the third directional fibers can effectively inhibit delamination by increasing the interlaminar shear strength. Three dimensional composites also possess better damage tolerance, fracture toughness, and fatigue life. However, a high stitching density can degrade the in-plane properties of the composites.
    Additional Material: 5 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/pen.760310108
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  • 6
    Electronic Resource
    Electronic Resource
    Injection molding of polypropylene/polycarbonate blends (1990)
    Stamford, Conn. [u.a.] : Wiley-Blackwell
    Polymer Engineering and Science 30 (1990), S. 1051-1055 
    Details
    ISSN: 0032-3888
    Keywords: Chemistry ; Chemical Engineering
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology , Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics , Physics
    Notes: This work deals with the effects of material and processing parameters on the mechanical behavior and morphology of noncompatlbilized polypropylene-polycarbonate (PP-PC) blends. The blends containing between 0 and 40 vol. percent of polycarbonate were compounded using a twin screw extruder and converted by injection molding using molds with rectangular as well as dogbone shaped cavities. The blends exhibit a complex skin-core morphology which evolves with the composition. Despite the absence of interfacial adhesion, the low strain modulus increases with PC concentration and follows approximately the Takayanagi model for systems with perfect adhesion. A slight increase of stiffness and strength with increasing PP/PC viscosity ratio is also observed. Weldline strength of these blends is generally poor and decreases with the increasing PC concentration.
    Additional Material: 11 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/pen.760301708
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  • 7
    Electronic Resource
    Electronic Resource
    Nonlinear model-predictive control: Closed-loop stability analysis (1996)
    Hoboken, NJ : Wiley-Blackwell
    AIChE Journal 42 (1996), S. 3388-3402 
    Details
    ISSN: 0001-1541
    Keywords: Chemistry ; Chemical Engineering
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology , Process Engineering, Biotechnology, Nutrition Technology
    Notes: A method to analyze the closed-loop stability of a system composed of a nonlinear process and a discrete controller is developed. The closed-loop system is described by a set of difference equations resulting from the discretization of the continuous-time model. A commonly used method of discretization (forward difference) offers an incorrect relative order compared to exact discretization. The state and input sensitivity equations of the continuous-time model are used in computing the nominal closed-loop stability criteria. The nominal stability analysis is extended to the important cases of unmeasured states and uncertain model parameters. A numerical Lyapunov function is used to estimate closed-loop regions of attraction. A simulation example (a CSTR with input multiplicity) presented illustrates the analysis methods and closed-loop behavior.
    Additional Material: 11 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/aic.690421210
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  • 8
    Electronic Resource
    Electronic Resource
    Sludge suspension in waste storage tanks (1989)
    Hoboken, NJ : Wiley-Blackwell
    AIChE Journal 35 (1989), S. 1391-1394 
    Details
    ISSN: 0001-1541
    Keywords: Chemistry ; Chemical Engineering
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology , Process Engineering, Biotechnology, Nutrition Technology
    Additional Material: 3 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/aic.690350820
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  • 9
    Electronic Resource
    Electronic Resource
    Letters to the editor (1992)
    Hoboken, NJ : Wiley-Blackwell
    AIChE Journal 38 (1992), S. 635-640 
    Details
    ISSN: 0001-1541
    Keywords: Chemistry ; Chemical Engineering
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology , Process Engineering, Biotechnology, Nutrition Technology
    Additional Material: 2 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/aic.690380421
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  • 10
    Electronic Resource
    Electronic Resource
    Turbulence structure in bubble disengagement zone: Role of polymer addition (1995)
    Hoboken, NJ : Wiley-Blackwell
    AIChE Journal 41 (1995), S. 1329-1332 
    Details
    ISSN: 0001-1541
    Keywords: Chemistry ; Chemical Engineering
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology , Process Engineering, Biotechnology, Nutrition Technology
    Additional Material: 5 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/aic.690410529
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