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  • Institute of Physics  (33)
  • American Society of Hematology  (18)
  • Wiley-Blackwell  (18)
  • 2005-2009
  • 2000-2004
  • 1995-1999  (28)
  • 1990-1994  (41)
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  • 1999  (28)
  • 1994  (41)
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  • 2005-2009
  • 2000-2004
  • 1995-1999  (28)
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  • 1
    Electronic Resource
    Electronic Resource
    Effect of sample size on the microwave heating rate: Oil vs. water (1994)
    Hoboken, NJ : Wiley-Blackwell
    AIChE Journal 40 (1994), S. 1433-1439 
    Details
    ISSN: 0001-1541
    Keywords: Chemistry ; Chemical Engineering
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology , Process Engineering, Biotechnology, Nutrition Technology
    Notes: It is generally believed that oil samples heat faster in a microwave oven than do water samples of the same mass. For sufficiently large and thich samples this conventional wisdom is indeed correct, but this trend can be far from true in smaller samples. In a commercially-made home microwave oven, we observed that with decreasing sample size the heating rate of a water sample increases much faster than that of an oil sample. At 50 g the heating rate of a water sample is several times greater than that of an oil sample. Additionally, in studies of cylindrical samples in a customized oven having a unidirectional microwave source, the heating rate of water samples smaller than 2.4 cm in radius is greater than that of oil samples and is a strongly oscillatory increasing function of decreasing sample radius. Combining Maxwell's theory of microwave penetration and the heat conduction equation, we show that this previously unreported oscillatory heating behavior results from the added power absorbed by samples due to resonant absorption of microwaves. The added power arises from standing waves produced by internally reflected microwaves. This effect is small for oil because only 3% of the microwave power is reflected at an oil-air interface. On the other hand, 64% is reflected at a water-air interface, which causes strong resonant heating. Our findings might prove to be useful for future consumer food product development or oven design.
    Additional Material: 6 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/aic.690400902
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  • 2
    Electronic Resource
    Electronic Resource
    Microwave driven convection in a square cavity (1994)
    Hoboken, NJ : Wiley-Blackwell
    AIChE Journal 40 (1994), S. 1268-1272 
    Details
    ISSN: 0001-1541
    Keywords: Chemistry ; Chemical Engineering
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology , Process Engineering, Biotechnology, Nutrition Technology
    Additional Material: 7 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/aic.690400718
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  • 3
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    Vibration isolation and suppression system for precision payloads in space (1999)
    Institute of Physics
    Details
    Publication Date: 1999-12-01
    Print ISSN: 0964-1726
    Electronic ISSN: 1361-665X
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics
    Published by Institute of Physics
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    PAPER CURRENT
  • 4
    Electronic Resource
    Electronic Resource
    Iodine binding by amylopectin and stability of the amylopectin-iodine complex (1994)
    Bognor Regis [u.a.] : Wiley-Blackwell
    Journal of Polymer Science Part A: Polymer Chemistry 32 (1994), S. 2267-2274 
    Details
    ISSN: 0887-624X
    Keywords: amylopectin, iodine binding capacity ; amylopectin, iodine binding energy of ; iodine binding and amylopectin fine structures ; Amylose-iodine and amylopectin-iodine complexes of fixed composition ; peak shift in amylose-iodine spectrum and different iodine species ; Chemistry ; Polymer and Materials Science
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology
    Notes: The iodine binding capacity (IBC) of amylopectin (AP, from potatoes) is determined to be around 0.38% (w/w) of the total AP in the solution. The mass of iodine bound comprises about 13.6% of the mass of AP involved with the complex, suggesting that with every four iodine atoms bound there are 23 anhydroglucose residues (AGU). Since our previous study indicates that four iodine atoms within the helix of 11 AGUs form a chromophore unit in the API complex, only 48% of the AGUs (11 out of 23) in the AP molecule are directly involved with the iodine. The heat of reaction for the API complex formation is determined to be around -47 kJ/mol of I-I units bound and is significantly lower in magnitude than that of the amylose-iodine (AI) complex [Biopolymers, 31, 57 (1991)]. A possible mechanism has been proposed for the formation of AI and API complexes with fixed compositions. © 1994 John Wiley & Sons, Inc.
    Additional Material: 6 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/pola.1994.080321208
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  • 5
    Electronic Resource
    Electronic Resource
    Determining the chromophore in the amylopectin-iodine complex by theoretical and experimental studies (1994)
    Bognor Regis [u.a.] : Wiley-Blackwell
    Journal of Polymer Science Part A: Polymer Chemistry 32 (1994), S. 2257-2265 
    Details
    ISSN: 0887-624X
    Keywords: helix in amylopectin-iodine complex ; I4 unit in amylopectin-iodine complex ; spectra of amylopectin-iodine complex ; amylopectin-iodine chromophore composition ; amylopectin fine structures and complex formation ; Chemistry ; Polymer and Materials Science
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology
    Notes: A partial hydrolysis of amylose followed by the addition of iodine provides a spectrum almost identical to that of the amylopectin-iodine (API) complex suggesting the involvement of smaller “amylose-like” units in the API complex. Our theoretical studies on different polyiodine and polyiodide species suggest that a nearly linear I4 unit stabilized within the cavity of a small “amylose-like” helix is responsible for the characteristic API spectrum. Since there are 2.75 anhydroglucose residues (AGU) for every iodine atom in the amylose-iodine (AI) complex and a structural similarity exists between the API and the AI (amylose-iodine) complexes, we identify (C6H10O5)11I4 to be the chromophore in the API complex. © 1994 John Wiley & Sons, Inc.
    Additional Material: 6 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/pola.1994.080321207
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  • 6
    Electronic Resource
    Electronic Resource
    Hindered settling function with no empirical parameters for polydisperse suspensions (1994)
    Hoboken, NJ : Wiley-Blackwell
    AIChE Journal 40 (1994), S. 570-575 
    Details
    ISSN: 0001-1541
    Keywords: Chemistry ; Chemical Engineering
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology , Process Engineering, Biotechnology, Nutrition Technology
    Additional Material: 6 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/aic.690400317
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  • 7
    Electronic Resource
    Electronic Resource
    New lattice model for adsorption of small molecules in zeolite micropores (1994)
    Hoboken, NJ : Wiley-Blackwell
    AIChE Journal 40 (1994), S. 925-934 
    Details
    ISSN: 0001-1541
    Keywords: Chemistry ; Chemical Engineering
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology , Process Engineering, Biotechnology, Nutrition Technology
    Notes: A new adsorption model is developed for small molecules in zeolites whose form is based on features revealed by molecular simulation. Adsorption is assumed to occur onto a 3-D polyhedral lattice, and both the energy and entropy of the lattice sites are accounted for using a statistical mechanics approach. Energetic interactions are described by an Ising model with both 2- and multibody nearest-neighbor in-teractions. Entropic interactions are included by an adsorption site volume term which accounts for the loss of traslational freedom associated with lattice crowding.The model is applied to a system of small molecules (xenon, methane) adsorbed in idealized zeolite NaA, where adsorption has been shown by computer simulation to occur on finite, cuboctahedral lattices (Van Tassel et al., 1992). The model quantitavely predicts the simulated isotherm over the entire pressure range. Comparison is made with a Langmuir model and a van der Waals gas model which, although valid at low pressures, fail at high pressures due to overestimation of translational entropy and inaccurate portrayal of sorbate-sorbate interaction energy.
    Additional Material: 16 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/aic.690400603
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  • 8
    Electronic Resource
    Electronic Resource
    A Novel Sensitive Colorimetric Assay for Visual Detection of Solid-Phase Bound Amines (1999)
    Weinheim : Wiley-Blackwell
    Liebigs Annalen 1999 (1999), S. 2787-2791 
    Details
    ISSN: 1434-193X
    Keywords: Solid-phase peptide synthesis ; Disperse Red 1 ; p-Nitrophenyl ester ; Chemistry ; General Chemistry
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology
    Notes: A new simple and efficient method for the detection of incomplete coupling reactions during solid-phase peptide synthesis is decribed. Using p-nitrophenyl ester 1 (NF31), free amino groups can be visually detected on the resin by direct coloring of the beads. A specific feature of the assay resides in the possibility of detection of sterically hindered primary amines.
    Additional Material: 3 Ill.
    Type of Medium: Electronic Resource
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  • 9
    Electronic Resource
    Electronic Resource
    Ab initio molecular orbital calculations on the transition state for the addition of a methyl radical to vinyl monomers (1994)
    Weinheim : Wiley-Blackwell
    Macromolecular Theory and Simulations 3 (1994), S. 905-913 
    Details
    ISSN: 1022-1344
    Keywords: Chemistry ; Polymer and Materials Science
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology , Physics
    Notes: Ab initio molecular orbital calculations have been performed on the transition state for the addition of methyl radical to twelve vinyl monomers using the SV 3-21G basis set. A linear relationship has been found between the calculated energies of activation and previously calculated energies of reaction. This supports the assumption of an Evans-Polanyi type rule in previous work which attempted to correlate reactivity with calculated energies of reaction. The activation energies obtained for methyl addition to butadiene and styrene were calculated to be negative. This is caused by errors introduced by a number of sources, viz. basis set superposition error, spin contamination and zero point energy. These errors are discussed. Previous authors have reported reasonable agreement between calculated activation energies at SV3-21G and experimental values for methyl addition to ethylene, this work suggests that this agreement was coincidental and results from the fortuitous cancellation of errors. The nature of the transition state for these radical addition reactions is discussed and the limitations of the SV3-21G basis set are highlighted. The theoretical prediction of activation energies for radical addition reactions would require much larger calculations, beyond the computational means of most research laboratories.
    Additional Material: 5 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/mats.1994.040030507
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  • 10
    Electronic Resource
    Electronic Resource
    Cytogenetic, cellular, and developmental consequences of cryopreservation of immature and mature mouse and human oocytes (1994)
    New York, NY [u.a.] : Wiley-Blackwell
    Microscopy Research and Technique 27 (1994), S. 165-193 
    Details
    ISSN: 1059-910X
    Keywords: Cryopreservation ; Mammalian oocyte ; Cytogenetics ; Fertilization ; Embryogenesis ; Life and Medical Sciences ; Cell & Developmental Biology
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Natural Sciences in General
    Notes: This study examined the effects of cryopreservation on cellular organization, chromosomal complement, and developmental potential of immature and mature mouse and human oocytes. Chromosomal analyses were performed by DNA fluorescence microscopy and karyotyping on the same metaphase II-stage oocytes before and after freezing. Cellular analyses involved electron microscopy, time-lapse video recording, and fluorescent-probe microscopy of cortical granules. The findings demonstrate that while profound cytoplasmic, nuclear, and nucleolar alterations occur in the immature oocyte during cryopreservation, an apparently normal nucleus and cytoplasm is re-established progressively after thawing and culture. The resulting oocytes mature at high frequency and for the mouse, are fertilizable and capable of normal preimplantation of embryogenesis. Cryopreservation of mature mouse and human oocytes is not accompanied by a significant increase in the frequency of aneuploidy. However, cryopreserved human oocytes, while fertilizable, arrest development during the early cleavage stages and display aberrant patterns of cytokinesis. The possible etiologies of developmental failure in the human embryo that may be related to oocyte cryopreservation, as well as the potential benefits of cryopreservation of the immature oocyte, are discussed with respect to clinical and commercial applications. © 1994 Wiley-Liss, Inc.
    Additional Material: 118 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/jemt.1070270209
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