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  • INSTRUMENTATION AND PHOTOGRAPHY  (60)
  • Analytical Chemistry and Spectroscopy  (46)
  • SPACE SCIENCES
  • 1990-1994
  • 1975-1979  (106)
  • 1970-1974
  • 1976  (106)
Collection
Keywords
Publisher
Years
  • 1990-1994
  • 1975-1979  (106)
  • 1970-1974
Year
  • 1
    Electronic Resource
    Electronic Resource
    La résonance magnétique du 77Se dans des composés organiques (1976)
    Chichester : Wiley-Blackwell
    Organic Magnetic Resonance 8 (1976), S. 354-356 
    Details
    ISSN: 0030-4921
    Keywords: Chemistry ; Analytical Chemistry and Spectroscopy
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology
    Description / Table of Contents: 77Se n.m.r. spectra of twenty-six organoselenium compounds, including some with an endocyclic selenium atom, have been recorded. Our measurements complete the scale of chemical shifts previously established by McFarlane. It seems difficult to define a range of chemical shifts which is characteristic of the valency state of selenium or of its endo- or exocyclic position. Some results are discussed qualitatively. In the case of selenolo[2,3-b]thiophene, evidence has been obtained for a 4J[Se, H] coupling across the sulphur atom.
    Notes: La résonance magnétique du 77Se a été observée dans vingt-six composés organiques dont certains contiennent un atome de sélénium endocyclique. Nous avons pu ainsi compléter l'échelle de déplacements chimiques établie par McFarlane. II apparaît difficile de définir une gamme de déplacement chimique du 77Se caractéristique de son état de valence ou de sa position endo- ou exocyclique. Certains résultats sont discutés qualitativement. Dans le cas du sélénolo [2,3-b]thiophène, des arguments en faveur d'un couplage 4J(Se, H) à travers l'atome de soufre ont été découverts.
    Additional Material: 4 Tab.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/mrc.1270080706
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    Paper (German National Licenses)
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  • 2
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    Laboratory calibration of AAFE radiometer/scatterometer (RADSCAT) (1976)
    In:  CASI
    Details
    Publication Date: 2019-06-27
    Description: A brief description of the electrical and mechanical instrument configuration, followed by an extensive discussion of laboratory tests and results are contained herein. This information is required to provide parameters for data reduction, and a basis for analysis of the measurement errors in data taken with this instrument.
    Keywords: INSTRUMENTATION AND PHOTOGRAPHY
    Type: NASA-TM-X-73900
    Format: application/pdf
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  • 3
    Electronic Resource
    Electronic Resource
    Derivatization of aminoalkylphosphonic acids for characterization by gas chromatography mass spectrometry (1976)
    Chichester : Wiley-Blackwell
    Biological Mass Spectrometry 3 (1976), S. 28-31 
    Details
    ISSN: 1052-9306
    Keywords: Chemistry ; Analytical Chemistry and Spectroscopy
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology
    Notes: A general derivatization method has been developed for both primary and secondary aminoalkylphosphonic acids. Derivatization is effected by reaction with trifluoroacetic acid and trifluoroacetic acid anhydride followed by esterification using ethereal diazo-n-butane. This method can be used for microgram quantities and permits ready characterization by both gas chromatography and gas chromatography mass spectrometry. The structure of this derivative has been verified by mass spectrometry and proton magnetic resonance. Fragmentation patterns were confirmed by high resolution mass spectrometry, isotope labeling and the formation of derivative analogs.
    Additional Material: 5 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/bms.1200030106
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    Paper (German National Licenses)
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  • 4
    Electronic Resource
    Electronic Resource
    The structure of narasin and a related ionophore (1976)
    Chichester : Wiley-Blackwell
    Biological Mass Spectrometry 3 (1976), S. 272-277 
    Details
    ISSN: 1052-9306
    Keywords: Chemistry ; Analytical Chemistry and Spectroscopy
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology
    Notes: Using electron impact and field desorption mass spectrometry, structures are proposed for narasin and a related ionophore, A28086B, derived from fermentation. The ionic fragmentation of these compounds and their derivatives is discussed and compared with that of salinomycin, whose structure has been determined by X-ray diffraction.
    Additional Material: 6 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/bms.1200030604
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  • 5
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    Readout electrode assembly for measuring biological impedance (1976)
    In:  CASI
    Details
    Publication Date: 2019-06-27
    Description: The invention comprises of a pair of readout ring electrodes which are used in conjunction with apparatus for measuring the electrical impedance between different points in the body of a living animal to determine the amount of blood flow therebetween. The readout electrodes have independently adjustable diameters to permit attachment around different parts of the body between which it is desired to measure electric impedance. The axial spacing between the electrodes is adjusted by a pair of rods which have a first pair of ends fixedly attached to one electrode and a second pair of ends slidably attached to the other electrode. Indicia are provided on the outer surface of the ring electrodes and on the surface of the rods to permit measurement of the circumference and spacing between the ring electrodes.
    Keywords: INSTRUMENTATION AND PHOTOGRAPHY
    Format: application/pdf
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  • 6
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    Static coefficient test method and apparatus (1976)
    In:  CASI
    Details
    Publication Date: 2019-06-27
    Description: The static coefficient of friction between contacting surfaces of a plurality of bodies is determined by applying a load to the bodies in a direction normal to the contacting surfaces. Opposite ends of a flexible filament are connected to a load cell and the first of the bodies. A motor continuously moves the second of the bodies away from the load cell at constant velocity at right angles to the force of the normal load so that the first body moves intermittently relative to the second body across a contact surface between them. The load on the surfaces, the nature of the surfaces, and the speed of the first body relative to the load cell are such that the filament is alternately and cyclically tensioned and relaxed as the movement occurs. The maximum tension occurs at the incipient stages of movement of the first body relative to the second body. The load cell derives a series of measurements which are coupled to an x-y recorder, from which the maximum forces of the filament are determined to enable the static coefficient of friction to be determined. From the maximum forces and the normal force, the coefficient is determined. For determining coefficients of friction where there are large compression loads, the normal load is applied with a calibrated compression spring that is deflected by a predetermined amount determined by a spring load vs. deflection calibration curve.
    Keywords: INSTRUMENTATION AND PHOTOGRAPHY
    Format: application/pdf
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  • 7
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    Particulate and aerosol detector (1976)
    In:  CASI
    Details
    Publication Date: 2019-06-27
    Description: A device is described for counting aerosols and sorting them according to either size, mass or energy. The component parts are an accelerator, a capacitor sensor and a readout. The accelerator is a means for accelerating the aerosols toward the face of the capacitor sensor with such force that they partially penetrate the capacitor sensor, momentarily discharging it. The readout device is a means for counting the number of discharges of the capacitor sensor and measuring the amplitudes of these different discharges. The aerosols are accelerated by the accelerator in the direction of the metal layer with such force that they penetrate the metal and damage the oxide layers, thereby allowing the electrical charge on the capacitor to discharge through the damaged region. Each incident aerosol initiates a discharge path through the capacitor in such a fashion as to vaporize the conducting path. Once the discharge action is complete, the low resistance path no longer exists between the two capacitor plates and the capacitor is again able to accept a charge. The active area of the capacitor is reduced in size by the damaged area each time a discharge occurs.
    Keywords: INSTRUMENTATION AND PHOTOGRAPHY
    Format: application/pdf
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  • 8
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    A demonstration of an independent-station radio interferometry system with 4-cm precision on a 16-km base line (1976)
    In:  Other Sources
    Details
    Publication Date: 2019-06-27
    Description: Radio interferometry promises eventually to measure directly, with accuracies of a few centimeters, both whole earth motions and relative crustal motions with respect to an 'inertial' reference frame. Interferometry measurements of arbitrarily long base lines require, however, the development of new techniques for independent-station observation. In connection with the development of such techniques, a series of short base line demonstration experiments has been conducted between two antennas. The experiments were related to a program involving the design of independent-station instrumentation capable of making three-dimensional earth-fixed base line measurements with an accuracy of a few centimeters. Attention is given to the instrumentation used in the experiments, aspects of data analysis, and the experimental results.
    Keywords: INSTRUMENTATION AND PHOTOGRAPHY
    Type: Journal of Geophysical Research; 81; Feb. 10
    Format: text
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  • 9
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    Hand-held spectral radiometer to estimate gramineous biomass (1976)
    In:  Other Sources
    Details
    Publication Date: 2019-06-27
    Description: A simple hand-held instrument has been designed and constructed to nondestructively estimate above-ground gramineous biomass using radiometric measurements. The prototype unit consists of a modified two-channel digital radiometer interfaced to a pocket calculator. A digital interface was constructed to join electronically and control the radiometer and calculator to enable the radiometer-calculator system to solve a linear conversion solution from radiometric units to estimated biomass. This instrument has been used to estimate radiometrically gramineous biomass in a more efficient fashion with a high degree of accuracy.
    Keywords: INSTRUMENTATION AND PHOTOGRAPHY
    Type: Applied Optics; 15; Feb. 197
    Format: text
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  • 10
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    Vector magnetometer design study: Analysis of a triaxial fluxgate sensor design demonstrates that all MAGSAT Vector Magnetometer specifications can be met (1976)
    In:  CASI
    Details
    Publication Date: 2019-06-27
    Description: The design of the vector magnetometer selected for analysis is capable of exceeding the required accuracy of 5 gamma per vector field component. The principal elements that assure this performance level are very low power dissipation triaxial feedback coils surrounding ring core flux-gates and temperature control of the critical components of two-loop feedback electronics. An analysis of the calibration problem points to the need for improved test facilities.
    Keywords: INSTRUMENTATION AND PHOTOGRAPHY
    Type: NASA-CR-144825
    Format: application/pdf
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